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DSpace at VNU: Effect of the crystalline electric field on the Neel temperatures of RCu2 compounds

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E!ect of the crystalline electric "eld on the NeHel temperatures of RCu compounds Faculty of Physics, Center for Materials Science, National University of Hanoi, 334 Nguyen Trai, Hanoi,

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* Corresponding author Fax: #84-4-858-94-96.

E-mail address: luong@cms.edu.vn (N.H Luong).

E!ect of the crystalline electric "eld on the NeHel temperatures

of RCu compounds

Faculty of Physics, Center for Materials Science, National University of Hanoi, 334 Nguyen Trai, Hanoi, Viet Nam

Van der Waals-Zeeman Laboratorium, Universiteit van Amsterdam, Valckenierstraat 65, 1018 XE Amsterdam, Netherlands

Abstract

Values for the NeHel temperature of the RCu compounds (R"Tb}Tm) have been calculated using a molecular-"eld model including crystalline-electric-"eld e!ect as presented by Noakes and Shenoy The calculated results show that the unusual behavior, at the NeHel temperatures, of these compounds can be explained on the basis of this model  2001 Published by Elsevier Science B.V.

Keywords: Crystal-"eld e!ect; NeHel temperature; Rare-earth intermetallic compounds

The RCu (R"rare-earth) compounds

crystal-lize in the orthorhombic CeCu structure The

magnetic properties of these compounds were "rst

studied by Sherwood et al [1] as early as in 1964

Most of the RCu order antiferromagnetically with

values for the NeHel temperature, ¹,, below 55K

Hashimoto et al [2] performed magnetization and

magnetic susceptibility measurements on

single-crystalline RCu samples A large magnetic

anisot-ropy was found to be present The magnetic

properties of the RCu compounds have been

extensively studied in recent years (see a review

by Luong and Franse [3] and references

therein)

One of the features of the RCu compounds is

that the values of the NeHel temperature for these

compounds are not simply proportional to the de

Gennes factor (gH!1)J(J#1) and reach a

max-imum for TbCu This fact suggests that the Ruder-man}Kittel}Kasuya}Yosida (RKKY) interaction alone is not su$cient to fully understand the mag-netic interactions in the RCu compounds In spite

of a substantial progress in the study of the mag-netic properties of the RCu compounds, the above-mentioned exception to the de Gennes rule remained unexplained

In this paper, we report on our calculations that have been performed in order to explain the anom-alous behavior, at the NeHel temperature, of the RCu compounds (R"Tb}Tm)

Our calculations are based on the model of Noakes and Shenoy [4] When considering only the exchange Hamiltonian, the de Gennes rule can

be derived in the simple molecular-"eld model: the rare-earth-atom Hamiltonian

(where the z-axis is de"ned to be the

ordered-moment axis andC the exchange parameter) leads

to an implicit equation for1JX2, and the ordering

0304-8853/01/$ - see front matter  2001 Published by Elsevier Science B.V.

PII: S 0 3 0 4 - 8 8 5 3 ( 0 0 ) 0 1 3 9 0 - 1

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Table 1 Values for the crystalline-electric-"eld parameters and the NeHel temperatures in the heavy RCu compounds

R B (K) B (K) ¹,exp (K) ¹,cal (K)

41 [1]

42 [6]

53.5 [2]

48.5 [5]

48 [14]

31.4 [2]

26.7 [5]

27 [7]

9.8 [2]

9.6 [5]

11 [19]

Er ! 0.28 [7] ! 0.22 [7] 11 [1] 9.1, 11.7

13.5 [2]

11.5 [5]

Tm ! 0.94 [8] ! 1.23 [8] 6.3 [20] 4.3, 6.7

NeHel temperature predicted by the full CEF Hamiltonian with

the B KL sets from Refs [7,8] for ErCu and TmCu, respectively.

temperature is obtained from the small 1JX2 limit

as

¹"2C (gH!1)J(J#1)/3. (2)

When the crystalline-electric-"eld (CEF) e!ects

are signi"cant, the de Gennes behavior is not to be

expected In this case, CEF Hamiltonian should be

added to the H This leads to the following

expression for the ordering temperature:

¹+"2C (gH!1)1JX(¹+)2!#$, (3)

where 1JX(¹+)2!#$ is the expectation value of

J X under the in#uence of CEF Hamiltonian alone

at the temperature ¹+ The exchange parameter, C,

can be evaluated from the ordering temperature of

the Gd compound when modeling a series of

rare-earth compounds, because Gd, an ¸"0 ion, is

essentially una!ected by CEF

For calculating values of the NeHel temperatures,

¹,, of the RCu compounds, expression (3) is used

in which ¹+ stands for ¹, For evaluating C in

these compounds, we take ¹,(GdCu)"¹"

