Agilent infinitylab lc series familiarization checklist

G7102A ELSDIssued: 9-Aug-2018 Revision: 3.3 Copyright: 2017, 2018 Agilent Technologies Select pages for required products  Section NOT Applicable  Explain installation, especially inst

Trang 1

Issued: 9-Aug-2018 Revision: 3.3 Copyright: 2017, 2018 Agilent Technologies

Select pages for required products

Thank you for purchasing an Agilent instrument solution This checklist is used to provide a guide

on what aspects of your instrument should be covered when the Familiarization service has been included in your order This checklist will be completed at the end of the service and provided to you as a record of the familiarization

Customer Information

• Familiarization is intended to give operators a basic overview of the operation and

maintenance of new instruments and is not designed to substitute for a full operator-training course

• Further training, advice and consultation can be obtained upon request

Agilent Information Center

The Agilent Information Center (delivered with the system) contains the eFamiliarization information, which will be used as a guide during familiarization Please make sure the Agilent Information Center and the eFamiliarization are available

• Specifically Not Included in the Familiarization service (unless explicitly ordered):

• Training on basic PC operation, peripherals and/or operating systems

• Training to groups larger than five people

• Customized method/application development and/or testing or testing of customer samples

• Fundamentals/theory of instrument techniques unless explicitly stated

• Preventative Maintenance advice

Service Engineer’s Responsibilities

Discuss familiarization topics and agree upon focus areas with customer within the allotted time Only complete/printout sections or pages that relate to the system that has been installed

Complete empty fields with the relevant information

Complete the relevant checkboxes in the checklist using a “X” or tick mark “ ” in the checkbox Complete Not Applicable check boxes to indicate optional services or product functionality not included

Complete the Service Review section together with the customer In case of diagnostic tests, record test results in section service review (test results)

Trang 2

General Familiarization

 Provide the customer with an overview of their system, its components and locations which have been installed and indicate the parts of the system that familiarization will be provided on

 Identify associated instrument connections, including power connections, communications and LAN interface connections

 Describe where to find the resources available (e.g Agilent Information Center, on-line help) for the instrument

 Demonstrate how to use the Agilent Information Center and on-line help

 Explain need for avoiding growth of algae within the system which can create problems and high costs for customers as this is not covered by the warranty or support contract (Customer

is liable for repair charges)

 Explain need for stopping flow into the instrument, when instrument is powered off

 Explain availability of consumables, supplies and accessories, e.g columns, capillary kits for low dispersion systems, starter kits, tool kits, and maintenance parts

 Give recommendations on solvents (solvent quality, possible degradation, growth of algae, pH range, buffer concentrations etc.), see section "Best Practices" in the Agilent Information Center

 Give recommendations on correct storage of the system (flush with organic solvents etc.)

 If applicable: explain emulation mode, instrument control framework (ICF) and potential consequences for feature set

System Start-up

 Explain how to start up and close down the instrument/modules in the correct order

 Explain where to find the status indicators and what they mean

Trang 3

G7102A ELSD

 Section NOT Applicable

 Explain installation, especially installation of front drain to waste bottle, and rear exhaust tube

 Explain why inert gas (typically nitrogen) must be used with inflammable solvents or samples

 Explain how noble gases may give different performance Explain the importance of setting the right nitrogen pressure by using the correct pressure regulator, and avoiding pressure fluctuations

 Explain how to avoid and check for leaks

 Explain the operating principle of the ELSD

 Explain the detection principle in contrast to UV/Vis (absorption vs intensity of scattered light)

 Explain using the front panel keypad

 Explain optimization for instrument sensitivity by monitoring solvent quality, gas cleanliness etc

 Explain basic troubleshooting in case of baseline noise issues

 If applicable, explain interfaces to third party instruments

 Explain “steam cleaning” procedure

 Explain that no self repair is possible for internal parts due to safety reasons

Trang 4

G7104A 1290 Infinity II Flexible Pump, G7104C 1260 Infinity II Flexible Pump,

G7120A 1290 Infinity II High Speed Pump

 Explain the basic operating principle of the pump, features and key specifications

 Explain pump settings in the Agilent Control Software

 Explain the use of solvent types and generic solvents

 Explain the Prepare Pump procedures in the Agilent Control Software

 Explain the seal wash function and its benefits

 Explain the purpose of the tuning signal and its boundaries

 G7120A: Explain regular maintenance of high pressure filter assembly (PTFE frits) and solvent bottle filters

