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Thermochemical Processes Episode 14 pps

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Superexchange, in magnetic oxides, 237,

238

Supported catalysts, 128 – 9, 133 – 4, 138

Surface diffusion, 15

in catalysts, 128

in sintering, 204 – 7, 303

Surface energy,

of alloys, 126, 139 – 40

of ionic solids, 232 – 3

of metals, 12 – 15, 125 – 6, 196 – 7,

295 – 6

of nuclei, 25, 27

Surface enrichment of alloys, 126,

139 – 40

Surface morphology

of catalysts, 122 – 5

of metals, and temperature on, 199

due to grain boundaries, 195 – 6, 197

of nuclei, 27 – 8

and surface energy, 125 – 6

techniques for studying, 120 – 2

and vaporization, 12 – 15

Swalin equation for diffusion of liquid

metals, 291 – 4

Synthesis gas,

production of, 134 – 5

syntheses from, 142

Tantalum, 93, 349

Tantalum silicides, vaporization of, 97 – 9

Temperature,

choice of for CVD, 107

Debye, 165 – 6

effect of,

on diffusion, 30, 171 – 3, 174

on gas-phase reactions, 45 – 6

on gas transport properties, 112

on nucleation of metallic glasses,

297 – 300

Ternary gaseous systems, 95 – 7, 97 – 9

Terrace surfaces, 122, 123 – 4

Thermal conductivity, 164, 166 – 8

of gases, 110, 115

of metal oxides, 167 – 8

of metals, 167 – 8, 296 – 7

Thermal decomposition, to produce thin

films, 106 – 8

Thermal deposition, see Chemical

vapour deposition (CVD); Vapour deposition

Thermal diffusion, 102, 103 Thermal spikes, in metal sputtering,

18 – 19 Thermal transport,

in condensed phases, 163 – 4

in gas – solid reactions, 277 – 9

in the vapour phase, 89 – 91, 102 – 3 Thin films,

formation of, 24 – 37

by gas-phase dissociation, 43

by laser techniques, 16 – 17, 21,

82 – 3

by metal sputtering, 17 – 20 from nuclei, 28 – 30

by vapour deposition, 3 – 16, 106 – 8 interdiffusion and interaction in,

219 – 21 orientation effects on, 126 thickness of, 107 – 8 Third-order reactions, 50, 51 Thorium oxide (thoria), 12, 159, 239 – 2 Time dependence of reactions, 52 – 3

T–T–N curves for nucleation of

metallic glasses, 297 – 8, 300

T–T–T diagrams for iron-carbon

system, 187 – 8 Titanium, oxidation of, 254 Titanium carbide,

composite of, with chromium, 268 diffusion in, 183 – 4

preparation of thin films of, 10, 107, 219

Titanium– carbon system, oxidation of,

267 – 8 Titanium diboride, CVD of, 106, 107 composite of, with MgO, 216 – 17 Titanium halides, 68

Titanium oxides, 254, 226, 313 Titanium silicide, , 219 Titanium– silicon system, 268

Trang 2

Transition metals,

carburizing of, 262 – 4

as industrial catalysts, 129 – 143

passim

interstitial atoms in, 182

Transition state theory, 42, 47 – 9, 183

Translational energy of molecules, 43

Transport number, 160

Trimolecular reactions, 50, 51

Tungsten, 186, 266, 271 – 2

Tungsten carbide, sintering of, 301

Tungsten – nickel system, sintering of,

303 – 4

Tungsten oxides, structure of, 226

Turbulent flow, 58 – 9, 277 – 9

Unimolecular reactions, 50 – 2

Uranium, 194 – 5, 346

Uranium dioxide,

diffusion in, 228 – 9, 249 – 50

grain growth of, 101 – 2, 250

redistribution of fission products in,

249 – 50

thermal conductivity of, 167

Uranium tetrahalides, reduction of, 346

Vacant sites, 31 – 2, 33

energy of formation of, 173 – 4

in metal oxides, 225

migration of, 173 – 5, 176, 181, 208 – 9

Vacuum refining of liquid steel, 361 – 3

van Arkel refining of metals, 91 – 2

van der Waals equation for real gases,

112 – 14

Vanadates, hot corrosion by, 319 – 20,

321

Vanadium, 174, 186

Vaporization,

evaporation coefficients, 11 – 16

rate of, 7, 8 – 10

thermodynamics of, 4

Vapour deposition,

from organometallic compounds,

68 – 71

for thin film preparation, 3 – 16, 42 – 3,

62 – 3

Vapour pressure, effect of thermal diffusion on, 103

of the elements, 4, 38 – 41

of two-component systems, 8 Vapour-phase transport, 86 – 116 grain growth by, 100 – 2, 250

of uranium dioxide in nuclear fuel rods, 250

Vibrational energy of molecules, 44 Viscosity,

of gases, 110, 115

of liquid metals, 294 – 5

of liquid silicates, 309

of molten metal halides, 317

of slags, 323 – 4, 335 Volume diffusion, 170 – 6, 181, 198 – 9

in Ostwald ripening, 211, 212

in oxidation, 251 – 2, 255

in sintering of metals, 204 – 7 passim

Vycor glass, 311

Wagner equations for growth kinetics,

211, 212 Water-cooled nuclear reactors, 194 Water-gas shift reaction, 129 – 30, 131 – 2 Work-hardening of metals, 181

Wulff’s theorem, 15

Yttrium, effect of, on nickel oxidation, 255

in ceramic superconductors 217 Yttrium iron garnet, 238 – 9

Zero point energy, 44 Zeroth-order reactions, 118 – 19 Zinc,

extraction of, 330 – 1, 332, 334 – 5 refinement and separation of, 357 – 60 vaporization of, 21

Zinc oxide, fuming of, 332 nanoparticles of, 21 point defects in, 225, 226 – 8 Zinc sulphide, preparation of thin films

of, 16 Zircalloy, 194

Trang 3

extraction of, 345 – 6, 349

oxidation of, 265 – 6

in PZT materials, 159 – 60, 236

refining and purification of, 92 – 3

vapour-phase transport of, 87 – 8,

89 – 91

Zirconium diboride, CVD of, 107

Zirconium dioxide (zirconia),

electron transport in, 159

formation of, 265 – 6

in fuel cells, 244

in oxygen sensors, pumps and membranes, 239 – 43, 247 vacancy formation in, 228 vaporization of, 12, 16 Zirconium tetrachloride, reduction of,

345 – 6 Zirconium titanate, 159 – 60 Zone refining, 304 – 6

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