The disadvantage is that the combined fractions still yield a resolution III design, with all main effects other than X4 aliased with two-factor interactions.. Case when purpose is simpl
Trang 2patterns and
effects that
can be
estimated in
the example
design
The two-factor alias patterns for X4 are: Original experiment: X4 =
X1X2 = X3X7 = X5X6; "Reverse X4" foldover experiment: X4 = -X1X2
= -X3X7 = -X5X6.
The following effects can be estimated by combining the original
with the "Reverse X4" foldover fraction:
X1 + X3X5 + X6X7 X2 + X3X6 + X5X7 X3 + X1X5 + X2X6 X4
X5 + X1X3 + X2X7 X6 + X2X3 + X1X7 X7 + X2X5 + X1X6 X1X4
X2X4 X3X4 X4X5 X4X6 X4X7 X1X2 + X3X7 + X5X6
Note: The 16 runs allow estimating the above 14 effects, with one
degree of freedom left over for a possible block effect.
Advantage
and
disadvantage
of this
example
design
The advantage of this follow-up design is that it permits estimation of
the X4 effect and each of the six two-factor interaction terms involving
X4.
The disadvantage is that the combined fractions still yield a resolution
III design, with all main effects other than X4 aliased with two-factor
interactions.
Case when
purpose is
simply to
estimate all
two-factor
interactions
of a single
factor
Reversing a single factor column to obtain de-aliased two-factor interactions for that one factor works for any resolution III or IV design When used to follow-up a resolution IV design, there are relatively few new effects to be estimated (as compared to designs) When the original resolution IV fraction provides sufficient precision, and the purpose of the follow-up runs is simply to estimate all two-factor
interactions for one factor, the semifolding option should be considered.
Semifolding
5.3.3.8.2 Alternative foldover designs
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Trang 3Number of
runs can be
reduced for
resolution IV
designs
For resolution IV fractions, it is possible to economize on the number of runs that are needed to break the alias chains for all two-factor
interactions of a single factor In the above case we needed 8 additional runs, which is the same number of runs that were used in the original experiment This can be improved upon.
Additional
information
on John's 3/4
designs
We can repeat only the points that were set at the high levels of the factor of choice and then run them at their low settings in the next experiment For the given example, this means an additional 4 runs instead 8 We mention this technique only in passing, more details may
be found in the references (or see John's 3/4 designs).
5.3.3.8.2 Alternative foldover designs
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Trang 4A notation such as "20" means that factor A is at its high level (2) and factor B
is at its low level (0).
The 33 design
The model
and treatment
runs for a 3
factor, 3-level
design
This is a design that consists of three factors, each at three levels It can be expressed as a 3 x 3 x 3 = 33 design The model for such an experiment is
where each factor is included as a nominal factor rather than as a continuous variable In such cases, main effects have 2 degrees of freedom, two-factor interactions have 22 = 4 degrees of freedom and k-factor interactions have 2k
degrees of freedom The model contains 2 + 2 + 2 + 4 + 4 + 4 + 8 = 26 degrees
of freedom Note that if there is no replication, the fit is exact and there is no error term (the epsilon term) in the model In this no replication case, if one assumes that there are no three-factor interactions, then one can use these 8 degrees of freedom for error estimation.
In this model we see that i = 1, 2, 3, and similarly for j and k, making 27
5.3.3.9 Three-level full factorial designs
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Trang 5Table of
treatments for
the 33 design
These treatments may be displayed as follows:
Factor A
Pictorial
representation
of the 33
design
The design can be represented pictorially by
5.3.3.9 Three-level full factorial designs
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Trang 6Two types of
3k designs
Two types of fractions of 3k designs are employed:
Box-Behnken designs whose purpose is to estimate a second-order model for quantitative factors (discussed earlier in section 5.3.3.6.2)
●
3k-p orthogonal arrays.
●
5.3.3.9 Three-level full factorial designs
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Trang 7illustrating
the
generation
of a design
with one
factor at 2
levels and
another at 3
levels from a
2 3 design
A X L X L AX L AX L X Q AX Q TRT MNT
If quadratic
effect
negligble,
we may
include a
second
two-level
factor
If we believe that the quadratic effect is negligible, we may include a second two-level factor, D, with D = ABC In fact, we can convert the design to exclusively a main effect (resolution III) situation consisting
of four two-level factors and one three-level factor This is accomplished by equating the second two-level factor to AB, the third
to AC and the fourth to ABC Column BC cannot be used in this manner because it contains the quadratic effect of the three-level factor X
More than one three-level factor
3-Level
factors from
2 4 and 2 5
designs
We have seen that in order to create one three-level factor, the starting design can be a 23 factorial Without proof we state that a 24 can split off 1, 2 or 3 three-level factors; a 25 is able to generate 3 three-level factors and still maintain a full factorial structure For more on this, see Montgomery (1991)
Generating a Two- and Four-Level Mixed Design
Constructing
a design
with one
4-level
factor and
two 2-level
factors
We may use the same principles as for the three-level factor example in creating a four-level factor We will assume that the goal is to construct
a design with one four-level and two two-level factors
Initially we wish to estimate all main effects and interactions It has been shown (see Montgomery, 1991) that this can be accomplished via
a 24 (16 runs) design, with columns A and B used to create the four
level factor X.
