/home/gencode/cen/w12877p4/12877p4 1 12811 | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |[.]
Trang 1|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
12877-4:2000
The European Standard EN 12877-4:1999 has the status of a
British Standard
ICS 83.040.30
NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW
Colouring materials in
plastics Ð
Determination of colour
stability to heat during
processing of colouring
materials in plastics Ð
Part 4: Determination by two-roll milling
Trang 2This British Standard, having
been prepared under the
direction of the Sector
Committee for Materials and
Chemicals, was published under
the authority of the Standards
Committee and comes into effect
on 15 January 2000
BSI 01-2000
ISBN 0 580 35857 7
BS EN 12877-4:2000
Amendments issued since publication
National foreword
This British Standard is the English language version of EN 12977-4:1999
The UK participation in its preparation was entrusted to Technical Committee STI/1, Pigments, which has the responsibility to:
Ð aid enquirers to understand the text;
Ð present to the responsible European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed;
Ð monitor related international and European developments and promulgate them in the UK
A list of organizations represented on this committee can be obtained on request to its secretary
Cross-references
The British Standards which implement international or European publications referred to in this document may be found in the BSI Standards Catalogue under the section entitled ªInternational Standards Correspondence Indexº, or by using the ªFindº facility of the BSI Standards Electronic Catalogue
A British Standard does not purport to include all the necessary provisions of a contract Users of British Standards are responsible for their correct application
Compliance with a British Standard does not of itself confer immunity from legal obligations.
Summary of pages
This document comprises a front cover, an inside front cover, the EN title page, pages 2 to 4, an inside back cover and a back cover
The BSI copyright notice displayed in this document indicates when the document was last issued
Trang 31250((8523e(11(
(8523b,6&+(1250
(1
2FWREHU
,&6
(QJOLVKYHUVLRQ
&RORXULQJPDWHULDOVLQSODVWLFV'HWHUPLQDWLRQRIFRORXUVWDELOLW\
