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Effects of high temperatures on mechanical behavior of high strength concrete reinforced with high performance synthetic macro polypropylene (HPP) fibres

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Today, the advancement of technology and the achievement of increasing innovations in the field of building materials have increased high-strength concrete (HSC) production. The use of this material has been increased due to economic and technical reasons in the construction of concrete sections. However, the more compressive strength of the concrete is, the more concrete becomes brittle and its tensile strength does not increase with increasing compressive strength. HSC is also more vulnerable to high temperatures due to its high density and low porosity compared to conventional concrete. Researchers have proposed different methods including the use of polypropylene fibres in concrete mix designs in order to overcome these defects of HSC. In this study, a new type of polypropylene fibres, called high performance synthetic macro polypropylene fibres (HPP), have been used in dosages of 1, 2 and 3 kg/m3 . Tests on hardened concrete include compressive strength, tensile strength and flexural strength at temperatures of 25, 100, 200 and 300 C. By adding 1 kg of fibres to HSC, its compressive strength, tensile strength and flexural strength increased up to 14, 17 and 8.5%, respectively. Furthermore, the greatest improvement in the mechanical properties of concrete exposed to high temperatures was obtained when 1 kg/m3 of fibres was added to HSC.

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Effects of high temperatures on mechanical behavior of high strength

concrete reinforced with high performance synthetic macro

polypropylene (HPP) fibres

Department of Civil Engineering, Isfahan (Khorasgan) Branch, Islamic Azad University, Isfahan, Iran

h i g h l i g h t s

HPP Fibers did not have significant effect on the compressive strength of concrete

Mechanical properties of HSC were enhanced when HPP fibers were added

Addition of HPP fibers postponed the spalling of HSC when exposed to high temperatures

Discussion about the optimum dosages of HPP fibers was made

a r t i c l e i n f o

Article history:

Received 29 September 2017

Received in revised form 8 January 2018

Accepted 9 January 2018

Keywords:

High strength concrete

High performance synthetic macro

polypropylene fibres (HPP)

Fibre reinforced concrete

High temperatures

a b s t r a c t

Today, the advancement of technology and the achievement of increasing innovations in the field of building materials have increased high-strength concrete (HSC) production The use of this material has been increased due to economic and technical reasons in the construction of concrete sections However, the more compressive strength of the concrete is, the more concrete becomes brittle and its tensile strength does not increase with increasing compressive strength HSC is also more vulnerable

to high temperatures due to its high density and low porosity compared to conventional concrete Researchers have proposed different methods including the use of polypropylene fibres in concrete mix designs in order to overcome these defects of HSC In this study, a new type of polypropylene fibres, called high performance synthetic macro polypropylene fibres (HPP), have been used in dosages of 1, 2 and 3 kg/m3 Tests on hardened concrete include compressive strength, tensile strength and flexural strength at temperatures of 25, 100, 200 and 300°C By adding 1 kg of fibres to HSC, its compressive strength, tensile strength and flexural strength increased up to 14, 17 and 8.5%, respectively Furthermore, the greatest improvement in the mechanical properties of concrete exposed to high tem-peratures was obtained when 1 kg/m3of fibres was added to HSC

Ó 2018 Elsevier Ltd All rights reserved

1 Introduction

Concrete is one of the most important and most popular

building materials, featuring advantages such as plasticity prior

to hardening, good compressive strength and the availability of

its constituent materials Due to advances in technology, the use

of high-strength concrete (HSC) has been increasing in recent

years In parallel, many studies have been done to improve the

weaknesses of this type of concrete, including its low tensile

strength and ductility compared to its compressive strength[1,2] and its greater vulnerability at high temperatures among various types of concrete Studies show low resistance of concrete in high temperatures, so that exposure of concrete to high temperatures leads to cracking and explosive spalling Accordingly, the strength and modulus of elasticity of HSC drops significantly[3–9] Concrete may be exposed to high temperatures in cases such as the occurrence of fire in concrete structures, in the explosion of jet engines, in factories in the extraction and melting of metals, in some chemical plants where concrete is close to the furnace, and related-nuclear activities Adding fibres is the most widely known method to prevent spalling of HSC[10–17] Among fibres, adding polypropy-lene (PP) into HSC shows better performance in order to increase

https://doi.org/10.1016/j.conbuildmat.2018.01.064

0950-0618/Ó 2018 Elsevier Ltd All rights reserved.

