This European Standard Leak detection systems consists of 7 parts: — Part 1: General principles — Part 2: Requirements and test/assessment methods for pressure and vacuum systems — Pa
Trang 1Leak detection systems
Part 7: Requirements and test/assessment methods for interstitial spaces, leak
detection linings and leak detection jackets
BSI Standards Publication
Trang 2National foreword
This British Standard is the UK implementation of EN 13160-7:2016
It supersedes BS EN 13160-7:2003 which is withdrawn
The UK participation in its preparation was entrusted to TechnicalCommittee PVE/393/2, Leak detection devices
A list of organizations represented on this committee can beobtained on request to its secretary
This publication does not purport to include all the necessaryprovisions of a contract Users are responsible for its correctapplication
© The British Standards Institution 2016 Published by BSI StandardsLimited 2016
ISBN 978 0 580 86638 8ICS 23.020.01; 23.040.99; 29.260.20
Compliance with a British Standard cannot confer immunity from legal obligations.
This British Standard was published under the authority of theStandards Policy and Strategy Committee on 31 July 2016
Amendments issued since publication
Trang 3Systèmes de détection de fuites - Partie 7: Exigences et
méthodes d'essai/d'évaluation pour les espaces
interstitiels, les détecteurs de fuite des revêtements et
les détecteurs de fuite d'enveloppes
Leckanzeigesysteme - Teil 7: Anforderungen und /Bewertungsverfahren für Überwachungsräume,
Prüf-Leckschutzauskleidungen und Leckschutzummantelungen This European Standard was approved by CEN on 8 April 2016
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member
This European Standard exists in three official versions (English, French, German) A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom
EUROPEAN COMMITTEE FOR STANDARDIZATION
C O M I T É E UR O P É E N DE N O R M A L I SA T I O N
E UR O P Ä I SC H E S KO M I T E E F ÜR N O R M UN G
CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2016 CEN All rights of exploitation in any form and by any means reserved
worldwide for CEN national Members Ref No EN 13160-7:2016 E
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European foreword 4
1 Scope 6
2 Normative references 6
3 Terms and definitions 7
4 Requirements 7
4.1 Effectiveness of leak detection lining kits and leak detection jacket kits 7
4.1.1 Tightness against liquid and vapour 7
4.1.2 Permeability of leak detection linings and leak detection jackets 7
4.1.3 Free passage of liquid in the interstitial space 8
4.1.4 Free passage of air 8
4.1.5 Flow resistance after impact of stored media 8
4.1.6 Mechanical resistance against the imposed load by the stored medium 8
4.1.7 Chemical resistance 15
4.2 Durability of effectiveness 15
4.2.1 Durability against temperature 15
4.2.2 Durability against chemical attack 15
4.2.3 Durability against mechanical load 15
5 Testing, assessment and sampling methods 15
5.1 Effectiveness of leak detection lining kits and leak detection jacket kits 15
5.1.1 Tightness against liquid and gas 15
5.1.2 Permeability 17
5.1.3 Free passage of liquid in the interstitial space 18
5.1.4 Free passage of air 19
5.1.5 Flow resistance after impact of stored media 22
5.1.6 Mechanical resistance against the imposed load by the stored medium 25
5.1.7 Chemical resistance 25
5.2 Durability of effectiveness 25
5.2.1 Durability against temperature 25
5.2.2 Durability against chemical attack 25
5.2.3 Durability against mechanical load 25
6 Assessment and verification of constancy of performance – AVCP 27
6.1 General 27
6.2 Type testing 28
6.2.1 General 28
6.2.2 Test samples, testing and compliance criteria 29
6.2.3 Test reports 29
6.2.4 Shared other party results 29
6.2.5 Cascading determination of the product type results 30
6.3 Factory production control (FPC) 31
6.3.1 General 31
6.3.2 Requirements 32
6.3.3 Product specific requirements 34
6.3.4 Procedure for modifications 35
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6.3.5 One-off products, pre-production products (e.g prototypes) and products
produced in very low quantity 35
7 Marking, labelling and packaging 36
8 Environmental aspects 37
