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Steel Heat Treatment - Metallurgy and Technologies 2nd ed - G. Totten (CRC_ 2007) Episode 11 pdf

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Intensive quenching requires appropriate quenching facilities and quenching media.. Figure 9.52 shows a quenching chamber for the intensive cooling of an automobile semiaxis using pressu

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and minimal distortion Furthermore, it has been demonstrated that the service life under cyclic loads may be increased by approximately one order of magnitude [54]

Intensive quenching requires appropriate quenching facilities and quenching media Quenching media include pressurized water streams, water containing various additives, and liquid nitrogen Figure 9.52 shows a quenching chamber for the intensive cooling of an automobile semiaxis using pressurized water flow

The water supply to the chamber and the charging and discharging of the axles are controlled by two sensors The first sensor (5 in Figure 9.52) analyzes the process of film boiling and nucleate boiling, and the second, 6, describes the transformation of austenite into martensite by the change of the ferromagnetic state of the material One method of intensive quenching has been used that achieves maximum compressive stresses at the surface when sensor 6 indicates a specific magnetic phase transformation In this case, sensor 5 is used to minimize the duration of film boiling by regulating the water flow velocity A second method has also been used, with sensor 5 indicating the beginning and completion of nucleate boiling, while sensor 6 controls the water pressure and determines the end of intensive quenching, so that no more than 30% martensite is formed

Intensive quenching methods offer many possibilities for the successful cooling of parts with optimized strength properties and improved service life However, a precondition for the use of this technology is the development of appropriate quenching equipment that enables precise control of the quenching performance Ref [4c] provides an overview of intensive quenching probes design

9.8 PROPERTY PREDICTION METHODS

There are increasing demands on the heat treater to achieve as-quenched properties while simultaneously reducing heat treatment costs To achieve these goals it is becoming increingly important that experimentally or mathematically based methods to predetermine the as-quenched strength and hardness properties be applied with sufficient accuracy Currently, a computer-based selection of steels and optimization of quenching conditions according to the desired service properties are generally possible Hardenability is one of the most important properties to be predicted because it determines as-quenched microstructure formation The ability to predict hardenability curves from chemical composition has already been described

in Chapt er 5, Secti on 5.4 How ever, these harden ability curves pro vide only lim ited informa-tion about the distribuinforma-tion of mechanical properties in the quenched part It is necessary to correlate steel chemical composition, cooling rates during quenching, metallurgical trans-formation behavior, and the final physical properties These correlations are often complex

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FIGURE 9.52 Quenching chamber for intensive quenching of semiaxes in a pressurized water flow: 1, semiaxis; 2, quenching chamber; 3, water flow; 4, mechanical drive for the semiaxis; 5, sensor for analyzing the process of film boiling and nucleate boiling; 6, sensor for analyzing the portion of formed structures; 7, 8, amplifiers

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and minimal distortion Furthermore, it has been demonstrated that the service life under cyclic loads may be increased by approximately one order of magnitude [54]

Intensive quenching requires appropriate quenching facilities and quenching media Quenching media include pressurized water streams, water containing various additives, and liquid nitrogen Figure 9.52 shows a quenching chamber for the intensive cooling of an automobile semiaxis using pressurized water flow

The water supply to the chamber and the charging and discharging of the axles are controlled by two sensors The first sensor (5 in Figure 9.52) analyzes the process of film boiling and nucleate boiling, and the second, 6, describes the transformation of austenite into martensite by the change of the ferromagnetic state of the material One method of intensive quenching has been used that achieves maximum compressive stresses at the surface when sensor 6 indicates a specific magnetic phase transformation In this case, sensor 5 is used to minimize the duration of film boiling by regulating the water flow velocity A second method has also been used, with sensor 5 indicating the beginning and completion of nucleate boiling, while sensor 6 controls the water pressure and determines the end of intensive quenching, so that no more than 30% martensite is formed

