Difu ion phenomena oc ur at the contact s r faces givin rise to, inthe interface, a series of new a lloy diferent from one another and diferent from b th the joinin material and the b as
Trang 1~
INT ER AT I N L OR A IZATION FR ST AN A DIZAT IO *MEX.U H P A A O PrA HM3AlJMR n CTA A PTM3A~CIMWR A lS TlO INTE N T I N LE D NORMALIS T I N
So dag e t te h iq e c n ee - Asemblag se é uté av cde produis d'ap ort debrasag te dre et de brasag fort
-Méth de d'e saimé aniq e
Fir st e ition - 198 5-0 -01
Desc ipto s : weldin , b ra zin - a d s ld rin , b ra ze - a d s ld re joints, t est s, me h nic l t est s, se r te ts, t en io te sts , te t e uipme t
Trang 2IS0(the InternationalOr ganization for Stand rdization)is a worldwid fe eration of
national stand r ds b dies (IS0 memb r b dies) The work of pre arin International
Stand r ds is normaly car r ie out throu h IS0tec nical commite s Eac memb r
b dy intereste ina s bject for whic a tec nical commite has b en esta ls e has
the rig t to b re resente on that commite International or ganization , govern-
mental and non-gover nmental, in laison with EO, a lso take p rt inthe work
Draf InternationalStand rds a o te by the tec nical commite s are circ late to
the memb r b dies for a proval b fore their ac e tan e as International Stand r ds by
the IS0Cou ci They are a pr ove inac ord n e with IS0proce ur es re uirin at
lea st 7 % a proval by the memb r b dies votin
International Stand rd IS0518 w a s pr ep r ed b Tec nical Commite ISO/TC 4,
Weldin and aled pro es s
I ca nc els and re la c es IS036 8 3-197 8 the s o e of whic w as more lmite
0 International Or ganization for Stand r dization, 19 5 O
Printe in Sw itzerla d
Trang 3soft solder s and brazing fi ler metals - Mechanical test
O Introduction
A joint is not a homogene u b dy but a heterogenou as s em-
bly forme from diferent mater ials havin diferent ph sical
and c emical pro erties In the simplest case, it con ists of fi er
metal and the b as e metal Difu ion phenomena oc ur at the
contact s r faces givin rise to, inthe interface, a series of new
a lloy diferent from one another and diferent from b th the
joinin material and the b as e metal
Inthe study of the stren th of s c heter ogene u joints, the
simplfie h p theses of the the ry of elasticity - vald for a
homogene u metal c b dy or st res es due to external forces
tran mite u iformly fromanelement of s rface or volume to
neig b urin elements - are no lon er a plca le
He nce , the notion of "joinin material stren th" ne ds to b
lmite strictly tometal soldifie afer meltin Conversely , the
stren thof an as embly is a fu ctionofthe intrin ic stren th of
the fi er metal and a s e ries of exter nal factors I folows that
tests d sig e to d termine this stren thne d to b car rie out
.ac or din topr ecise con ention , tak in into ac ou t ina di-
tion to the c aracteristic of the joinin material itself
a s e rie s
of external factor s, nota ly:
s a e of the sp cimen;
flu us e d;
-in temp r atur e, he tin rat e, etc ;
- time at joinin temp ratur e;
- joint c lea ra nc e;
- n mb r of tests;
-
-comp sition and stren th of b ase metal;
ge metry and state of the s rface of the joint
brazin or sold rin tec nique u e (he t sourc e, join-
metho u e to interpret the r es lts;
nature and s iz e of faults at the fracture s rface
To u d rstand the stren th of a joine a ssembly, this Inter
national Stand rd alows the d termination of the folowin
c aracteristic :
a) for brazin fi er metal
-temp rature or hot
-temp rature or hot
the in tantane u ten ie stren th, c old, at ambient
the in tantane u s e r stren th, cold, at ambient
-the cr ee stren th at elevate temp r atur es;