Annex A (normative) Determination of the interstitial space volume for class I-systems 38
A.1 Test equipment 38
A.2 Preparation 38
A.3 Procedure 39
A.4 Evaluation 41
Annex B (informative) Environmental aspects 42
Annex ZA (informative) Clauses of this European Standard addressing the provisions of the EU Construction Products Regulation 305/2011/EU 44
ZA.1 Scope and relevant characteristics 44
ZA.2 Procedure for AVCP of leak detection linings and leak detection jackets 45
ZA.2.1 System(s) of AVCP 45
ZA.2.2 Declaration of performance (DoP) 46
ZA.2.2.1 General 46
ZA.2.2.2 Content 47
ZA.2.2.3 Example of DoP 47
ZA.3 CE marking and labelling 49
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European foreword
This document (EN 13160-7:2016) has been prepared by Technical Committee CEN/TC 393
“Equipment for storage tanks and for filling stations”, the secretariat of which is held by DIN
This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by December 2016, and conflicting national standards shall be withdrawn at the latest by March 2018
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights
This document supersedes EN 13160-7:2003
This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association, and supports essential requirements of EU Directive(s)
For relationship with EU Directive(s), see informative Annex ZA, which is an integral part of this document
According to edition 2003 the following fundamental changes are given:
— requirements and tests for permeation added;
— material properties revised;
— requirements from EN 13160-1:2003 included, which are no longer contained in
EN 13160-1:2016
This European Standard Leak detection systems consists of 7 parts:
— Part 1: General principles
— Part 2: Requirements and test/assessment methods for pressure and vacuum systems
— Part 3: Requirements and test/assessment methods for liquid systems for tanks
— Part 4: Requirements and test/assessment methods for sensor based leak detection systems
— Part 5: Requirements and test/assessment methods for in-tank gauge systems and pressurized
pipework systems
— Part 6: Sensors in monitoring wells
— Part 7: Requirements and test/assessment methods for interstitial spaces, leak detection linings and
leak detection jackets
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
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Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom
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1 Scope
This European Standard gives requirements and the corresponding test/assessment methods applicable to leak detection lining kits and leak detection jacket kits Leak detection lining kits and leak detection jackets kits intended to be used to create an interstitial space or leakage containment in single skin underground or above ground, non-pressurized, tanks designed for water polluting liquids The kit has to be used only in conjunction with leak detection kits covered by EN 13160-2 to
EN 13160-4
2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application For dated references, only the edition cited applies For undated references, the latest edition of the referenced document (including any amendments) applies
EN 228, Automotive fuels — Unleaded petrol — Requirements and test methods
EN 495–5, Flexible sheets for waterproofing — Determination of foldability at low temperature — Part
5: Plastic and rubber sheets for roof waterproofing
EN 1107-2, Flexible sheets for waterproofing — Determination of dimensional stability — Part 2: Plastic
and rubber sheets for roof waterproofing
EN 1849-2, Flexible sheets for waterproofing — Determination of thickness and mass per unit area —
Part 2: Plastic and rubber sheets
EN 10300:2005, Steel tubes and fittings for onshore and offshore pipelines — Bituminous hot applied
materials for external coating
EN 13121-1, GRP tanks and vessels for use above ground — Part 1: Raw materials — Specification
conditions and acceptance conditions
EN 13121-2:2003, GRP tanks and vessels for use above ground — Part 2: Composite materials —
Chemical resistance
EN 13160-1:2016, Leak detection systems — Part 1: General principles
EN 13160-2:2016, Leak detection systems — Part 2: Requirements and test/assessment methods for