⇑ Corresponding author.

E-mail addresses: hamidbehbahani@gmail.com , hbehbahani@khuisf.ac.ir

(H.P Behbahani).

Contents lists available atScienceDirect Construction and Building Materials

j o u r n a l h o m e p a g e : w w w e l s e v i e r c o m / l o c a t e / c o n b u i l d m a t

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resistance of HSC at elevated temperatures[18–20] In addition, it

caused improvement in the mechanical properties of HSC and its

shrinkage control[21–27] Investigating the spalling phenomena

for concrete by incorporating polypropylene fibres, Lura and Terrasi

[18]found that spalling was substantially decreased by adding to the

concrete small quantities (almost 0.1% by volume) of fibres made

from a low melting-point polymer Noumowe[28]and Sahmaran

et al.[29]studied the mechanical and microstructure properties of

HSC in face of high temperatures It was found that the pore

struc-ture at high temperastruc-ture may have a considerable influence on the

spalling behavior of the high strength polypropylene fibre concrete

Polypropylene fibres are melted when exposed to high

tempera-tures, and creating channels in concrete mass prevents the

forma-tion of high vapor pressure in concrete pores, which reduces the

spalling of concrete In addition, the fibrous concrete cool slower

than normal concrete, resulting in fewer cracks in cooling phase

Other researches have studied properties of HSC with combination

of Polypropylene and other fibres, e.g steel fibres in order to improve

the mechanical properties of HSC[30,31]

This study investigates the effects of adding a new type of

polypropylene fibres, called high performance synthetic macro

polypropylene fibres (HPP), on the mechanical properties of

con-crete at elevated temperatures up to 300°C These fibres are made

of polymer materials that have an especial sine-shape The physical shape of these fibres makes them superior for concrete mixture when compared with the common type of fibres In addition, com-pared to typical fibres, they also have a higher modulus of elasticity and tensile strength[32,33] Among advantages of this type of fibre are enhancing the concrete resistance to stress, fatigue, heat, and increase tensile, shear and flexural strength in concrete.Table 1 shows the differences between properties of HPP fibers and a common type of polypropylene fibers Their physical shapes are displayed inFig 1 The objectives of this research are (i) to obtain the effect of high temperatures on the mechanical properties of conventional normal concrete (NC) and HSC; (ii) to study the effect

of adding polypropylene fibres with different dosages on mechan-ical properties of HSC; (iii) to examine mechanmechan-ical behavior of high strength HPP fibre concrete at elevated temperatures up to 300°C

2 Test program and procedures 2.1 Concrete mix design and testing Two different types of concrete including normal concrete and HSC are used in this research with strength of 25 and 69 (MPa)

Table 1

Technical specifications of studied HPP fibres compared with a typical PP fibre.

Type of Fibre Physical Shape Density (gr/cm 3

) Tensile Strength (MPa) Modulus of Elasticity (MPa) Melting Point (°C) Diameter (mm) Length (mm)

Fig 1 Physical shape of fibres (a) studied HPP fibres (b) typical type of PP fibres.

Table 2

Concrete mix design of samples.