WRKHDWGXULQJSURFHVVLQJRIFRORXULQJPDWHULDOVLQSODVWLFV
3DUW'HWHUPLQDWLRQE\WZRUROOPLOOLQJ
0DWLqUHVFRORUDQWHVGDQVOHVSODVWLTXHV'pWHUPLQDWLRQGH
ODVWDELOLWpGHODFRXOHXUjODFKDOHXUDXFRXUVGHODPLVHHQ
RHXYUHGHVPDWLqUHVFRORUDQWHVGDQVOHVSODVWLTXHV
3DUWLH'pWHUPLQDWLRQSDUFDODQGUDJHVXUELF\OLQGUH
)DUEPLWWHOLQ.XQVWVWRIIHQ%HVWLPPXQJGHU%HVWlQGLJNHLW GHU)DUEHJHJHQ+LW]HEHLP9HUDUEHLWHQYRQ)DUEPLWWHOQLQ XQVWVWRIIHQ7HLO%HVWLPPXQJLP'DXHUZDO]WHVW
7KLV(XURSHDQ6WDQGDUGZDVDSSURYHGE\&(1RQ6HSWHPEHU
&(1PHPEHUVDUHERXQGWRFRPSO\ZLWKWKH&(1&(1(/(&,QWHUQDO5HJXODWLRQVZKLFKVWLSXODWHWKHFRQGLWLRQVIRUJLYLQJWKLV(XURSHDQ 6WDQGDUGWKHVWDWXVRIDQDWLRQDOVWDQGDUGZLWKRXWDQ\DOWHUDWLRQ8SWRGDWHOLVWVDQGELEOLRJUDSKLFDOUHIHUHQFHVFRQFHUQLQJVXFKQDWLRQDO VWDQGDUGVPD\EHREWDLQHGRQDSSOLFDWLRQWRWKH&HQWUDO6HFUHWDULDWRUWRDQ\&(1PHPEHU
7KLV(XURSHDQ6WDQGDUGH[LVWVLQWKUHHRIILFLDOYHUVLRQV(QJOLVK)UHQFK*HUPDQ$YHUVLRQLQDQ\RWKHUODQJXDJHPDGHE\WUDQVODWLRQ XQGHUWKHUHVSRQVLELOLW\RID&(1PHPEHULQWRLWVRZQODQJXDJHDQGQRWLILHGWRWKH&HQWUDO6HFUHWDULDWKDVWKHVDPHVWDWXVDVWKHRIILFLDO YHUVLRQV
&(1PHPEHUVDUHWKHQDWLRQDOVWDQGDUGVERGLHVRI$XVWULD%HOJLXP&]HFK5HSXEOLF'HQPDUN)LQODQG)UDQFH*HUPDQ\*UHHFH ,FHODQG,UHODQG,WDO\/X[HPERXUJ1HWKHUODQGV1RUZD\3RUWXJDO6SDLQ6ZHGHQ6ZLW]HUODQGDQG8QLWHG.LQJGRP
(8523($1 &200,77(( )25 67$1'$5',=$7,21
& 2 0 , 7 e ( 8 5 2 3 e ( 1 ' ( 1 2 5 0 $ / , 6 $ 7 , 2 1 ( 8 5 2 3 b, 6 &+ ( 6 2 0 , 7 ( ( ) h 5 12 5 0 8 1 *
&HQWUDO6HFUHWDULDWUXHGH6WDVVDUW%%UXVVHOV
&(1 $OOULJKWVRIH[SORLWDWLRQLQDQ\IRUPDQGE\DQ\PHDQVUHVHUYHG
Trang 4(1
%6,
)RUHZRUG
7KLV (XURSHDQ 6WDQGDUG KDV EHHQ SUHSDUHG E\ 7HFKQLFDO &RPPLWWHH &(17& 3LJPHQWV DQG H[WHQGHUV WKH 6HFUHWDULDWRIZKLFKLVKHOGE\',1
7KLV(XURSHDQ6WDQGDUGVKDOOEHJLYHQWKHVWDWXVRIDQDWLRQDOVWDQGDUGHLWKHUE\SXEOLFDWLRQRIDQLGHQWLFDOWH[WRUE\ HQGRUVHPHQW DW WKH ODWHVW E\ $SULO DQG FRQIOLFWLQJ QDWLRQDO VWDQGDUGV VKDOO EH ZLWKGUDZQ DW WKH ODWHVW E\
$SULO
$FFRUGLQJWRWKH&(1&(1(/(&,QWHUQDO5HJXODWLRQVWKHQDWLRQDOVWDQGDUGVRUJDQL]DWLRQVRIWKHIROORZLQJFRXQWULHV DUH ERXQG WR LPSOHPHQW WKLV (XURSHDQ 6WDQGDUG $XVWULD %HOJLXP &]HFK 5HSXEOLF 'HQPDUN )LQODQG )UDQFH
*HUPDQ\ *UHHFH ,FHODQG ,UHODQG ,WDO\ /X[HPERXUJ 1HWKHUODQGV 1RUZD\ 3RUWXJDO 6SDLQ 6ZHGHQ 6ZLW]HUODQG DQGWKH8QLWHG.LQJGRP
,QWURGXFWLRQ
7KLVLVRQHRIDQXPEHURI3DUWVRI(1GHDOLQJZLWKPHWKRGVIRUGHWHUPLQLQJWKHFRORXUVWDELOLW\RIFRORXULQJ PDWHULDOV XQGHU WKH LQIOXHQFH RI WKH WKHUPDO VWUHVV HQFRXQWHUHG GXULQJ SODVWLFV SURFHVVLQJ ,W VKRXOG EH UHDG LQ FRQMXQFWLRQZLWK(1