pressure and vacuum systems
EN 13160-3:2016, Leak detection systems — Part 3: Requirements and test/assessment methods for
liquid systems for tanks
EN 13160-4:2016, Leak detection systems — Part 4: Requirements and test/assessment methods for
sensor based leak detection systems
EN 14879-4:2007, Organic coating systems and linings for protection of industrial apparatus and plants
against corrosion caused by aggressive media — Part 4: Linings on metallic components
EN ISO 62, Plastics — Determination of water absorption (ISO 62)
EN ISO 75-1, Plastics — Determination of temperature of deflection under load — Part 1: General test
method (ISO 75-1)
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EN ISO 75-2, Plastics — Determination of temperature of deflection under load — Part 2: Plastics and
ebonite (ISO 75-2)
EN ISO 75-3, Plastics — Determination of temperature of deflection under load — Part 3: High-strength
thermosetting laminates and long-fibre-reinforced plastics (ISO 75-3)
EN ISO 175, Plastics — Methods of test for the determination of the effects of immersion in liquid
chemicals (ISO 175)
EN ISO 178, Plastics — Determination of flexural properties (ISO 178)
EN ISO 179-1, Plastics — Determination of Charpy impact properties — Part 1: Non-instrumented
impact test (ISO 179-1)
EN ISO 179-2, Plastics — Determination of Charpy impact properties — Part 2: Instrumented impact test
(ISO 179-2)
EN ISO 527-1, Plastics — Determination of tensile properties — Part 1: General principles (ISO 527-1)
EN ISO 527-3, Plastics — Determination of tensile properties — Part 3: Test conditions for films and
sheets (ISO 527-3)
EN ISO 604, Plastics — Determination of compressive properties (ISO 604)
EN ISO 1183-1, Plastics — Methods for determining the density of non-cellular plastics — Part 1:
Immersion method, liquid pyknometer method and titration method (ISO 1183-1)
EN ISO 24345, Resilient floor coverings — Determination of peel resistance (ISO 24345)
ISO 2528, Sheet materials — Determination of water vapour transmission rate — Gravimetric (dish)
method
ISO 6133, Rubber and plastics — Analysis of multi-peak traces obtained in determinations of tear
strength and adhesion strength
3 Terms and definitions
For the purposes of this document, the terms and definitions given in EN 13160-1:2016 apply
4 Requirements
4.1 Effectiveness of leak detection lining kits and leak detection jacket kits
4.1.1 Tightness against liquid and vapour
The integrity of the leak detection linings and leak detection jackets shall be maintained under all operating pressures
4.1.2 Permeability of leak detection linings and leak detection jackets
The permeation shall be according to Table 1 and Table 2
No condensation of vapour of the stored product in the interstitial space should occur
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Table 1 — Permeation of leak detection linings
Property Required value
Passage of stored products at installation of the leak protecting lining in metal tanks
with a passage of stored product of 0 g/m 2 ⋅ d max 100 g/m
2 ⋅ day
Passage of stored products at installation of the leak protecting lining in tanks with a
passage of stored product > 0 g/m 2 ⋅ d max 0,1 g/m
2 ⋅ day
Passage of deionized water max 4 g/m2 ⋅ day
NOTE By permeation rates > 0 g/m 2 ⋅ d the exhaust line of the leak detector should be connected to the vapour space of the stored tank
Table 2 — Permeation of leak detection jackets
Property Required value
Passage of stored product max 2 g/m2 ⋅ day
Passage of deionized water max 4 g/m2 ⋅ day
4.1.3 Free passage of liquid in the interstitial space
The quantity of liquid, calculated according to EN 13160–2:2016, Formula (4) and the specific volume
Vsp according to Annex A shall enter the interstitial space by a vacuum change from (60 ± 5) kPa (pPA)
to (30 ± 5) kPa (pPE)
Additional for leak detection systems class II according to EN 13160-3 the flow rate at the test nozzles shall be > 0,5 l/min
4.1.4 Free passage of air
4.1.4.1 Free passage of air through intermediate layer
The back pressure of the intermediate layer shall not be higher than 1 kPa at a volume flow of (85 ± 5) l/h of air
4.1.4.2 Free passage of air through double skin tanks and pipes