Type of Concrete Sample W/C D max

(mm)

Coarse Aggregate (kg/m 3 )

Fine Aggregate (kg/m 3

(kg/m 3 ) Fibre Content (kg/m 3 )

Super Plasticizers (%)

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Effects of adding HPP fibres on properties of HSC were studied at

three different dosages of 1, 2 and 3 kg per cubic meter of concrete

The mix design to achieve HSC was in accordance with DOE

method [34] and is presented in Table 2 Naming the samples

was done in such a way as to represent the type of sample HSC

represents high strength concrete and the number after that

indicates the fibre content in a cubic meter of HSC NC represents

the normal concrete

Concrete samples were tested at day 7 and day 28, and three

samples were made for each design The experiments carried out

in this study are compressive strength test in accordance with B

S 1881: Part 116 standard, splitting tensile strength test according

to ASTM C496/C496 M-04 regulation, flexural strength test

follow-ing ASTM C293 The samples were exposed to three different

tem-peratures of 100, 200 and 300°C according to ISO-834 standard

using oven The electric oven used in this study is shown in

Fig 2 The number and type of studied specimens and testing

pro-cedure are presented inTable 3

Different methods are used to make fibre reinforced concrete

Type of work, facilities and equipment are among the factors that

are important in choosing production methods It should be noted

that in any method of production of fibre reinforced concrete, the

distribution of fibres in a mixture should be homogeneous to

pre-vent fibres from balling The balling or conglobation of fibres

dur-ing the mixdur-ing process depends on several factors, with the most

important parameter being the aspect ratio Other factors that

affect the fibre distribution include fibre percentages, grain size,

aggregate size and quantity, the ratio of water to cement, mixing

method Higher amount of aspect ratio, volume percentage of

fibres, and size of the aggregates increased the tendency for

bal-ling The fibre concrete mixing design is similar to other concrete

and for a specified mixture, the slump decreases with increasing

fibre content For a uniform distribution of fibres in the mixture,

the proper performance of the concrete is important Additives

materials may be used to create air bubbles, water reduction and

shrinkage control InFig 3, an illustration of the studied fresh fibre

reinforced HSC is presented

2.2 Materials The cement used in this research was the production of Ardestan cement plant with the shown properties in Table 4 In order to make experimental samples, a washed sand from Isfahan flood plain was used with a fineness modulus of 1/3 in accordance with ASTM C-125 standard The sand used in this study was moun-tainous materials in Isfahan with a maximum size of 19.5 mm, specific gravity of 2.68 gr/cm3and bulk density of 1500 kg/m3 In this research, super plasticizer Dynamon SP 5600, without any chlorine based on formulations containing advanced poly-carboxylate molecular chains, is used to provide the required

Fig 2 A view of used electric oven.

Table 3

Number and type of concrete samples for testing.

 10  50

59

50

0 20 40 60 80

Temperature (°C )

HSC NC

Fig 4 Effects of high temperatures on NC and HSC samples.

Fig 3 Studied fresh concrete containing HPP fibres.

Table 4 Properties of used cement.

Chemical analysis Blaine (cm 2

/gr) 3200 ± 100

Al 2 O 3 (%) 5.2 ± 0.2

Fe 2 O 3 (%) 4.6 ± 0.2

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performance for high-strength concrete This product is

manufac-tured in accordance with type F, G ASTM C-494 and EN 934-2

standards

3 Results and discussion

This part is categorized into four sections Section3.1presents

results of compressive strength test on NC and HSC specimens

exposed to high temperatures In Section3.2, the results of adding fibres on workability of HSC are discussed Section3.3presents the effects of HPP fibres on mechanical properties of HSC, including compressive strength, tensile strength and flexural strength Finally, mechanical behavior of HSC with addition of HPP fibres

at designated high temperatures are described in Section3.4 3.1 Compressive strength of ordinary concrete and HSC against heat The results of the compressive strength test on ordinary con-crete and HSC samples are demonstrated inFig 4at temperatures

of 100°C, 200 °C, and 300 °C It should be noted that the heated samples were tested after removal from the oven, followed by cooling to ambient temperature of about 25 ± 2°C