Table
showing
design with
4-level, two
2-level
factors in 16
runs
TABLE 3.39 A Single Four-level Factor and Two
Two-level Factors in 16 runs
5.3.3.10 Three-level, mixed-level and fractional factorial designs
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Some Useful (Taguchi) Orthogonal "L" Array Designs
L 9
design
L 9 - A 3 4-2 Fractional Factorial Design 4 Factors
at Three Levels (9 runs)
L 18
design
L 18 - A 2 x 3 7-5 Fractional Factorial (Mixed-Level) Design
1 Factor at Two Levels and Seven Factors at 3 Levels (18 Runs)
5.3.3.10 Three-level, mixed-level and fractional factorial designs
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design
L 27 - A 3 13-10 Fractional Factorial Design Thirteen Factors at Three Levels (27 Runs)
Run X1 X2 X3 X4 X5 X6 X7 X8 X9 X10 X11 X12 X13
L 36
design
L36 - A Fractional Factorial (Mixed-Level) Design Eleven Factors at Two Levels and Twelve Factors at 3
Levels (36 Runs) Run X1 X2 X3 X4 X5 X6 X7 X8 X9 X10 X11 X12 X13 X14 X15 X16 X17 X18 X19 X20 X21 X22 X23
5.3.3.10 Three-level, mixed-level and fractional factorial designs
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Advantages and Disadvantages of Three-Level and Mixed-Level
"L" Designs
Advantages
and
disadvantages
of three-level
mixed-level
designs
The good features of these designs are:
They are orthogonal arrays Some analysts believe this simplifies the analysis and interpretation of results while other analysts believe it does not
●
They obtain a lot of information about the main effects in a relatively few number of runs
●
You can test whether non-linear terms are needed in the model,
at least as far as the three-level factors are concerned
●
On the other hand, there are several undesirable features of these designs to consider:
They provide limited information about interactions
●
They require more runs than a comparable 2k-pdesign, and a two-level design will often suffice when the factors are continuous and monotonic (many three-level designs are used when two-level designs would have been adequate)
●
5.3.3.10 Three-level, mixed-level and fractional factorial designs
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Trang 115 Process Improvement
5.4 Analysis of DOE data
5.4.1 What are the steps in a DOE analysis?
General
flowchart
for
analyzing
DOE data
Flowchart of DOE Analysis Steps
DOE Analysis Steps
Analysis
steps:
graphics,
theoretical
model,
actual
model,
validate
model, use
model
The following are the basic steps in a DOE analysis.
Look at the data Examine it for outliers, typos and obvious problems Construct as many graphs as you can to get the big picture.
Response distributions ( histograms , box plots , etc.)
❍
❍ Responses versus factor levels (first look at magnitude of factor effects)
❍
Typical DOE plots (which assume standard models for effects and errors) Main effects mean plots
■ Block plots
■
■
❍
1
5.4.1 What are the steps in a DOE analysis?
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Trang 12Interaction plots
■
Sometimes the right graphs and plots of the data lead to obvious answers for your experimental objective questions and you can skip to step 5 In most cases, however, you will want to continue by fitting and validating a model that can be used to answer your questions.
❍
Create the theoretical model (the experiment should have been designed with this model in mind!).
2
Create a model from the data Simplify the model, if possible, using stepwise regression methods and/or parameter p-value significance information.
3
Test the model assumptions using residual graphs.
If none of the model assumptions were violated, examine the ANOVA.
Simplify the model further, if appropriate If reduction is appropriate, then return to step 3 with a new model.
■
❍
If model assumptions were violated, try to find a cause.
Are necessary terms missing from the model?
■
Will a transformation of the response help? If a transformation is used, return
to step 3 with a new model.
■
❍
4
Use the results to answer the questions in your experimental objectives finding important factors, finding optimum settings, etc.
5
Flowchart
is a
guideline,
not a
hard-and
-fast rule
Note: The above flowchart and sequence of steps should not be regarded as a "hard-and-fast rule"
for analyzing all DOE's Different analysts may prefer a different sequence of steps and not all
types of experiments can be analyzed with one set procedure There still remains some art in both
the design and the analysis of experiments, which can only be learned from experience In addition, the role of engineering judgment should not be underestimated.
5.4.1 What are the steps in a DOE analysis?
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Trang 13Plots for
viewing
main effects
and 2-factor
interactions,
explanation
of normal or
half-normal
plots to
detect
possible
important
effects
Subsequent Plots: Main Effects, Comparisons and 2-Way Interactions
Quantile-quantile (q-q) plot
● Block plot
● Box plot
● Bi-histogram
● DEX scatter plot
● DEX mean plot
● DEX standard deviation plot
● DEX interaction plots
● Normal or half-normal probability plots for effects Note: these links show how to generate plots to test for normal (or
half-normal) data with points lining up along a straight line, approximately, if the plotted points were from the assumed normal (or half-normal) distribution For two-level full factorial and fractional factorial experiments, the points plotted are the estimates of all the model effects, including possible interactions Those effects that are really negligible should have estimates that resemble normally distributed noise, with mean zero and a
constant variance Significant effects can be picked out as the ones that do not line up along the straight line Normal effect plots use the effect estimates directly, while half-normal plots use the absolute values of the effect estimates.
●
Youden plots
●
Plots for
testing and
validating
models
Model testing and Validation
Response vs predictions
● Residuals vs predictions
● Residuals vs independent variables
● Residuals lag plot
● Residuals histogram
● Normal probability plot of residuals
●
Plots for
model
prediction
Model Predictions
Contour plots
●
5.4.2 How to "look" at DOE data
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designs
Response surface initial models include quadratic terms and may occasionally also include cubic terms These models were described in section 3.
Model
validation
Of course, as in all cases of model fitting, residual analysis and other tests of model fit are used to confirm or adjust models, as needed.
5.4.3 How to model DOE data
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