b) for sof sold r
-temp rature or hot
-hot the in tantane u s he ar stren th, cold, at ambient
the cr ee stren th, cold, atambient temp rature or
for a given brazin fi er met a l, flu and b as e metal
So that the tests are re ro u ible and c omp rable, it is imp r
tant to u e ten ie and s e ar sp cimen of a wel-d fine typ
and have r ecour se to a p rec ise o eratin metho This Inter
national Stand rd me ts this o jective
1
Scope and field of appl c tion
This International Stand rd d fines the prin iples and the
tec nique of the tests d sig e tod termine the con entional
mec anical c aracteristic of a ssembles pro u e with sof
sold rs and brazin fi er metals: it also sp cifies a- metho of
interpretin the res lts o taine
This International Stand rd is a plca le to joinin mater ials
and their flu es whic are u e for sold rin and brazin of fer
rou and non-ferou metals and aloy
2 1.1 Con entionals e r stren th
For the d termination of the con entional s he ar stren th, an
a ssembly of two fite p iec es is u e with pr ed termine joint
cle r an e so that the br aze joint is s bject to a s ea r str es
when a ten ie force is a ple to the sp cimen
Two sp cimen are pro ose (se fig res 1and 21 , the o erator
havin a c oice b twe n the two The typ of sp cimen c osen
s al b note inthe test re ort
2.1.2 Con entionalten ie stren th
For the d termination of the con entionalten ie stren th, an
a ssembly ma de end-to-end on two ba rs with a pre etermine
joint cle r an e atthe extremities is us ed
Fig r e 3 gives the dimen ion of the ten ie sp cimen
Trang 42.2 Ch ic of ba e metal an joint cle ranc
In or der too tainfracture at the joint the b ase metal s a ll b
c hosen, as far as p s ible, so that the fractur e lo d of the
br a ze a ssembly is lower than the loa d cor r esp ndin to the
ela stic lmit of the b ase metal
In pr a ct ice, if da ta is r equire for a sp cific a pplc a tion, the
p r ent metal for the sp c imen s a ll b the metal u e for the
comp nents in the cas e b in c on id red Simia r ly , the joint
c lea r a nc e inthe sp cimen s al b that u e inthe a plcation
The b as e metal and the joint c le ranc e s a ll b indicate inthe
test r ep r t
2.3 Preparatio of the surfa e
Bef or e the br azin o er ation, the s r f a ces to b br a ze ne d to
b clea n and c le r of oxid s, gre ase , oi, pa int etc A pr oces
a nd a cle nin agent s ite to the r equirements of the b as e
meta l s a ll b u e
Simiar l , the sp ec imen s a ll p os s e s s, at the joints, a s r face
conditioncor resp ndin to a r ou h es , Ra,b tw een 1,6 and
3,2 pm if they are c op er or co p r a lloy and a rou h es
b twe n 1,6 and 6,3 Iim if they are in non-aloye ste l
If the tests a r e d sig e for a p rtic lar case, the s r face con-
ditions a ll b that corr esp ndin tothe cas e u d r con id r -
at ion
The cle nin pro u t and proc es as wel as the s r face con-
dition at the joints s al b indicate inthe test r ep r t
2.4 Appl c tio of joining materiel an flux
The comp nent p r ts of the sp ec imen are a ssemble ina v er -
tical p sition, and the joinin ma terial, inan a pro r iate form
(w ir e, p wd r , etc is place at one sid of the joint ins f-
ficient quantity to fi the joint afer meltin
I it is neces a r y tou e a flu , a teste flu s ita le for the fi er
ma ter ia l and the b se metal s al b u e ; the u e of the flu
s a ll conformto the man factur er ’ in tru tion
The c aracter i tic of the flu s al b d taie in the test
r ep r t
2.5 He ting co ditio s
A s p ort d sig e to hold the sp cimen v er tica lly , in the
p sitionindicate in fig r es 1, 2 and 3, can b u e In order to