An opening of the interstitial space shall result in a pressure change in the interstitial space
4.1.5 Flow resistance after impact of stored media
The flow resistance shall not exceed the value of 1 kPa at an air volume flow of (85 ± 5) l/h
4.1.6 Mechanical resistance against the imposed load by the stored medium
4.1.6.1 Influence of the mechanical resistance to the free passage in the interstitial space
The flow resistance of the intermediate layer shall not be higher than 1 kPa at a volume flow of (85 ± 5) l/h of air under load
4.1.6.2 Mechanical properties
Mechanical properties for polyvinylchloride (PVC) shall be according to Table 3
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Table 3 — Mechanical properties for polyvinylchloride (PVC)
No Property Test method Dimension Required value
1 Tensile strength,
Lengthwise and across
EN ISO 527-1 and EN ISO 527-3;
Test speed: 200 mm/min ± 10 % Specimen: Type 2
N/mm ≥ 15
2 Tensile elongation,
Lengthwise and across
EN ISO 527-1 and EN ISO 527-3;
Test speed: 200 mm/min ± 10 % Specimen: Type 2
% > 200
3 Reaction of joint to shear test EN ISO 527-1 and EN ISO 527-3;
Test speed: 200 mm/min ± 10 % Specimen: Type 2
at normal climate on a cover, which shall not affect the dimensions
deviation ± 2 Effects of test media for polyvinylchloride (PVC) shall be according to Table 4
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Table 4 — Effects of test media for polyvinylchloride (PVC)
Property Test method Dimension Required value
Change of mass after storage in
deionized water and stored product
or test liquids according to Annex C of
EN 14879–4:2007
In conformity with EN ISO 62 at normal climate, change shall be determined after the following storage periods: 3, 14 and 56 d
%
≤ 15
Change of tensile strength and
elongation, in either direction after
storage in deionized water and stored
product (56 d at 23 °C) or test liquids
according to Annex C of EN 14879–
4:2007
EN ISO 527-1 and EN ISO 527-3 Test speed: 200 mm/min ± 10 % Specimen: Type 2 %
≤ 25 for tensile elongation the measured value
as per Table 3
Change of tensile strength and
elongation, in either direction after
storage in of folded materials in
deionized water and stored product
%
≤ 25
Change of reaction of the joint to
shear test after storage in deionized
water and stored product
Off-joint fracture
Mechanical properties for thermoplastic and thermoplastic elastomers except polyvinylchloride (PVC) shall be according to Table 5
Trang 13Lengthwise and across
EN ISO 527-1 and EN ISO 527-3;
Test speed: 200 mm/min ± 10 % Specimen: Type 2
N/mm ≥ 15
2 Tensile elongation,
Lengthwise and across
EN ISO 527-1 and EN ISO 527-3;
Test speed: 200 mm/min ± 10 % Specimen: Type 2
% > 200
3 Reaction of joint to shear
test EN ISO 527-1 and EN ISO 527-3; Test speed: 200 mm/min ± 10 %
Specimen: Type 2
— Off-joint
fracture, joint factor ≥ 0,5
deviation ± 10
deviation ± 10 % Effects of test media for thermoplastic and thermoplastic elastomers except polyvinylchloride (PVC) shall be according to Table 6
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Table 6 — Effects of test media for thermoplastic and thermoplastic elastomers except
polyvinylchloride (PVC)
Property Test method Dimension Required value
Change of mass after storage in
deionized water and stored
product or test liquids according to
Annex C of EN 14879–4:2007
In conformity with EN ISO 62 at normal climate, change shall be determined after the following storage periods: 3 d, 14 d and 56 d
%
≤ 20
Change of tensile strength and
elongation, in either direction after
storage in deionized water and
Change of tensile strength and
elongation, in either direction after
storage in of folded materials in
deionized water and stored
%
≤ 60 for tensile elongation the measured value
as per Table 5
Change of reaction of the joint to
shear test after storage in
deionized water and stored
Trang 15Flexural strength MPa EN ISO 178 EN ISO 178 5 ≥ 80
Impact strength kJ/m2 EN ISO 179-1 and
EN ISO 179-2 EN ISO 179-1 5 ≥ 5 Dimensional stability under
heat °C EN ISO 75-1 EN ISO 75-2
EN ISO 175 Cut surfaces shall be sealed
3
3
+4
−2
Change of flexural strength
after 28 days storage