It was seen that the strength of both NC and HSC reduced when exposed to high temperatures The compressive strength of normal concrete in the face of heat was reduced with a slight slope and reduced by 4%, 8%, and 14% when exposed to temperatures of

100, 200 and 300°C, respectively Compressive strength of HSC decreased significantly such that its strength reduced up to 7.2%, 14.5%, and 27.5% after exposure to 100°C, 200 °C and 300 °C, respectively This proves that the HSC is more susceptible to spalling than normal concrete at high temperatures

3.2 Effects of adding HPP fibres on workability of fresh HSC The slump test was used in order to measure workability of concrete samples.Table 5indicates the slump value of different types of samples

Table 5

Results of the slump test on fresh concrete.

66.12

60.2

54

56

58

60

62

64

66

68

70

Type of Sample Fig 5 The effect of HPP fibres on compressive strength of HSC.

12.2

12.5

11.5

11.7

11.9

12.1

12.3

12.5

12.7

Type of Sample Fig 6 The effect of HPP fibres on splitting tensile strength of HSC.

6.5

6.71

6.8

7.09

6.2 6.3 6.4 6.5 6.6 6.7 6.8 6.9 7 7.1 7.2

Type of Sample Fig 7 The effect of HPP fibres on the flexural strength of HSC.

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According to mentioned table, the amount of concrete

worka-bility reduced by adding HPP fibres and it continued to reduce by

increasing amount of fibres However, addition of 1 kg HPP fibres

had no significant effect, reducing workability by only 5%

3.3 Effect of adding HPP fibres on mechanical properties of HSC

HSC specimens with different dosages of HPP fibres The results

showed that the compressive strength of the HSC had negligible

change by adding 1 kg fibres The compressive strength decreased

with increasing fibers content; however, this reduction is not

sig-nificant Addition of fibres into HSC led to decrease by 4.3%, and

12.7% in compressive strength of mixtures with fibre content of

2 kg and 3 kg, respectively Similarly, reduction in compressive

strength of concrete due to addition of different types of

polypropylene fibres was obtained in other studies, e.g.[27,35]

This reduction could be attributed to the presence of voids due

to the addition of HPP fibre and the existence of weak interfacial

bonds between the HPP fibers and cement particles[36]

tensile strength of HSC As can be seen, addition of 1 kg fibres did

not affect the tensile strength of HSC The tensile strengths of HSC

specimens containing higher content of fibres were higher than those of the HSC specimens without fibres When the splitting occurred and was sustained, the HPP fibres bridging the split parts of the specimens acted over the stress transfer from the matrix to the fibres, and gradually supported the full tensile stress The transferred stress enhanced the tensile strain capacity

of the concrete matrix, and thus improved the tensile strength of

Table 6

Testing results of HSC specimens with fibres in different temperatures.

Type of Sample Temperatures (°C) Compressive strength (MPa) Tensile strength (MPa) Flexural Strength (MPa)

7-day 28-day change (%) 7-day 28-day change (%) 7-day 28-day change (%)

45

50

55

60

65

70

75

Temperature (° C)

Fig 9 28-day compressive strength of HSC with different dosages of fibres in

different temperatures.

8 9 10 11 12 13

Temperature (° C)

Fig 10 28-day tensile strength of HSC with different dosages of fibres in different temperatures.

4 5 6 7 8

Temperature (° C)

Fig 11 28-day flexural strength of HSC with different dosages of fibres in different temperatures.

