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Introduction Background The vast majority of research into solid-state polymer electrolytes for low-temperature o200 1C fuel cells has focused on proton-exchange membrane PEM fuel cells

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Anion-Exchange Membranes

JR Varcoe, JP Kizewski, DM Halepoto, SD Poynton, RCT Slade, and F Zhao,University of Surrey, Guildford, UK

& 2009 Elsevier B.V All rights reserved.

Introduction

Background

The vast majority of research into solid-state polymer

electrolytes for low-temperature (o200 1C) fuel cells has

focused on proton-exchange membrane (PEM) fuel cells

(PEMFCs) Recently, there has been interest in the

ap-plication of the analogous anion-exchange membranes

(AEMs), in alkaline forms, in low-temperature fuel cells

(AAEMs), which are at an early stage of development,

conduct hydroxide (OH) anions (and/or (bi)carbonate

anions –HCO3 

/CO3 

) rather than protons (Hþ) This article will discuss the current understanding on the

application of AEMs in chemical fuel cells containing

hydrogen, carbon-, boron-, and nitrogen-containing fuels

and also in microbial fuel cells (MFCs) utilizing

bio-logical energy generation

The Driver for and Concerns with the Use of

Alkaline Anion-Exchange Membranes in Fuel

Cells

The cost of fuel cells still retards commercialization in

most markets Alkaline fuel cells (AFCs), which

tradi-tionally utilize caustic aqueous potassium hydroxide as a

cheap electrolyte, are promising on a cost basis mainly

because cheap and relatively abundant non-platinum

group metals (non-PGM) are viable catalysts Catalyst

electrokinetics (for fuel oxidation and oxygen reduction)

is also improved in alkaline, as opposed to acidic,

con-ditions (the acid-stability criterion precludes the use of

most non-PGM catalysts in PEMFCs) However, there

are concerns that carbon dioxide, which is a natural

component of air, will lead to performance losses due to the formation in the aqueous alkaline electrolyte of less ionically conductive, and less basic, bicarbonate (HCO3) and carbonate (CO3 ) anions (eqns [I] and [II]) The pH of aqueous solutions at 25 1C increases from 8–8.5 for sodium hydrogen carbonate (NaHCO3) to 10.5–12 for Na2CO3and to 13–14 for sodium hydroxide (NaOH) (approximate pKbvalues¼ 7.7, 3.7, and 0.2, re-spectively):

CO2þ OH"HCO

HCO3 þ OH"CO3þ H2O ½II

Metal CO3 =HCO3 solid precipitates can also form and these can not only block the pores of the AFC electrodes, but also mechanically degrade the active layers

The replacement of the potassium hydroxide (aq) electrolyte with an AAEM in AFCs retains the electro-catalytic advantages but introduces carbon dioxide tol-erance along with the additional advantage of being an all solid-state fuel cell (as with PEMFCs – i.e., no seep-ing out of aqueous potassium hydroxide) Addi-tionally, thin (low electronic resistance) and easily stamped (cheap) metal monopolar/bipolar plates can be used with reduced corrosion-derived problems at high

pH (the cost of bipolar plates for PEMFCs can be rela-tively high) A key requirement (see the section entitled

‘Alkaline Ionomer Developments’) is the development

of an alkaline ionomer (anionomer) to maximize ionic contact between the catalyst reaction sites and the

3H2

3H2O

CO2

Catalyst

PEM

Anode Cathode

6 H +

H2O

3H2

CH3OH

6H2O

CO2+ 5H2O

1½O2 + 3H2O

Load

Catalyst

Anode Cathode

6 OH –

H2O

Load

AAEM

Figure 1 Schematic comparison between hydrogen or methanol-fuelled alkaline anion-exchange membrane (AAEM) and proton-exchange membrane (PEM) fuel cells.

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