30 % under the values of Table 7 The single value of the other properties shall fulfil the requirements of Table 7
Requirements for intermediate layer of resin and spacer of leak detection linings and of leak detection jackets according to Figure 1 shall be according to Table 8
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Table 8 — Requirements for intermediate layer of resin and spacer of leak detection linings
and of leak detection jackets
Property Dimension Test method
sample
Values of property
dimension
mm number Compression strength at
condition at time of supply
N/mm 2 EN ISO 604
length and width according to
EN ISO 604 height: sampling
≥ 1,0 (no break) for tanks with a height
or diameter of ≤ 3 m
≥ 3,0 (no break) for tanks with a height
or diameter of > 3 m
Change of compression
strength after 112 days
storage at ambient
temperature in water and
stored product or test liquids
Cut surfaces shall
be sealed
5
≥ 0,6 (no break) for tanks with a height
or diameter of ≤ 3 m
≥ 1,8 (no break) for tanks with a height
or diameter of > 3 m The construction of leak detection linings and leak detection jackets can be according to Figure 1
4 inner layer by leak detection linings/ outer layer by leak detection jackets combined with spacer
5 inner layer by leak detection linings/outer layer by leak detection jacket combined with spacer, fixed to the tank wall
Figure 1 — Construction of leak detection linings and leak detection jackets
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4.1.7 Chemical resistance
4.1.7.1 Inner layer and outer layer in contact with the stored liquid
The components of the thermoplastic and thermoplastic elastomers leak detection lining kits according to Table 4 and Table 6
The components of the UP and EP leak detection lining kits or leak detection jacket kits according to
4.2.1 Durability against temperature
For thermoplastic and thermoplastic elastomers leak detection linings according to Table 3 and Table 5
For intermediate layer according to 5.1.4.2
For UP and EP leak detection linings or leak detection jackets according to Table 7
4.2.2 Durability against chemical attack
The thermoplastic and thermoplastic elastomers leak detection linings according to Table 4 and Table 6
The UP and EP leak detection linings or leak detection jackets according to Table 7 and intermediate layer and spacer of leak detection linings and of leak detection jackets according to Table 8
4.2.3 Durability against mechanical load
4.2.3.1 Leak detection lining kits
The components of the thermoplastic and thermoplastic elastomers leak detection lining kits according to Table 3 to Table 6
The components of the UP and EP leak detection lining kits shall fulfil the requirements according to
EN 13121-1
4.2.3.2 Leak detection jacket kits
There shall be no damage indicated by a crack, de-bonding or delamination after the test according to 5.2.3.2
5 Testing, assessment and sampling methods
5.1 Effectiveness of leak detection lining kits and leak detection jacket kits
5.1.1 Tightness against liquid and gas
5.1.1.1 Test equipment
— vacuum pump with constant volume flow of 85 l/h;
Trang 18The tightness and the strength of the interstitial space shall be proved by a pressure test on a sample
of a tank or pipework at ambient pressure in the tank or pipework
The difference of the ambient temperature shall be within a range of 1 K at the beginning and at the end of the test
The following minimum test pressures (pt2) shall be used:
— for interstitial spaces, which are part of a leak detection system working on the basis of leak detection liquid or pressure at 1,1 times of the set pressure of the pressure relief valve, but at least
at 60 kPa (0,6 bar) pressure;
— for the interstitial spaces, which are part of a leak detection system working on the basis of vacuum at 1,1 times of the negative working pressure of the leak detector and at 1,1 times of the operating pressure of the pipework or the tank at pressurization of the pipework or tank at the same time
5.1.1.4 Evaluation
The test shall be deemed to have been passed if the condition in Formula (1) is fulfilled:
t
V p
pB E) 1
(
where
pB is the pressure at the beginning of the test, in Pascal
pE is the pressure at the end of the test, in Pascal
t is the test time, in seconds