a v oid a ny lo d onthe joint durin co ln , this s p ort s a ll not
o stru t the contraction and exp n ion of the sp ec imen
as embly
In the cas e of he tin with an oxy -a cety lene f la me, the a -
pa r a tu s owninfig re 4 can b u e This con ists of a b se
pla te (1)onwhic is mou te a sp cimen s p ort (21, a c lamp-
in s stem (3) and a pivotin s p ort (4) for the blow-pip
s own s hematicaly at r ef er enc e p int (5 )
Other jg in arr an ements can b u e to s it the c osen
he tin metho
The as embly is r a ise tothe joinin temp r atur e by mea ns of
the selecte he tin metho (torc , indu tion, f ur nac e, etc If
it is not hea te u iformly ov er the complete len th (for
exa mple, torc hea tin , indu tion he tin ) it is es ential to
en ur e thatthe u iformjoinin temp r atur e is reac he ov er a
distan e of 10 mmeither sid of the joint
Su gestion
I he tin is c arr ie out by torc or indu tion, the sp cimen
he tin c yc le s ould b s c that the meltin temp r atur e
of the joinin mater ial is r eac he in 4 to 60 s , the he tin
c cle b in prolon e for 5 s afer this temp r atur e ha s
b en r ea che W ith the ex e tion of p r tic lar sp cifica-
tion , the sp cimen ne d to b maintaine at the brazin
temp ratur e for a p r io of 10 to 3 s
Al the o er atin condition s a ll b enter ed in the test r ep r t
NOTE - I the sp ci m en s h ave to b mae in order to ob tain f un-
damental nformation, the he atin condition are lef to the init ia t ive of
the test controle r
2.6 Number of spe imens
2.6.1
at ambient temp r ature or cold
Fiv e sp c imen are neces a r y to d ter mine the stren th
2.6.2 Fiv e toten sp ec imen a r e nec es ary toplot a c r ve of
stren that hig temp r atur e or u d r c r ee
Afer joinin , the ten ie and s e r sp c imen are mac ine a c -
cordin to fig r es 1, 2 and 3 in s c a way thatthe stren th
pr op r ties of the joint wi not b influen e
Al tests are c arr ie out injg ona mac ine p s es in (pr efe-
r ably) a dju ta ble c lamps in ord r to avoid pa r a sitic
b ndin stres es inthe sp c imen The s ea r tests onthe sp -
c imen s owninfig r es 1and 2 a r e c arr ie out withthe mou -
tin a r r a ngement s s own infig r es 5 and 6
The joint stren th expres e inmega pa sca ls (MPa) is o taine
by dividin the fracture lo d expres e in newton by the s r -
f ac e area of the braze joint’) expres e in squa r e mi metr es
The r es lts ofthe fracture examination s a ll b note in the test
r ep r t
For the in tantane u s ea r and ten ie tests at cold, at
ambient temp r atur e (b twe n 18 and 2 OC) or at hottemp -
r a ture, imp sin of the lo d ne ds to b ca r rie out withthe
test mac ine r eg late [rate of displacement expres e in
micrometres p r second (pm/s) or reg lation of force ex-
pr es e innewton p r second (N/s)lso as to b comp tible
with the c ar acter i tic of the fi er meta l s bmite to the
tests
1)
If faults h ave a p ar ed in the fractured s rface, the surface s al b analy ed a d the presen e of faults indicate d in the test re ort
2
Trang 5The in tantane u hots e ar orten ie sp cimen s al b e put
u d r lo d ona ten ie mac ine e uip e witha furnace The
sp cimen temp rature s al b sta i ze for 1 h b fore imp -
sin the lo d and furnace temp rature reg lation s al b e within
+I %
For cr ee test sp c imen , a cre plfracture mac ine s al b
u e The temp rature s al b sta i ze for 2 hb fore imp s-
in the lo d and furnace temp rature reg lation s al b within
f 1 % If cre p is carr ie out at amtjent temp r atur e, the later
re uirement is a question of judgment
The fracture s rface ne ds to b examine and the res lts of
the examinations al b e note in the test re ort
3.1
tensie te ts at ambient temperature
