Agilent infinitylab lc series installation checklist

G7120A High Speed Pump, G7104A/C Flexible Pump Section NOT applicable  Set up the pump  solvent inlet/outlet tubing  waste and seal wash sensor outlet  remote control if used  conn

Thank you for purchasing an Agilent instrument solution This checklist is used by the installing engineer to ensure that the instrument and associated systems are correctly installed, upgraded and functioning as designed in your facility This checklist will be completed at the end of the service and provided to you as a record of the installation

Customer Information

Customers should provide all necessary operating supplies upon request of the engineer

Service Engineer’s Responsibilities

Only complete/printout sections or pages that relate to the system that has been installed.Complete empty fields with the relevant information

Complete the relevant checkboxes in the checklist using a “X” or tick mark “ ” in the checkbox.Complete Not Applicable check boxes to indicate services not delivered, as needed

Complete the Service Review section together with the customer In case of diagnostic tests, record test results in section service review (test results)

System Information

Guidance:

 Check box if instrument configuration report is attached instead of completing the table below

Instrument System Name/I.D: Instrument Location:

Record the list of system component product numbers

 Discuss any specific questions or issues with the customer prior to starting

 Discuss any configuration options with the customer prior to starting

 Check for required service note applicability and firmware updates if connecting to

instruments

 When plumbing the customers system, make sure that the relevant capillary kit and

instructions are used

 If you use the PC or the Instant Pilot for firmware updates, use the correct date/time

 Check that customer-supplied PC hardware meets minimum requirements e.g Site

Preparation Tool http://www.agilent.com/en-us/support/software-informatics/swsitepreptool

 Upgrades only - Ensure with customer that instrument control settings, data, methods etc

have been properly saved or archived prior to starting any installation procedures

 The installation of ELSD drivers depends upon the customer's choice of software platform If OpenLAB version A.02.01 is installed then ELSD drivers' version 1.2 is installed as part of the installation An UPGRADE to 1.3 will be seen during the new install If a THIRD PARTY software package is used a minimum of ICF A.02.02 is required

Agilent Information Center

 Install the Agilent Information Center to the PC controlling the system

G7122A Degasser

 Section NOT applicable

 Set up the degasser(s)

 solvent inlet/outlet

 Prime each channel with isopropanol from solvent bottle to pump inlet

G7120A High Speed Pump, G7104A/C Flexible Pump

 Section NOT applicable

 Set up the pump

 solvent inlet/outlet tubing

 waste and seal wash sensor outlet

 remote control (if used)

 connect LAN

Agilent LAN connection is made between one (1) of the Agilent Infinity II modules and the Agilent Control Software PC If a detector is installed connect the LAN to this module.

 fill each channel with Isopropanol from solvent bottle to degassing unit inlet

 Prepare the pump

 prepare solvents

 turn on module

 activate Prime

 configure the purge

 activate the purge

 condition the pump, the tuning should be between ±0.2

N O T E

G7110B Isocratic Pump, G7111A Quaternary Pump VL, G7111B Quaternary Pump, G5654A Bio-inert Pump, G7112B Binary Pump

 Section NOT applicable

 Install optional field upgrade kits for Active Seal Wash (G1398A/G1399A):

 Install seal wash pump head parts

 Install the seal wash pump motor and peristaltic pump

 Install tubing connections for the ASW

 After completing the pump installation, run a leak rate test

 Set up the pump(s)

 solvent inlet/outlet

 waste drain

 remote control (ERI) (if used)

 seal wash tubing (if installed)

 connect LAN

Agilent LAN connection is made between one (1) of the Agilent Infinity II modules and the Agilent Control Software PC If a detector is installed, connect the LAN to this module.

 Install the solvent cabinet (optional)

 Priming the pump

 Fill each channel with Isopropanol from solvent bottle to degassing unit inlet

 Turn on the pump

 Purge each channel for 3 min at 3 mL/min

 After completing the stack installation, purge the complete system

• Monitor the pressure, ripple should be <2 %

N O T E

G7129A/B/C Vialsampler

G7129A/B/C Vialsampler

 Section NOT applicable

 Set up the sampler(s)

 solvent inlet

 multi-draw kit (if ordered)

 waste drain (must be in a straight line down, no bends, no kinks) - check manual for further info

 remote control (ERI) (if used)

 Section NOT applicable

 Set up the ICC heater G7130

 Note the product number / Serial number of the Integrated Column Compartment heater

 install the solvent inlet/outlet

 Install the column

 Perform ICC Heater Test

G7167A/B Multisampler, G5668A Bio-Inert Multisampler

 Section NOT applicable

 Perform an auto referencing under operating conditions

 Set up the Multisampler(s)

 solvent inlet

 drawer configuration update (if necessary)

 multi-draw kit (if ordered)

 waste drain (must be in a straight line down, no bends, no kinks) - check manual for further info

 remote control (ERI) (if used)