 G7104A/C: Explain flushing the inline filter (if installed) and maintenance of the

high-pressure filter assembly and inline filter

 Explain the use of the Jet Weaver and availability of different volumes (Jet Weaver is optional for the G7104A/C Flexible Pumps)

 Explain availability of ISET as a temporary license Give a short introduction to ISET features,

a detailed familiarization is included if a full license is purchased

 Explain diagnostic features in Lab Advisor: Pump leak rate test and system pressure test

Trang 5

G7110B 1260 Infinity II Isocratic Pump, G7111A 1260 Infinity II Quaternary Pump VL, G7111B 1260 Infinity II Quaternary Pump, G5654A 1260 Infinity II Bio-Inert

Quaternary Pump, G7112B 1260 Infinity II Binary Pump

 Explain the basic operating principle of the pump, features and key specifications

 Explain pump settings in the Agilent Control Software

 G7112B: Explain solvent tables, solvent compressibility and pump elasticity calibration Explain low delay volume configuration

 Explain when and how to optimize compressibility settings

 Quaternary pump: Explain recommended installation of solvent lines, especially for buffers

 Explain procedures for priming and flushing the pump and system and changing solvents

 If applicable, explain seal wash function Recommend using the seal wash if installed

 Explain diagnostic features in Lab Advisor: Pump leak rate test and system pressure test

 Explain availability of optional upgrades: SSV for binary pumps, seal wash for all pumps, quaternary option for isocratic pump, active inlet valve for isocratic and quaternary pumps

 Explain availability of optional PE seals for normal phase applications

 Explain regular maintenance of purge valve (PTFE frits) and solvent bottle filters

Trang 6

G7122A Degasser

 Explain basic operating principle, applications and key specifications

Trang 7

G7114A 1260 Infinity II VWD, G7114B 1290 Infinity II VWD, G7115A 1260 Infinity II DAD, G7117A 1290 Infinity II DAD FS, G7117B 1290 Infinity II DAD, G7117C 1260 Infinity II DAD HS, G7121A/B 1260 Infinity II FLD/FLD Spectra, G7162A/B Infinity II RID, G7165A 1260 Infinity II MWD

 Explain the basic operating principle of the detector, features and key specifications

 Explain detector settings in the Agilent Control Software

 Explain the pressure and pH range limitiations of the flow cells

 Explain the preventive use of over pressure regulators to secure the flow cell (G7117A/B/C)

 Explain the flow cell maintenance (if applicable)

 Explain that a flow cell change (removal/insertion) requires a wavelength calibration using the FLD Calibration Kit (G7121-68001) (G7121A/B)

Trang 8

G7116A 1260 Infinity II MCT, G7116B 1290 Infinity II MCT

 Explain the basic operating principle of the column compartment, features and key

specifications

 Explain the settings in the Agilent Control Software: Temperature settings, door sensor

 Explain the different hardware features: low dispersion heat exchangers, column switching valve, door sensor, column ID Readers (if applicable)

 Explain the diagnostic features in Lab Advisor: Thermostat test and calibration possibilities

 Explain the functionality and usage of the column ID tags in OpenLAB Chemstation (if applicable)

 Explain the functionality and usage of the column ID tags in third party CDS (if applicable)

Trang 9

G7129A 1260 Infinity II Vialsampler VL, G7129B 1290 Infinity II Vialsampler,

G7129C 1260 Infinity II Vialsampler

G7129A 1260 Infinity II Vialsampler VL, G7129B 1290 Infinity II Vialsampler, G7129C 1260 Infinity II Vialsampler

 Explain the basic operating principle of the Vialsampler, features and key specifications (i.e the flow path, injection cycle, and components of the sampler, like needle assembly, needle seat, sample loop, and rotor seal)

 Explain Vialsampler method settings in the Chromatography Data System software, by using the CDS help (RC Driver Dashboard) Explain the relevant topics such as injection, needle wash, and auxiliary

 Show the use and configuration of the different drawers and explain which sample container and sample vessels are usable with the specific autosampler

 Explain the Vialsampler configuration, such as sample loop and needle seat

 Explain the use and configuration of the Integrated Column Compartment (ICC) (if

applicable)

 Explain the basic operating principle of the integrated column compartment, features and key specifications