6FRSH
7KLV SDUW RI (1 GHVFULEHV D PHWKRG IRU GHWHUPLQLQJ WKH FRORXU VWDELOLW\ RI FRORXULQJ PDWHULDOV XQGHU GHILQHG FRQGLWLRQVLQSODVWLFVE\WZRUROOPLOOLQJ7KHUHVXOWRIWKHGHWHUPLQDWLRQLVDUHODWLYHYDOXHQRWDQDEVROXWHRQH
7KHPHWKRGLVPDLQO\XVHGIRUWHVWLQJFRORXULQJPDWHULDOVLQSRO\YLQ\OFKORULGH
1RUPDWLYHUHIHUHQFHV
7KLV (XURSHDQ 6WDQGDUG LQFRUSRUDWHV E\ GDWHG RU XQGDWHG UHIHUHQFH SURYLVLRQV IURP RWKHU SXEOLFDWLRQV 7KHVH QRUPDWLYHUHIHUHQFHVDUHFLWHGDWWKHDSSURSULDWHSODFHVLQWKHWH[WDQGWKHSXEOLFDWLRQVDUHOLVWHGKHUHDIWHU)RUGDWHG UHIHUHQFHVVXEVHTXHQWDPHQGPHQWVWRRUUHYLVLRQVRIDQ\RIWKHVHSXEOLFDWLRQVDSSO\WRWKLV(XURSHDQ6WDQGDUGRQO\ ZKHQLQFRUSRUDWHGLQLWE\DPHQGPHQWRUUHYLVLRQ)RUXQGDWHGUHIHUHQFHVWKHODWHVWHGLWLRQRIWKHSXEOLFDWLRQUHIHUUHG WRDSSOLHV
(1 &RORXULQJ PDWHULDOV LQ SODVWLFV 'HWHUPLQDWLRQ RI FRORXU VWDELOLW\ WR KHDW GXULQJ
SURFHVVLQJRIFRORXULQJPDWHULDOVLQSODVWLFV3DUW*HQHUDOLQWURGXFWLRQ (1$ 7H[WLOHV 7HVWV IRU FRORXU IDVWQHVV 3DUW $ *UH\ VFDOH IRU DVVHVVLQJ FKDQJH LQ
FRORXU,62$
,62 3DLQWVDQGYDUQLVKHV&RORULPHWU\3DUW&RORXUPHDVXUHPHQW
,62 3DLQWVDQGYDUQLVKHV&RORULPHWU\3DUW&DOFXODWLRQRIFRORXUGLIIHUHQFHV
3ULQFLSOH
$PLOOHGVKHHWLVSUHSDUHGIURPWKHSODVWLFVPDWHULDODQGWKHFRORXULQJPDWHULDOWREHWHVWHGHQVXULQJWKDWWKHFRORXULQJ PDWHULDOLVZHOOGLVSHUVHG7KLVVKHHWLVWKHQPLOOHGDWDVSHFLILHGWHPSHUDWXUH$WDSSURSULDWHWLPHLQWHUYDOVVDPSOHV DUH WDNHQ IURP ZKLFK WHVW VSHFLPHQV DUH SUHSDUHG E\ KHDW SUHVVLQJ 7KH FRORXU GLIIHUHQFHV EHWZHHQ WKH WHVW VSHFLPHQV REWDLQHG IRU WKH GLIIHUHQW PLOOLQJ WLPHV DUH WDNHQ DV D PHDVXUH RI WKH FRORXU VWDELOLW\ RI WKH FRORXULQJ PDWHULDO7KHFRORXUFRPSDULVRQLVSHUIRUPHGHLWKHUFRORULPHWULFDOO\RUYLVXDOO\
0DWHULDOV
7HVWPHGLXPWREHDJUHHGEHWZHHQWKHLQWHUHVWHGSDUWLHV
:KHQ HYDOXDWLQJ SLJPHQWV LQ SRO\YLQ\O FKORULGH WKH WHVW PHGLXP VKDOO EH DGHTXDWHO\ VWDELOL]HG WR KHDW 7KH FRORXU VWDELOLW\RIWKHWHVWPHGLXPZKHQVXEMHFWHGWRKHDWVKDOOWKHUHIRUHEHWHVWHGZLWKDQGZLWKRXWWLWDQLXPGLR[LGHSLJPHQW XVLQJWKHVDPHSURFHGXUH,IWKHUHDUHFKDQJHVWKHVHVKDOOEHWDNHQLQWRDFFRXQWZKHQH[SUHVVLQJWHVWUHVXOWV
7LWDQLXPGLR[LGHSLJPHQWJUDGHDVUHFRPPHQGHGIRUXVHLQSODVWLFV
Trang 53DJH (1
%6,
$SSDUDWXV
/DERUDWRU\ WZR UROOPLOO ZLWK IDFLOLW\ IRU KHDWLQJ 7KH VSDFLQJ RI WKH UROOHUV VKDOO EH DGMXVWDEOH DQG WKH GLDPHWHURIWKHUROOHUVVKRXOGEHEHWZHHQPPDQGPPVHH1RWH7KHUDWLRRIWKHURWDWLRQDOVSHHGVRIWKH WZRUROOHUVIULFWLRQUDWLRVKDOOEHDGMXVWDEOHDQGWKHURWDWLRQDOVSHHGVKDOOEHPLQ7KHUDWLREHDGGLDPHWHU