 Prepare the sampler and fill the available channels with appropriate wash solvent from the solvent bottles

 Turn on the module

 Configure Prime for the available channels

 Activate Prime for the available channels

G7167-60005 Sample Cooler

 Section NOT applicable

Damage to the multisampler or the sample cooler electronics

➔Do not connect the Sample Cooler cables while the autosampler line power is connected

➔Wait at least 30 min before you switch on the compressor

 Set up the Sample Cooler (the module is integrated in the sampler)

 Sample cooler power cable

 Sample cooler signal cable

 Sample cooler condensed water drain (must be in a straight line down, no bends, no kinks)

- check the manual for further info

Check the proper horizontal position

Wait at least for 30 min before swichting on the sample cooler in the cds system

 Perform Sample Cooler Test

C A U T I O N

N O T E

N O T E

G7167-60101 Sample Thermostat

 Section not applicable

Flammable refrigerant Formation of flammable gas-air mixtures inside the sample thermostat.

➔Keep open fire or sources of ignition away from the device

➔Ensure a room size of 1 m3 for every 8 g of r600a refrigerant inside of the sample thermostat

➔Ensure adequate ventilation: typical air exchange of 25 m3/h per m2 of laboratory floor area

➔Do not use mechanical devices or other means to accelerate the defrosting process

Damage to the multisampler or the sample thermostat electronics

➔Do not connect the Sample Thermostat cables while the autosampler line power is connected

➔Wait at least 30 min before you switch on the compressor

 Set up the Sample Thermostat (the module is integrated in the sampler)

 Sample thermostat power cable

 Sample thermostat signal cable

 Sample thermostat condensed water drain (must be in a straight line down, no bends, no kinks) - check the manual for further info

Check the proper horizontal position

Wait at least 30 min before switching on the sample thermostat in the CDS system.

 Perform Sample Thermostat Function Test

WA R N I N G

C A U T I O N

N O T E

N O T E

G7116A/B MCT

 Section NOT applicable

 Set up the MCT

 install the back side of the divider assembly

 install valve head product (see separate section)

 Note the product number / part number of the installed valve head

(valve head part number or n/a)

 install the capillary kit, which belongs to the valve head product (if applicable)

 install the capillaries to heat exchanger

 install the heat exchanger

 install the column holders

 install the low dispersion heat exchangers (if applicable)

 install the heat exchanger with the InfinityLab Quick Turn Fitting (if applicable)

 connect the capillaries to the column, using the Infinity Lab Quick Connect or Quick Turn Fittings (if applicable)

 install the column into the column holders

 install the column ID Readers (if applicable), module has to be powerless

 Install the column ID Tag

 install the waste drain

 Install the CAN connection

 install the front cover of the divider assembly

 Turn on the module

 Perform Thermostat Test

G1170A Valve Drive

 Section NOT applicable

 Install the valve drive(s)

 Install the leak plane and waste drain

 Install the CAN connection

 Install the valve head product

 Note the product number / part number of the installed valve head

(valve head part number or n/a)

 Install the capillary kit delivered with the valve head

G7114A/B VWD

 Section NOT applicable

 Set up the detector

 deuterium lamp (if not installed)

 Turn on the detector and lamp as soon as possible (minimum one hour warm-up time)

 flow cell

 solvent inlet/outlet

 waste drain

 remote control (if used)

 analog output (if used)

 connect LAN (the detector should be always the host of the LAN communication with the PC)

 Verify the operation of the detector

 Perform the Lamp Intensity Test

 Perform the Wavelength Calibration Test

Lamp Intensity

WL calibration

Pass/Fail Wavelength Deviation of 0-Order Wavelength Deviation of Alpha Line (656 nm)

G7115A DAD, G7165A MWD

 Section NOT applicable

 Set up the detector(s)

 deuterium lamp (if not installed)

 Turn on the detector and lamp as soon as possible (minimum one hour warm-up time)

 solvent inlet/outlet

 waste drain

 remote control (if used)

 analog output (if used)

 connect LAN (the detector should be always the host of the LAN communication with the PC)

 Verify the operation of the detector

 Perform the Lamp Intensity Test

 Perform the Wavelength Calibration Test

Lamp Intensity

WL calibration

Pass/Fail D2 Alpha Line Deviation (486 nm) D2 Beta Line Deviation (656 nm)

G7117A DAD FS, G7117B DAD, G7117C DAD HS

 Section NOT applicable

 Set up the detector(s)

 deuterium lamp (if not installed)

 Turn on the detector and lamp as soon as possible (minimum one hour warm-up time)

 solvent inlet/outlet

 waste drain

 remote control (if used)

 analog output (if used)

 connect LAN (the detector should be always the host of the LAN communication with the PC)

 Verify the operation of the detector

 Perform the Lamp Intensity Test

 Perform the Wavelength Calibration Test

Lamp Intensity

WL calibration

Pass/Fail D2 Alpha Line Deviation (486 nm) D2 Beta Line Deviation (656 nm)

G7121A FLD, G7121B FLD Spectra

 Section NOT applicable

 Set up the detector

 solvent inlet/outlet

 waste drain

 remote control (if used)

 analog output (if used)

 connect LAN (the detector should be always the host of the LAN communication with the PC)

 Verify the operation of the detector

New instruments are shipped with a flow cell installed and have a factory wavelength calibration.

