Affinity guided isolation, structure elucidation and total synthesis of laetirobin a and its analogue synthesis for therapeutic development 7

Appendix 7 High-Resolution Mass Data... High-Resolution-Mass Data 389... High-Resolution-Mass Data 403O O MeO.

Appendix 7

High-Resolution Mass Data

Appendix 7

380

OH

HO O

I

3-11

C8H7IO3277.9440

High-Resolution-Mass Data 381

OTs

TsO O

I

3-2

C22H19IO7S2585.9617

High-Resolution-Mass Data 387

O O

O O

HO O

HO O

OH O

4-38

C48H38O14838.2262 O O

Appendix 7

388

High-Resolution-Mass Data 389

High-Resolution-Mass Data 391

O O

5-4

C36H24O4520.1675

Appendix 7

392

O O

O O

5-6

C36H24O4520.1675

High-Resolution-Mass Data 395

OBn OTs

O

OTs O

5-10

C43H36O9S2760.1801

Appendix 7

396

OBn OH

O

OH O

5-11

C29H24O5452.1624

High-Resolution-Mass Data 397

OBn O O

5-12

C29H24O5452.1624

Appendix 7

398

O O

High-Resolution-Mass Data 399

OTs I TsO

5-18

C20H17IO6S2543.9511

High-Resolution-Mass Data 401

O O

O

3-40

C19H14O5322.0841

Appendix 7

402

O O

O

5-23

C17H10O5294.0528

High-Resolution-Mass Data 403

O O MeO

Appendix 7

404

O O HO

High-Resolution-Mass Data 405

TES OTs

TsO O

3-56

C30H34O7S2Si 598.1515

Appendix 7

406

TES OH

HO O

3-57

C16H22O3Si 290.1338

High-Resolution-Mass Data 407

TES O HO

O

3-35

C16H22O3Si 290.1338

Appendix 7

408

I O HO

O

3-34

C10H7IO3301.9440

High-Resolution-Mass Data 409

O TsO

O

3-61

C36H28O10S2684.1124

O H

H

OTs O

Appendix 7

410

O HO

O

5-28

C14H16O3232.1099

Appendix 7

412

O AcO

O

5-32

C16H18O4274.1205

High-Resolution-Mass Data 413

OAc AcO

O

5-35

C18H20O5316.1311

Appendix 7

414

OAc

O AcO

O

5-38

C18H20O6332.1260

High-Resolution-Mass Data 415

O OH HO

O

5-40

C14H16O4248.1049

Appendix 7

416