+NEDQNWRJDSZLGWK+VVKRXOGEH+N+V
127(&KURPLXPSODWHGUROOHUVVKRXOGSUHIHUDEO\EHXVHG
127(,WKDVEHHQIRXQGWKDWFRPSDUDEOHUHVXOWVRQGLIIHUHQWWZRUROOPLOOVZLOOEHREWDLQHGXQGHUWKHIROORZLQJ FRQGLWLRQV
UDWLRRIUROOHUGLDPHWHUV EHWZHHQDQG
UDWLRRISHULSKHUDOVSHHGV EHWZHHQDQG
3ODWHSUHVVSURYLGHGZLWKDKHDWLQJDQGFRROLQJV\VWHP
6SHFWURSKRWRPHWHU RUWULVWLPXOXVFRORULPHWHUIRUFRORXUPHDVXUHPHQWVLQDFFRUGDQFHZLWK,62
6DPSOLQJ
6HH(1
7HVWVSHFLPHQV
)RUPDQGGLPHQVLRQV
7KHTXDQWLW\RIPDWHULDOVKDOOEHVXIILFLHQWWRILOOWKHJDSEHWZHHQWKHUROOVDQGSURYLGHWKHUHTXLUHGEHDGGLDPHWHU 8QOHVVRWKHUZLVHVSHFLILHGRUDJUHHGWHVWVSHFLPHQVRIGLPHQVLRQVPP[PP[PPVXLWDEOHIRUFRORULPHWU\ VKDOOEHXVHG
&RQFHQWUDWLRQRIFRORXULQJPDWHULDO
7KHFRORXULQJPDWHULDOVKDOOEHWHVWHGLQUHGXFHGVKDGHDQGRULQIXOOVKDGH
)RUWHVWLQJLQUHGXFHGVKDGHWKHFRQFHQWUDWLRQRIWKHFRORXULQJPDWHULDOLQWKHWHVWPHGLXPVKDOOFRUUHVSRQGWR
DVWDQGDUGGHSWKRIVKDGH6'LQDFFRUGDQFHZLWK(1DQQH[$RU
EVWDQGDUGGHSWKRIVKDGH6'LQDFFRUGDQFHZLWK(1DQQH[$RU
FDQDJUHHGUHGXFWLRQUDWLR
)RUDWHVWVSHFLPHQWKLFNQHVVRIPPRIWLWDQLXPGLR[LGHSLJPHQWLVQHFHVVDU\WRREWDLQIXOOKLGLQJ
)RU WHVWLQJ LQ IXOO VKDGH WKH FRQFHQWUDWLRQ RI WKH FRORXULQJ PDWHULDO LQ WKH WHVW PHGLXP VKDOO FRUUHVSRQG WR
D $OWHUQDWLYHO\ DFRQFHQWUDWLRQ RI WREH SUHIHUUHGIRURUJDQLFSLJPHQWV DQGG\HVWXIIVRUWR EH
SUHIHUUHGIRULQRUJDQLFSLJPHQWVRUDQRWKHUDJUHHGDSSURSULDWHFRQFHQWUDWLRQVKDOOEHWDNHQ
3URFHGXUH
3UHSDUHPLOOHGVKHHWVRQWKHWZRUROOPLOOIURPWKHFRORXULQJPDWHULDOWREHWHVWHGDQGWKHDJUHHGSODVWLFVPDWHULDO,Q WKHFDVHRISODVWLFL]HGSRO\YLQ\OFKORULGHXVHDWHPSHUDWXUHRI&DJDSZLGWKRIPPWRPPDQGD WRWDOPLOOLQJWLPHRIPLQLQFOXGLQJSODVWLILFDWLRQ&XWDQGIROGWKHVKHHWUHSHDWHGO\WRDFKLHYHDGHTXDWHGLVSHUVLRQRI WKHFRORXULQJPDWHULDO7DNHDVDPSOHIURPRQHRIWKHVKHHWVDQGSUHSDUHDWHVWVSHFLPHQIURPLWE\KHDWSUHVVLQJDW
&IRUPLQIRUXVHDVDUHIHUHQFHVSHFLPHQ
6HWWKHUROOVXUIDFHWHPSHUDWXUHVIRU39&SWREHWZHHQ&DQG&DQGIRU39&XWREHWZHHQ&DQG&
3URFHVVDVXIILFLHQWQXPEHURIVKHHWVVRWKDWWKHUHFRPPHQGHGPLQLPXPEHDGGLDPHWHULVDFKLHYHGVHHZKLOVW
VHWWLQJWKHUROOHUJDSWRSURGXFHDVKHHWRIXQLIRUPWKLFNQHVVRIDERXWPP6WDUWWLPLQJDQGPLOOWKHPDWHULDOOLPLWLQJ WKHZLGWKRIWKHVKHHWE\IUHTXHQWFXWWLQJWRRQHKDOIDQGE\UHYHUVDODQGODWHUDOUROOLQJWRSUHYHQWWKHPDWHULDOIURP UXQQLQJXSRQWRWKHUROOJXLGHV
Trang 6(1
%6,