 Explain the ICC temperature settings in the Agilent Control Software

 Explain the diagnostic features in Lab Advisor: ICC Heater Test

 Explain the needle wash function and solvent compatibility

 Explain when to use the different needle assemblies and seat assemblies and how to exchange them

 Show proper leak concept Show routing of waste capillary and condensation drain tube

 Show the position of the leak sensor

 Explain the Service & Diagnostics features in Lab Advisor: Injector steps, Alignment and

Parking, and Maintenance Position

 Explain the Instrument Control features in Lab Advisor: Sampler Reset, Drawer Configuration

and Park Position

 Explain availability of optional upgrades: available Drawers, Multidraw, and the 100 µL and

900 µL injection ugrade kit

 Explain regular maintenance of purge pump, needle assembly, needle seat assembly, rotor seal

 Explain the parameters in the Graphical User Interface, such as Assign Wellplates, Reset Injector, Mainpass/Bypass, Move Arm, and Control.

 Explain the wellplate orientation in the Driver Dashboard

Trang 10

 Explain the operating principle of the Sample Cooler (if applicable)

 Explain the Sample Cooler settings and limits in the Agilent Control Software

 Explain regular maintenance: cleaning and care for the ventilation and drain concept (if applicable)

 Clean the Sample Cooler, especially the ventilation and verify that the drain tube is positioned correctly

 Perform a Sample Cooler Test

Vialsampler with Sample Thermostat

 Explain the operating principle of the Sample Thermostat

The unit uses non-Freon refrigerant (isobutane), a natural gas with high environmental compatibility but combustible These materials are harmless to the environment and do not affect the ozone layer and global warming

 Explain the Sample Thermostat's requirments necessary to avoid the creation of a flammable gas-air mixture

 Check for adequate ventilation: typical air exchange of 25 m3/h per m2 of laboratory floor area

 Explain that open fire or sources of ignition must be kept away from the device

 Explain that the usage of mechanical devices or other means to accelerate the defrosting process is not allowed

 Explain the Sample Thermostat settings and limits in the Agilent Control Software

 Explain regular maintenance: cleaning and care for the ventilation and drain concept

 Clean the Sample Thermostat, especially the ventilation and verify that the drain tube is positioned correctly

 Perform a Sample Cooler Test

Trang 11

G7167B 1290 Infinity II Multisampler, G7167A 1260 Infinity II Multisampler, G5668A

1260 Infinity II Bio-inert Multisampler

G7167B 1290 Infinity II Multisampler, G7167A 1260 Infinity II Multisampler, G5668A 1260 Infinity II Bio-inert Multisampler

 Explain the basic operating principle of the Multisampler, features and key specifications (i.e the flow path, injection cycle, and components of the sampler, like needle assembly, needle seat, sample loop, and rotor seal)

 Explain Multisampler method settings in the Chromatography Data System software, by using the CDS help (RC Driver Dashboard) Explain the relevant topics such as injection, needle wash, and auxiliary

 Explain the Sample Entry Management Interface features in the Agilent Control Software (if applicable)

 Show the use and configuration of the Sample Hotel and drawer system and explain which sample container and sample vessels are usable with the specific autosampler

 Explain the Multisampler configuration, such as sample loop and needle seat

 Explain the needle wash function and solvent compatibility

 Explain when to use the different sample loop flex cartridges, the needle assembly and seat assemblies and how to exchange them

 Show where these parts can be configured in the Agilent Control Software

 Show proper leak concept Show routing of waste capillary and condensation drain tube

 Explain the Service & Diagnostics features in Lab Advisor: Injector steps, Auto Referencing,

Parking and Maintenance Position

 Explain the Instrument Control features in Lab Advisor: Sampler Reset, Drawer Configuration

and Park Position

 Explain availability of optional upgrades: available Drawers, Multiwash, Multidraw, Multiload, Dual Needle, and the 100 µL and 900 µL injection ugrade kit

 Explain regular maintenance of purge pump, needle assembly, needle seat assembly, rotor seal

 Explain the parameters in the Graphical User Interface, such as Assign Wellplates, Reset Injector, Mainpass/Bypass, Move Arm, and Control.

 Explain the wellplate orientation in the Driver Dashboard

Tiêu đề	Agilent InfinityLab LC Series Familiarization Checklist
Trường học	University of Example
Chuyên ngành	Laboratory Instrumentation
Thể loại	familiarization checklist
Năm xuất bản	2018
Thành phố	City of Example

Định dạng
Số trang	15
Dung lượng	252,32 KB