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the fibrous mixtures over the non- fibrous concrete mixture

counterpart

HSC specimens with different contents of fibres The results

show that using fibres increases the flexural strength of HSC

Adding different contents of 1 kg, 2 kg and 3 kg fibres into HSC

caused increase in flexural strength up to 3.1%, 4.6% and 9%,

respectively It could be due to bridging mechanism of fibres

which prevent the growth of cracks and reduce crack width

under flexural test

Overall, through observing the mechanical properties of HSC

equipped with HPP fibres, it can be obtained that the addition of

fibres caused reduction in compressive strength of HSC; however,

this reduction is negligible when 1 kg fibres were added Tensile

strength and flexural strength of concrete increased by addition

of fibres

3.4 Effects of adding HPP fibres on properties of HSC exposed to high

temperatures

HSC specimens without fibre and with fibres were put inside

the furnace and heated to temperatures of 100, 200 and 300°C

The samples were naturally cooled to reach ambient temperature

The results of measurement of compressive strength, tensile

strength and flexural strength of HSC with different dosages of

fibres in different temperatures are recorded in Table 6 and

depicted inFigs 9–11 All of experimentally obtained results are

provided in detail and presented inAppendix A

Generally, it can be seen that the concrete samples lost their

strength when exposed to high temperatures Non-fibrous HSC

were damaged more than fibrous concrete With respect to

Table 6, the plain HSC experienced drops in compressive

strength up to 7.2%, 14.5% and 27.5% when exposed to

temper-atures of 100, 200 and 300°C, respectively However,

compres-sive strength of HSC.1 reduced 5.2, 8.12 and 14% when

exposed to temperatures of 100, 200 and 300°C, respectively

In addition, Table 6 reveals that the specimens with content

of 1 kg fibres showed better performance in the face of high

temperatures compared to other specimens containing higher

amount of fibre Fig 12 shows an exterior of heated HSC

spec-imen reinforced by fibres and the channels formed on the sam-ple are observed

The results are in agreement with other studies Porosity of HSC increases with addition of fibres, resulted in reducing vapor pres-sure in the pores in the deeper concrete areas and control cracking

In addition, the melted polypropylene fibres due to high tempera-tures cause the creation of channels in the concrete mass that allows water vapor to evacuate, releasing pore pressure, gradually reducing the temperature, and decreasing the cracks in the cooling phase[8,22,37–39]

Finally, it should be mentioned that results of previous section showed addition of 1 kg/m3HPP fibres did not sacrifice workability and compressive strength of the concrete while increasing the flex-ural strength of the HSC Thus, it could be concluded that the opti-mum dosage of addition of HPP fibres into concrete is 1 kg/m3, which not only improves the mechanical properties of the HSC, but also caused higher resistance of the HSC at elevated tempera-tures up to 300°C

4 Conclusion This paper investigated effects of different dosages of HPP fibres on mechanical behavior of HSC The effects of high temper-atures on properties of non-fibre and fibrous HSC was also stud-ied Normal concrete was found to be less damaged than HSC when exposed to high temperatures The addition of HPP fibres

to HSC improved the tensile strength and flexural strength of HSC which could be due to distribution of tensile stresses and the prevention of growth of cracks in concrete Addition of HPP fibres reduced compressive strength of HSC which could be due

to fibre compression and reduction in concrete condensation However, this reduction was negligible when 1 kg of fibres were added Adding more than 1 kg/m3 of fibres caused significant reduction in workability of fresh concrete as well It could be con-cluded that the best improvement in properties of HSC was achieved by adding content of 1 kg/m3 fibres The addition of HPP fibres to HSC improved the behavior of concrete when exposed to high temperatures HSC exposed to heat at a temper-ature of 300°C experienced compressive strength reduction of about 28% while a 14% reduction was found in concrete contain-ing 1 kg/m3HPP fibres

Fig 12 View of the channels created by the melting of the fibres in the cube sample.

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Appendix A

Following tables display the experimentally obtained results for concrete specimens in detail

Table A.1 The 7-day test results of HSC specimens with fibres in different temperatures

Type of Sample Temperatures (°C) Compressive strength

(MPa)

Tensile strength (MPa) Flexural strength (MPa)

⁄ N.A.: Not Available.

Table A.2 The 28-day test results of HSC specimens with fibres in different temperatures

Type of Sample Temperatures (°C) Compressive strength

(MPa)

Tensile strength (MPa) Flexural strength (MPa)

⁄ N.A.: Not Available.

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