I NTERNATI ONAL STANDARD 1 61 9 I NTERNATI ONAL ORGANI ZATI ON FOR STANDARDI ZATI ON MEYl i YHAPOfl HAR OPrAHbi 3ALl HR I l O CTAHI I APTH3ALWi i 4 ORGANI SATI ON I NTERNATI ONALE DE NORMALl SATl ON C[.]
Trang 1INT ERA T IO NAL ORGA NIZA TION FOR ST A NDARDIZA T ION MEY liY HAOflHR OrA Hbi3ALlH IO CTAIATH3ALWi4.O GA NISA TIO INTR ATIO AL DE N RMALlSTlO
Cry lth , naturele et artific iele - Prepa ra tio et c n erv a tio d s k anti o s po r e sa i
F ir st editio - 197 -0 -15
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R ef No IS0 1619-197 (E)
Desc rip tors : aluminium ores, c ry olte, sa mples, prea ra tion, test spcimen , stora ge, cemica l a na ly sis
Trang 2IS0 (h Interna tio a l O rga niza tio for Sta nd rdiza tio ) is a worldwid fe era tio
of na tio a l sta d rds institutes (IS 0 Memb r B odies) T he work of d v lo in
interna tio a l Sta d rds is ca rrie out throug IS0 Tech ical Comm ite s Ev ry
Memb r Bo y intereste in a s bject for which a Tech ical Com ite h s b e set
up h s th rig t to b re rese te o tha t Com m ite Interna tio a l orga nizatio s,
g v rnm ental a d n n-g v ernm ental in la iso with ISO , a lso take pa rt in th work
D ra ft Interna tio a l Sta d rds a o te by th Tech ical Com mite s are circ la te
to th Memb r Bo ies for a pro al b fore th ir ac e ta ce as Interna tio a l
Sta d rds by th IS0 C ounci
P rior to 19 2, th res lts of th work of th Tech ical Com ite s were publsh d
tra sform ed into Interna tio a l Sta d rds As pa rt of this proces , Tech ical
tech ica lly s ita ble for tra nsform a tio Interna tio a l Sta d rd IS0 1619 th refore
re laces IS0 Recom e d tio R 1619-l 9 0
folowin countries :
Au tra lia
Au tria
Belgium
B ra zi
Ca a a
Czech slo ak ia
Egypt, Ara Re of
F ra ce
Germa y
Gre ce
Hun ary
In ia
Ira n
Isra el
Ita ly
Neth rla ds
New Z eala d
Norway
Pola d
Portug l
Roma ia
South Africa , Re of
Sp in
Swed n
Switzerla nd
Turk ey
U.S.S.R
Yug sla ia
No Memb r Bo y expres e disa prov a l of th Recom e d tio
Interna tio a l Sta d rd
o Interna tiona l Orga niza tion for S ta nda rdiza tion, 196 l
Trang 3C ry ol te, natural and a rtific ia l - Preparation and storage
This Interna tio a l Sta ndard spe ifie th proc ed re f or th
p repa ra tio a nd storag of te t sample , ie c ru e sample
and drie sample , of na tura l a nd arific i c ryolte, a nd of
natura l a nd sy nth tic materials havin a molar ra tio
(Na / AI F a) betwe n 3 a nd I7 a prox imately
IS0 C ry olte, na tura l a nd a rtific ial - Sampln )
3.1 L a boratory sample
F or th prepa ra tio of th la bora tory sample, u e th
meth d spec ifie in IS0
g ometic c harac teristic s, f or c erain phy sical a nd phy sic -
c hemical te ts a nd for moisture d terminatio
T ak aprox imately 3 0 g of th la ora tory sample a nd
plac e it in a n a irig t c onta in r of s c a c ap city that it is
n arly fi e by th sample
3.3 Drie sample, f or c emical te ts, f or th d terminatio
of c erain g ometic c harac teristic s a nd f or phy sical a nd
ph sic -c hemic al te ts
3.3.1 Princ iple
p s e thro g a sieve of me h aperure 0,12 m
3.3.2 Ap aratu
O rdinary la boratory a pa ra tu a nd
3.3.2.1 Sieve, of me h a perure 0,12 m , mad of a
material tha t c an ot c au e into uc tio of th impurity to
b e d termin d
T he siev e s al be s lec te in rela tio to th impurity to be
d termin d
3.3.2 2 Morar, of c ru d m or a ga te
3.3.2.3 Ele tic o e , c apble of bein c ontole a t
1 0 2c
3.3.3 Proc ed re
Siev e a prox imately 10 g of th la boratory sample u in
th sieve (3.3.2.1)
(3.3.2.2) a nd siev e a ga in Add th s siev in s to th material
c arefuly
th material is p se thro g th siev e
Plac th sample th s prepa re in a platin m dis a nd dry
for a t least 2 h in th oven (3.3.2.3) c ontole a t
1 0 + 2 ‘C R emov e th dis fom th oven a nd alow to
c ool in a d sic c ator
Ke p th drie sample in a n airig t c ontain r, th c ap c ity
of whic is s c tha t th sample fis it almo t c ompletely
The c ontain rs sal bea r a la bel in ic atin :
a)
th name of th pro uc t;
b) th origin of th pro uc t;
c)
th na ture of th sample (c ru e or drie );
d)
th ty pe of siev e u e ;
e) th da te of prepa ra tio
1) In prepa ra tio
Trang 4A N X
IS0 1619 - Pre aratio a d stora e of test samples
IS0 16 0 - Determin tio of si c a co te t - Re u e molyb osi cate sp ctro h tometric meth d
IS0 16 3 - Determin tio of fluorin co te t - Mo ifie Wi ard-Winter meth d
IS0 16 4 - Determin tio of iro co te t - l O -Ph n nthroln p otometric meth d
IS0 2 6 - Determin tio of so ium co te t - Flame emis io a d atomic a sorptio sp ctro h tometric meth ds
IS0 2 6 - Determin tio of aluminium co te t - 8-Hydrox quin ln grav imetric meth d
IS0 3 91 - Determin tio of calcium co te t - Flame atomic a sorptio meth d
IS0 3 9 - Determin tio of water co te t - Elec trometric meth d
IS0 3 9 - Determin tio of moisture co te t - Grav imetric meth d
IS0 4 7 - Ev aluatio of fre fluorid s co te t - Co v entio al titrimetric meth d
IS0 4 8 - Determin tio of s lp ates co te t - Barium s lp ate grav imetric meth d
IS0 - Sampln