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Synthetic studies of azido inositols and inositol based glycans 2

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23 NUS National University... NMR Spectra of the Selected Compounds in Chapter 2 | 2°12... NMR Spectra of the Selected Compounds in Chapter 2 | 2°12... =1 NUS Appendix I: NMR Spectra of

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Se SERERRRE 6 BSS RARKRA EXPNO : 2

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23 NUS National University

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Trang 4

=1 NUS Appendix I: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

Trang 5

23 NUS National University

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NMR Spectra of the Selected Compounds in Chapter 2 | 2°12

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National University of Singapore

| 6.0E+08 [ 5.5E+08 [ 5.0E+08 [ 4.5E+08

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SINUS National University

F 2.20E+08 [ 2.10E+08 [ 2.00E+08 [ 1.90E+08 [ 1.80E+08 [ 1.70E+08 [ 1.60E+08 [ 1.50E+08 [ 1.40E+08 [ 1.30E+08 [ 1.20E+08

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NMR Spectra of the Selected Compounds in Chapter 2 | 2°12

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NMR Spectra of the Selected Compounds in Chapter 2 | 2°12

Trang 12

12

6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5

fl (ppm) 7.0

75

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ANUS Appendix 1: NMR Spectra of the Selected Compounds in Chapter 2

National University

of Singapore

2012

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NMR Spectra of the Selected Compounds in Chapter 2 | 2°12

a

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=1 NUS Appendix I: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

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=1 NUS Appendix I: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

National University

of Singapore

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NMR Spectra of the Selected Compounds in Chapter 2 | 2°12

OH 2-20

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NMR Spectra of the Selected Compounds in Chapter 2 | 2°12

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Trang 22

23 NUS National University

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=1 NUS Appendix 1: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

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Trang 24

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Trang 25

=1 NUS Appendix I: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

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23 NUS National University

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Trang 27

National University of Singapore

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Trang 28

=1 NUS Appendix I: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

Trang 29

=1 NUS Appendix I: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

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Trang 30

23 NUS National University

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Trang 31

23 NUS National University

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Trang 32

23 NUS National University

32

Trang 33

=1 NUS Appendix I: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

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Trang 34

23 NUS National University

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34

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BE

3 NUS National University

Appendix I: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

| “* Current Data Parameters *** NAME sp0604 EXPNO 1 PROCNO 1

| *** Acquisition Parameters “**

AQ_mod dqd

| AUNM au_zg BF1 :_ 800.1300000 MHz BF2 : 800.1300000 MHz BF3 :_ 900.1300000 MHz BYTORDA : 0

| CPDPRG

| CPDPRGB :

CPDPRGT : DATE_t 03:37:59

DATE_d Apr 06 2009

DBP07 : edit DBPNAMO : DBPNAM1 : DBPNAM2 : DBPNAM3 : DBPNAM4 : DBPNAMS : DBPNAM6 : DBPNAM7 :

DE : 6.0 usec DECBNUC : off DECIM 16 DECNUC off DECSTAT : DO DIGTYP 8

| “* Acquisition Parameters ***

| AQ_mod qsim AUNM au_zg

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*** Acquisition Parameters **

AQ mod : dqd AUNM j au_zg

BF1 : 500.1300000 MHz BF2 :_ 800.1300000 MHz BF3 : 800.1300000 MHz DATEt : — 175105 DATEd : Apr162009 INSTRUM : av500

NS ‡ 3

O1 : 3088.51 Hz

02 : 3088.51 Hz

03 : 3088.51 Hz PARMODE : 1D SOLVENT : CDCI3

ỷ R28 x b§P Qror ¥ Current Data Parameters

** Acquisition Parameters ***

AQ_mod : qsim AUNM : au_zg

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TY ME SỐ ae Oe Pe ee BE ee ae so * 46; 40° SB So SSR Ber IB an ae Oa A4

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=1 NUS Appendix I: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

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Trang 39

23 NUS National University

Trang 40

=1 NUS Appendix I: NMR Spectra of the Selected Compounds in Chapter 2 | 2012

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Trang 41

SINUS National University

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Trang 42

23 NUS National University

Trang 43

23 NUS National University

F 3.4E+08

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43

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