V1 is the volume of the interstitial space according to Annex A in litres
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5.1.2 Permeability
5.1.2.1 Test equipment
— Stored product or the following test liquids:
a) For unleaded petrol: According to EN 228
1) with maximum 5 % (V/V) ethanol
The tolerance for the component of the test liquid shall be 0,1 %
b) for other products: according to Annex C of EN 14879-4:2007
— Scale, accuracy of minimum ± 0,1 g
— Length measuring device, accuracy of minimum ± 1 mm
— Volume measuring device, accuracy of minimum ± 1 ml
5.1.2.2 Preparation
The dimension of the test sample (e.g piece of pipe or bag of lining material) shall be measured and recorded A test sample in form of closed volume with a minimum inner surface of 0,12 m2 shall be used The volume of the test sample shall be filled with (1,0 ± 0,1) l of test liquid and shall be weighted The end-closures used for the permeation test will need to be fitted with FKM or rubber, seals The seal shall be resistant against the test liquid The test liquid shall be specially selected for their volatile nature, so that multiple seals may be required to ensure that loss through the end-closures is negligible
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The closure of the test samples may be grouted
5.1.2.3 Procedure
Store the samples in air at (23 ± 2) °C using the scale
In conformity with ISO 2528 at normal climate, passage shall be determined after the following storage periods: 1, 3, 7, 14 and 56 d
Determine the rate of mass loss of the 'steady-state’ period (gradient of the regression line) in g ⋅ d-1 Calculate the surface area A, where A = π ⋅L ⋅ D, in m2 Divide the rate of mass loss by A to give the permeation rate in g ⋅ m-2 ⋅ d-1 for each specimen
5.1.2.4 Evaluation
The test shall be deemed to have been passed, if the arithmetic average value over 56 d does not exceed the values according to Table 1
Each value measured at the different days shall fulfil the requirements of Table 1 and Table 2
5.1.3 Free passage of liquid in the interstitial space
5.1.3.1 Test equipment
— vacuum pump with constant volume flow of 85 l/h;
— measuring device for pressure accuracy 0,6 % of the maximum graduated value;
be installed at a distance of 2,5 m apart to the nozzles already available
A representative sample of the interstitial space of at least 1600 mm × 900 mm shall be used The test sample shall include any seams/welds and intermediate layer and shall have at least two test nozzles
The test shall be carried out at a temperature above the freezing point of water
In the interstitial space a vacuum of (60 ± 5) kPa shall be generated by the vacuum pump The measuring device for pressure shall be connected to the test sample at the highest test nozzle
Trang 21These values shall be identically with the calculated values according to 4.1.3 with a deviation ± 10 %
5.1.4 Free passage of air
5.1.4.1 Free passage of air through intermediate layer
5.1.4.1.1 Test equipment
— Thickness tester, with an accuracy of 0,01 mm;
— two quadratic steel retaining plates 100 mm × 100 mm, thickness 10 mm;
— two quadratic steel pressure plates 150 mm × 150 mm, thickness 10 mm, with a hole of 10 mm each in the corner sphere One steel plate has a hole in the middle of the plate with a diameter of
6 mm and a fitting with a diameter of 6 mm is also welded on in the middle of the plate;
— four locking screws, 8 mm;
— compression device, with an accuracy of 1 %;
— air impermeable foil, e.g PE 0,75 mm thickness;
— environmental chamber;
— vacuum pump with constant volume flow of 85 l/h;
— measuring device for pressure accuracy 0,6 % of the maximum graduated value;
— measuring device for the volume flow accuracy 0,6 % of the maximum graduated value
NOTE The test at (60 ± 3) °C includes the test at (40 ± 3) °C
For protecting the lining the intermediate layer shall be tested at 1,3 times the maximum possible
surface pressure (pMS) according to Formula (2) – but a minimum of 50 kPa (0,5 bar)
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For protecting the jacket the intermediate layer shall be tested at a minimum of 1 MPa (10 bar)
Maximum possible surface pressure according to Formula (2):