7DNHVDPSOHVDIWHUPLQDQGPLQPLOOLQJWLPH$IWHUDIXUWKHUSHULRGRIPLQWRWDOWHVWSHULRGPLQGUDZRII WKHPLOOVKHHWDQGWDNHDIXUWKHUVDPSOH3UHSDUHWHVWVSHFLPHQVIURPHDFKVDPSOHE\KHDWSUHVVLQJDW&IRU
PLQXVLQJVXIILFLHQWSUHVVXUHWRDFKLHYHDVPRRWKVXUIDFH
:$51,1* $WWHQWLRQ LV GUDZQ WR WKH QHHG IRU HIILFLHQW IXPH H[WUDFWLRQ ZKHQ WHVWLQJ SODVWLFL]HG SRO\YLQ\O FKORULGHRQDQRSHQPLOODWHOHYDWHGWHPSHUDWXUHV
&RPSDUHWKHFRORXURIWKHWHVWVSHFLPHQVZLWKWKDWRIWKHUHIHUHQFHVSHFLPHQHLWKHUFRORULPHWULFDOO\RUYLVXDOO\
127( &RORXULQJ PDWHULDOV VXFK DV &, 3LJPHQW 5HG DQG DQG GH\HVWXIIV FDQ FKDQJH FRORXU UHYHUVLEOHDIWHUKHDWWUHDWPHQWDQGWKHVSHFLPHQVVKRXOGEHPDLQWDLQHGDWURRPWHPSHUDWXUHIRUDWOHDVWK EHIRUHDVVHVVPHQW
,IFRORXUPHDVXUHPHQWLVVSHFLILHGSURFHHGLQDFFRUGDQFHZLWK,62DQG,62)RUYLVXDO
FRPSDULVRQXVHWKHJUH\VFDOHVSHFLILHGLQ(1$
([SUHVVLRQRIUHVXOWV
([SUHVVWKHWHVWUHVXOWVHLWKHUDVDFRORXUGLIIHUHQFHLQDFFRUGDQFHZLWK,62RUDVDVWHSRIWKHJUH\VFDOH WRJHWKHUZLWKWKHGLUHFWLRQRIDQ\FRORXUFKDQJH
7HVWUHSRUW
7KHWHVWUHSRUWVKDOOFRQWDLQDWOHDVWWKHIROORZLQJLQIRUPDWLRQ
DDUHIHUHQFHWRWKLV(XURSHDQ6WDQGDUG(1
EDOOGHWDLOVQHFHVVDU\WRLGHQWLI\WKHFRORXULQJPDWHULDOWHVWHG
FDOOGHWDLOVQHFHVVDU\WRLGHQWLI\WKHWHVWPHGLXPWRJHWKHUZLWKDQ\RWKHUDGGLWLYHVXVHGLQFOXGLQJWKHWLWDQLXPGLR[LGH SLJPHQW
GDOOGHWDLOVQHFHVVDU\UHJDUGLQJWKHSUHSDUDWLRQRIWKHWHVWVSHFLPHQVDQGWKHH[HFXWLRQRIWKHWHVWWHPSHUDWXUHDQG WHVWGXUDWLRQ
HWKHFKRVHQVWDQGDUGGHSWKVRIVKDGHRUIXOOVKDGHDQGWKHFRQFHQWUDWLRQVRIWKHFRORXULQJPDWHULDOWHVWHG
ILIFRORXUPHDVXUHPHQWKDVEHHQVSHFLILHGW\SHRIVSHFWURSKRWRPHWHURUWULVWLPXOXVFRORULPHWHUDVZHOODVVWDQGDUG LOOXPLQDQWDQGVWDQGDUGREVHUYHUXVHG
JFRQGLWLRQVRISUHVVLQJWKHWUHDWHGWHVWVSHFLPHQV
KWKHUHVXOWRIWKHWHVWDVLQGLFDWHGLQFODXVH
LDOOYLVXDOREVHUYDWLRQVIRUH[DPSOHGLVFRORXUDWLRQRIWKHWHVWPHGLXPRUEORRPLQJRIWKHFRORXULQJPDWHULDO
MDQ\GHYLDWLRQIURPWKHWHVWPHWKRGVSHFLILHG
NWKHGDWHRIWKHWHVW
3UHFLVLRQ
6WDWLVWLFDOGDWDDUHQRWDSSURSULDWH
Trang 7blank
Trang 8BS EN
12877-4:2000
BSI
389 Chiswick High Road
London
W4 4AL
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
BSI Ð British Standards Institution
BSI is the independent national body responsible for preparing British Standards It presents the UK view on standards in Europe and at the international level It is incorporated by Royal Charter
Revisions
British Standards are updated by amendment or revision Users of British Standards should make sure that they possess the latest amendments or editions