Interpretatio of instantaneo s she r an
To faci tate the a plcation of the in tantane u s he ar test
r es lts at ambient temp r ature, it is p s ible to us e a statistical
interpretation by calc latin the mea n and stand rd d viation
of the test res lts
This me an, 5 and stand rd d viation, s, are d termine as
folows:
- c Xi
x=
-n
Sin e the r es lts are for a given joinin mater ial, the mea n value
can b fixe totend toa minimum Mo
This proce ure can b explaine as folows:
- the ratios b twe n the varia i ty due to the test
metho and the varia i ty due to the joinin mater ial itself
are not known;
- to fix a ran e of "minimum toleran es" d mands
severa l prelminary tests for a ll the typ s of existin joinin
mater ials:
- the n mb r of tests re uire to evaluate the "minimum
toler an es" is gener aly hig er than that re uire for the
evaluation of me n
Und r these condition and con id rin the r es lts of n t est s,
one fixes as a rule to ac e t a joinin mater ial of a given
clas ificationwhen it is c ar acter i e by a minimum me n Mo
s c that
- the pro a i ty of ac e tin a joinin material for whic
the mea n stren th is le ss thanMo is at most e ual to a smal
n mb r
j?(c stomer's risk )
- a joinin material givin a lar ge the retical pro ortion P
of res lts hig er thanMo is ac e te ina large n mb r of
cas es ( - a), a b in the man facturer's risk
I S0 518 -1985 (E)
T hese condition s al b resp cte whatever the u known
stand rd d viation c aracterizin the b haviour of the joinin
material durin the test
Each joinin material is con id r ed to fulfi the fixe condition
con ernin M, if the mea n Xofthe r es lts xi of n tests satisfies
the condition :
Y- ks
>
Mo
I one fixes the risk a - B = 0,l for P = 1 %, one finds by
referin to existin var ia le sampln ta les that
for n = 5
k = 0,68
o
Und r these condition , i?b in the mea n of five tests, one
s ould ha v e
Y- 0,6 s > Mo
The calc lation k and n is b se on the fact that in a first
a proximation, the res lts folow a normal law The u certain
var ia le
folows Stud nt's law (if the mea n is Mo)or a d centre
Stud nt's law of 1,21 6 fi (whenP = 1 %), and k and n
va lues are d termine by the two condition :
Pr (t> k n) = a = 0,l ít centre )
Pr (t> k n) = j = 0,l ( decentre )
The en isage risk s ee ms r easona le for the fixe test condi-
tion b ca use it imples a smal n mb r of tests w hic , from an
economic viewp int is far from neglgible
3.2 Hot instantaneo s she r te t
The hot in tantane u s ea r tests p rmit the plotin of the
c rve for fracture s tre ss , in mega a sc als, as a fu ction of
temp r atur e, ind gr ees Celsiu
Fig r e 7 s ows an example of a c rve o taine from thre
temp rature tests
3.3 Cre p she r te ts
Withone or severa l temp r atur es, the o jective of these tests is
to plot one or several c rves:
Fr acture s tre s s, in mega pas a ls =
f (time to fr acture, in
hours)
The st res es ne d tob c osen ins c a way as too tainfrac-
ture times b twe n0,l and IO3 h For sp cial cas es , it wi b e
p s ible to researc h st res es givin fracture times of IO5 or
IO6 h
Fig r e 8gives a metho for presentin the res lts
Trang 6@ O h8
T
1 0
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-Te t pie e d tais
3
+
c
Dime sio s in mi metr es, s rfa e
ro g n s v lue s in micrometre
Fier metal
Te t pie e before brazin
Te t pie e afer ma hinin
Fig re 1 - T p e I s hea rin te t p ie c e dime ns io s
Trang 7D ime sio ns in mi metes , sura e
ro ug n ss valu s in micr ome tr e s
X A ccordin t o ga p
.Ga outlet
Fi er me ta l
7
Te t pie e d tais ' Te t pie e before brazin or sold rin Te t pie e afer ma hinin
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