If a flow cell is used other then the installed/shipped flow cell:

• verify that the installed flow cell is fixed very tight,

• perform a wavelength calibration using Glycogen (part of FLD Calibration Kit (G7121-68001)).

 Perform the Lamp Intensity Test & compare profile

 Perform the Wavelength test

• Perform Verification Test using the Raman band

Emission Deviation

• If test fails perform Wavelength Calibration

N O T E

G7162A/B RID

 Section NOT applicable

 Set up the detector

Depending on the detector different inlet tubings are used (from the Accessory Kit):

• G7162A:

• Interfacing capillary (G1362-87300)

• G7162B:

• Capillary ST 0.075 mm x 220 mm (5067-4784) (Sampler to MCT/TCC)

• Capillary ST 0.075 mm x 340 mm (5067-4783) (Column to RID)

 Turn on the detector and heater as soon as possible (minimum one hour warm-up time)

 Verify the operation of the detector

N O T E

G7102A, G426X A/B ELSD

 Section NOT applicable

 Set up the detector

 Verify that the instrument is the correct module for the regional voltage (120 V/240 V) Do NOT use instruments which have an incompatible voltage

 Connect the exhaust line to a fume hood or lab exhaust line

 Set the correct pressure at the regulator for the pressurized nitrogen line and connect it to the detector

 Install the capillary connection from detector to HPLC

 Install the RS-232 connection from detector to ChemStation control PC (if applicable)

 Install the Aux I/O cable connection from detector to the 1200 stack

 Connect the power lead

 Connect the front drain to the waste container/bottle

 Configure the detector in OpenLAB CDS ChemStation Edition or EZChrom Edition

"OpenLAB CDS ChemStation and EZChrom Edition, A.01.05 Minimum"

 ELSD driver version 1.3 Installation is essential for data collection

G7102A, G426X A/B Checkout

 Switch on the instrument

 Prepare the instrument:

 Set the detector nebulizer and evaporator temperature to 70 °C , and gas flow to 1.60 SLM

 Wait until instrument ready status is displayed on front panel or PC

 Record 10 min of baseline noise This is gas only noise and should be typically ≤0.5 LSU or

≤0.5 mV for G426X A/B (ASTM baseline noise)

 Set up a method for the checkout sample as below:

 Flush the system with Eluent for 15 min AND

 Verify instrument ready status is still displayed on front panel or PC

In the instrument or system, set up a method using the following parameters:

• Pump: 1.00 mL/min of 100 % water.

Depending on the flow rate setting, the system may overpressure and/or the PEEK fittings

N O T E

PMT Gain 1 (No PMT Gain setting for G7102A)

LED Intensity 100 %( No Laser setting for the Agilent G7102A or G4261B)

• Column Compartment:

Column Temperature Stability (default is 40°C)

If a column compartment is not installed, use ambient temperature

• Run Time: 2.0 minutes (adjust if necessary)

Signal Noise and Drift ASTM baseline noise

Slope of regression fit for drift

Noise: ≤ 2.000 LSU (or 2.000 mV for G4260X A/B)

Drift ≤ 5.000 LSU/hr (or ≤ 5.000 mV/hr for G4260X A/B)

Injection Precision: Injection Volume = 20 µL Height RSD ≤ 3.00 % Area

RSD ≤ 3.00 %

A/B)

 Run a test measurement

 Attach results to installation documentation

Table 1 Pass Specs

G4208A 1200 Instant Pilot

 Section NOT applicable

 Set up the control module

 Connect via CAN to available instrument module

 Assure that the latest firmware is installed

M8550A Lab Advisor Advanced

 Section NOT Applicable

 Install the Lab Advisor software on the controlling PC

 Open the Lab Advisor software Navigate to the License tab under Configuration and enter the Lab Advisor Advanced license

M8555A Lab Advisor Basic

 Section NOT Applicable

 Verify with customers if they would like it installed

 If applicable install the Lab Advisor software on the controlling PC

Service Review

 Attach available reports or printouts to this documentation

 Record the time and date of installation or upgrade completion in the customer’s records or logbook

 Complete the Service Engineer Comments section below if there are additional comments

 Review the installation or upgrade with the customer

 Explain Agilent warranty for instruments

 Explain how to use manuals, guides, online help

 Explain how to get self-help, FAQs from the web

 Explain how to log an instrument service call, support services available

 Advise customer of additional instrument training options

 If the instrument firmware was updated, record the details of the change in the Service Engineer Comments box below or if necessary, in the customer’s IQ records