It is the constant aim of BSI to improve the quality of our products and services We would be grateful if anyone finding an inaccuracy or ambiguity while using this British Standard would inform the Secretary of the technical committee responsible, the identity of which can be found on the inside front cover Tel: 020 8996 9000 Fax: 020 8996 7400
BSI offers members an individual updating service called PLUS which ensures that subscribers automatically receive the latest editions of standards
Buying standards
Orders for all BSI, international and foreign standards publications should be addressed to Customer Services Tel: 020 8996 9001 Fax: 020 8996 7001
In response to orders for international standards, it is BSI policy to supply the BSI implementation of those that have been published as British Standards, unless otherwise requested
Information on standards
BSI provides a wide range of information on national, European and international standards through its Library and its Technical Help to Exporters Service Various BSI electronic information services are also available which give details on all its products and services Contact the Information Centre Tel: 020 8996 7111
Fax: 020 8996 7048
Subscribing members of BSI are kept up to date with standards developments and receive substantial discounts on the purchase price of standards For details of these and other benefits contact Membership Administration Tel: 020 8996 7002 Fax: 020 8996 7001
Copyright
Copyright subsists in all BSI publications BSI also holds the copyright, in the UK, of the publications of the international standardization bodies Except as permitted under the Copyright, Designs and Patents Act 1988 no extract may be reproduced, stored in a retrieval system or transmitted in any form or by any means ± electronic, photocopying, recording or otherwise ± without prior written permission from BSI This does not preclude the free use, in the course of implementing the standard, of necessary details such as symbols, and size, type or grade designations If these details are to be used for any other purpose than implementation then the prior written permission of BSI must be obtained
If permission is granted, the terms may include royalty payments or a licensing agreement Details and advice can be obtained from the Copyright Manager
Tel: 020 8996 7070