First the initial thickness of the intermediate layers (s1) shall be measured with the thickness tester After the measurement the intermediate layers shall be laid between the two test plates Through the upper test plate the test samples shall be charged with the help of the compression device:
After reaching the steady-state condition but not before a minimum period of 14 days has elapsed the
residual thickness (s2) shall be measured and the test equipment shall be installed in the environmental chamber The test samples shall be charged further with the maximum possible surface
pressure (pMS) and the measurement of the thickness shall be repeated at the limiting temperatures
The steady-state condition has been reached, if two measurements of the residual thickness (s2) made
at intervals of 24 h do not differ by more than 1 % from the thickness (s1) If after 90 days the state condition has not been achieved the test has failed Following this test the intermediate layers shall be pressed with the help of the pressure plates and the locking screws until half of the residual
steady-thickness of the intermediate layers (s3) has been achieved or the pressure exceeds 2 ⋅ pMS
At the fittings, located in the middle of the plate, a vacuum pump with an inserted measuring device for pressure, e.g u-tube, shall be connected At the exit of the vacuum pump a valve for throttling the volume flow shall be installed, so that the volume flow can be adjusted to the given value of (85 ± 5) l/h through the secondary measuring device for the volume flow The length of the connecting line of the measuring device for pressure to the fittings of the interstitial space shall be 250 mm The flexible connecting lines at the connection of the vacuum pump and the measuring device for the volume flow shall be realized with an internal diameter of 6 mm
The total length of the connecting line from the fittings to the vacuum pump shall be max 1 m for the measurements
After installation of the test equipment as mentioned above and in Figure 2 the flow resistance shall be taken from the measuring device for pressure after turning-on the vacuum pump and adjusting the volume flow to (85 ± 5) l/h The measurement shall be repeated at each test sample The mean of the measured values shall be compared with the limiting value of −1 kPa
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Dimensions in millimetres
Key
1 connection for vacuum pump with 85 l/h air
2 measuring device for pressure
3 test plate
4 intermediate layer
5 air impermeable foil
Test sample Initial thickness
The test shall be deemed to have been passed, if the air current back pressure emanating from the
intermediate layer with the thickness s3 is not less than −1 kPa (10 mbar) at a volume flow of (85 ± 15) l/h of air
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5.1.4.2 Free passage of air through double skin tanks and pipes
5.1.4.2.1 Test equipment
— vacuum or pressure pump;
— measuring device for pressure accuracy 0,6 % of the maximum graduated value;
5.1.4.2.3 Procedure
The test shall be carried out at a temperature above the freezing point of water
The free passage of the interstitial space of the sample of the tank or pipework shall be tested by sampling by means of borings with a drill (2 mm) at positions determined by the person during the test The pressure or vacuum reached before the test is carried out shall be reduced within a short time according to the capacity of the interstitial space by charging and discharging and shall be visible
at the measuring device for pressure
5.1.4.2.4 Evaluation
The test shall be deemed to have been passed, if after opening of the interstitial space due to drilling a
2 mm hole air is deflated in the interstitial space at the pressure system and the pressure in the interstitial space falls or at the vacuum system air is sucked into the interstitial space due to drilling a
2 mm hole, so that the pressure in the interstitial space increases immediately
5.1.5 Flow resistance after impact of stored media
5.1.5.1 Test equipment
— valve;
— measuring device for pressure accuracy 0,6 % of the maximum graduated value;
— vacuum pump with constant volume flow of 85 l/h;