41 K [1,5,6]

In the coordinate system of b"z, c"x and

a"y, the orthorhombic CEF Hamiltonian of

a CeCu-type of structure is given by

H!#$"BO#BO#BO#BO

#B O#BO#BO

#B O#BO, (4)

where B KL are the CEF parameters and OKL the

Stevens equivalent operators As pointed out by

Luong and Franse [3], information about the

cry-stalline-electric-"eld interaction in RCu is not

complete Until now, the full set of CEF parameters

is available only for NdCu, ErCu and TmCu

Nevertheless, the two lowest-order CEF

para-meters B  and B have been derived for most of the

RCu compounds (see Ref [3] and references

therein) In our calculations, we "rst used the two

lowest-order terms in the CEF Hamiltonian

Values for B  and B were taken for TbCu,

DyCu and HoCu from Ref [2], for ErCu from

Ref [7] and for TmCu from Ref [8]

In TbCu, DyCu and HoCu the magnetic

moments lie along the a-axis, whereas in ErCu

and TmCu the magnetic moments are oriented

along the b-direction [2,9}17] The ¹, values for

ErCu and TmCu were calculated directly using the CEF Hamiltonian (4) with only the two lowest-order terms For the RCu compounds with R"Tb, Dy and Ho, we used the CEF Hamiltonian transformed in the new coordinate system of

a"z, b"x, c"y as follows [18]:

H!#$"()(!B!B)O#()(3B!B)O (5)

The calculated values of ¹, are compared with experimental data in Table 1 and also in Fig 1 As one can see from Table 1 and Fig 1, addition of CEF interaction enhances ¹, over the de Gennes values in the RCu compounds Moreover, calcu-lations predict that TbCu has a highest NeHel tem-perature, in good agreement with experiments The calculated values for the NeHel temperatures across the series are in good agreement with experimental ones Calculations gave the value of ¹, for HoCu

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Fig 1 Comparison of experimental and calculated NeHel

tem-peratures for the RCu compounds The open circles represent

experimental data The solid circles (solid line) represent

calcu-lations using a CEF Hamiltonian with two lowest-order terms,

and the solid squares * calculations with the full CEF

Hamil-tonian as discussed in the text The dashed line represents the de

Gennes rule.

to be somewhat higher than the one obtained from

experiments

We tried also to derive the values for the NeHel

temperature of ErCu and TmCu with the full

B KL set taken from Refs [7,8], respectively The

results of these calculations using the full CEF

Hamiltonian (4) are also given in Table 1 and in

Fig 1 As it can be seen, the use of the full CEF

Hamiltonian gives better results than the use of the

two lowest-order CEF terms only

In conclusion, the magnetic ordering

temper-atures in the RCu compounds can be explained by

a combination of the RKKY interaction and

cry-stalline-electric-"eld e!ects

References

[1] R.C Sherwood, H.J Williams, J.H Wernick, J Appl Phys.

35 (1964) 1049.

[2] Y Hashimoto, H Fujii, H Fujiwara, T Okamoto, J Phys Soc Japan 47 (1979) 67.

[3] N.H Luong, J.J.M Franse, in: K.H.J Buschow (Ed.), Handbook of Magnetic Materials, Vol 8, North-Holland, Amsterdam, 1995, p 415.

[4] D.R Noakes, G.K Shenoy, Phys Lett 91A (1982) 35 [5] N.H Luong, J.J.M Franse, T.D Hien, J Magn Magn Mater 50 (1985) 153.

[6] M.K Borombaev, R.Z Levitin, A.S Markosyan, V.A Reimer, E.V Sinitsyn, Z Smetana, Zh Eksp Teor Fiz 93 (1987) 1517 (Eng Transl., Sov Phys JETP 66 (1987) 866).

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[14] Z Smetana, V Sima, Czech J Phys B 35 (1985) 1232 [15] Y Hashimoto, H Kawano, H Yoshizawa, S Kawano,

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J Bischof, J Phys.: Condens Matter 1 (1989) 10153 [17] M Heidelmann, B Lebech, Z Smetana, M Loewenhaupt,

J Phys.: Condens Matter 4 (1992) 8773.

[18] M Divis, S Zajac, V Sima, Z Smetana, J Magn Magn Mater 68 (1987) 253.

[19] R.R Birss, R.V Houldsworth, D.G Lord, J Magn Magn Mater 15}18 (1980) 917.

[20] Z Smetana, V Sima, J Bischof, P Svoboda, S Zajac,

L Havela, A.V Andreev, J Phys F 16 (1986) L201.

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