— measuring instrument for volume flow accuracy 2 % of the measured value
Trang 25The sides of the test specimen shall be closed gas tight At the exit of the vacuum pump a flow control valve shall be installed, so that the volume flow can be adjusted by the downstream volume indicator
to the given value of 85 l/h (Figure 3) The flexible interconnection lines for the connection of the leak detector and the volume indicator shall be designed with an inside diameter of 6 mm The entire length of the interconnection line of the connecting nozzle up to the measuring device for pressure shall be 1 m for the measurement
Dimensions in millimetres
Key
1 test nozzle ∅ 4 mm
2 measuring device for pressure
3 vacuum pump with constant volume flow of 85 l/h
4 measuring instrument for volume flow
5 interstitial space of the test sample
Figure 3 — Suitability test of the construction of the interstitial space
With tanks, the tests for determination of the flow resistance shall be carried out at three further test nozzles, which shall be distributed over the tank circumference With pipework, additionally to the connecting nozzles for the leak detector and to the test nozzles, two further test nozzles shall be installed at a distance of 2,5 m apart to the nozzles already available The testing apparatus shall be installed according to Figure 4 and Figure 5
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Key
1 valve
2 interstitial space
3 measuring device for pressure
4 vacuum pump with constant volume flow of 85 l/h
5 measuring instrument for volume flow
Figure 4 — Test set-up for the determination of the flow resistance of the interstitial space of
tanks
Key
1 valve
2 measuring device for pressure
3 vacuum pump with constant volume flow of 85 l/h
4 measuring instrument for volume flow
5 double skin pipework if needed with formed pieces and fittings
Figure 5 — Test set-up for the determination of the flow resistance of the interstitial space of
pipework 5.1.5.3 Procedure
The flow resistance for the interstitial space shall be determined by means of the test arrangement in Figure 3 to Figure 5
The test shall be carried out at a temperature above the freezing point of water
After installation of the test apparatus as shown above, the flow resistance shall be taken from the measuring device for pressure after starting the vacuum pump and adjusting the volume flow to
85 l/h The measurement shall be repeated at each test nozzle, while the test nozzle with the greatest
Trang 275.1.6 Mechanical resistance against the imposed load by the stored medium
5.1.6.1 Influence of the mechanical resistance to the free passage in the interstitial space
The test shall be carried out according to 5.1.4.2
5.1.6.2 Mechanical properties
The tests shall be carried out according to Table 3 to Table 8
5.1.7 Chemical resistance
5.1.7.1 Inner layer/outer layer in contact with the stored liquid
The components of the thermoplastic and thermoplastic elastomers leak detection lining kits according to Table 4 and Table 6
The components of the GRP leak detection lining kits and GRP leak detection jackets kits according to
EN 13121-1 and 5.2, 5.5 and 5.6 of EN 13121-2:2003
5.1.7.2 Intermediate layer in contact with the stored liquid
After the test according to 5.1.5 the flow resistance shall not exceed the value of 1 kPa at an air volume flow of (85 ± 5) l/h
5.2 Durability of effectiveness
5.2.1 Durability against temperature
For thermoplastic and thermoplastic elastomers leak detection lining kits according to Table 3 and Table 5
For intermediate layer according to 5.1.4.2
For GRP leak detection lining kits and leak detection jacket kits according to Table 7 and Table 8
5.2.2 Durability against chemical attack
The thermoplastic and thermoplastic elastomers leak detection lining kits according to Table 4 and Table 6
The UP and EP leak detection lining kits and leak detection jacket kits according to Table 7 or Table 8
5.2.3 Durability against mechanical load
5.2.3.1 Leak detection lining kits
The components of the thermoplastic and thermoplastic elastomers leak detection lining kits according to Table 3 and Table 5
The components of the UP and EP leak detection lining kits shall fulfil the requirements according to
EN 13121-1