Intensive quenching methods offer many possibilities for the successful cooling of parts with optimized strength properties and improved service life However, a precondition for the use of this technology is the development of appropriate quenching equipment that enables precise control of the quenching performance Ref [4c] provides an overview of intensive quenching probes design

9.8 PROPERTY PREDICTION METHODS

There are increasing demands on the heat treater to achieve as-quenched properties while simultaneously reducing heat treatment costs To achieve these goals it is becoming increingly important that experimentally or mathematically based methods to predetermine the as-quenched strength and hardness properties be applied with sufficient accuracy Currently, a computer-based selection of steels and optimization of quenching conditions according to the desired service properties are generally possible Hardenability is one of the most important properties to be predicted because it determines as-quenched microstructure formation The ability to predict hardenability curves from chemical composition has already been described

in Chapt er 5, Secti on 5.4 How ever, these harden ability curves pro vide only lim ited informa-tion about the distribuinforma-tion of mechanical properties in the quenched part It is necessary to correlate steel chemical composition, cooling rates during quenching, metallurgical trans-formation behavior, and the final physical properties These correlations are often complex

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4

FIGURE 9.52 Quenching chamber for intensive quenching of semiaxes in a pressurized water flow: 1, semiaxis; 2, quenching chamber; 3, water flow; 4, mechanical drive for the semiaxis; 5, sensor for analyzing the process of film boiling and nucleate boiling; 6, sensor for analyzing the portion of formed structures; 7, 8, amplifiers

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10 Distortion of Heat-Treated Components

Michiharu Narazaki and George E Totten CONTENTS

10.1 Introduction 614

10.2 Basic Distortion Mechanisms 609

10.2.1 Relief of Residual Stresses 609

10.2.2 Material Movement Due to Temperature Gradients during Heating and Cooling 610

10.2.3 Volume Changes during Phase Transformations 610

10.3 Residual Stresses 612

10.3.1 Residual Stress in Components 612

10.3.2 Residual Stresses Prior to Heat Treatment 612

10.3.3 Heat Treatment after Work-Hardening Process 612

10.4 Distortion during Manufacturing 613

10.4.1 Manufacturing and Design Factors Prior to Heat Treatment That Affect Distortion 613

10.4.1.1 Material Properties 614

10.4.1.2 Homogeneity of Material 614

10.4.1.3 Distribution of Residual Stress System 614

10.4.1.4 Part Geometry 614

10.4.2 Distortion during Component Heating 615

10.4.2.1 Shape Change Due to Relief of Residual Stress 615

10.4.2.2 Shape Change Due to Thermal Stresses 615

10.4.2.3 Volume Change Due to Phase Change on Heating 615

10.4.3 Distortion during High-Temperature Processing 616

10.4.3.1 Volume Expansion during Case Diffusion 616

10.4.3.2 Distortion Caused by Metal Creep 616

10.4.4 Distortion during Quenching Process 617

10.4.4.1 Effect of Cooling Characteristics on Residual Stress and Distortion from Quenching 617

10.4.4.2 Effect of Surface Condition of Components 624

10.4.4.3 Minimizing Quench Distortion 625

10.4.4.4 Quench Uniformity 629

10.4.4.5 Quenching Methods 630

10.5 Distortion during Post Quench Processing 631

10.5.1 Straightening 631

10.5.2 Tempering 631

10.5.3 Stabilization with Tempering and Subzero Treatment 632

10.5.4 Metal Removal after Heat Treatment 633

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Spray (open) lateral Spray (submerged) lateral

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FIGURE 10.11 Effect of agitation methods on residual stress after water quenching of JIS S45C steel rod (20-mm diameter by 60 mm long) Quenchant was 308C city water Agitation methods were still, 0.3 m/s upward flow, 0.7 m/s upward flow, and lateral submerge in immersion quenching, and lateral open spray quenching in air (a) Axial stress on surface, (b) tangential stress on surface (From

M Narazaki, G.E Totten, and G.M Webster, in Handbook of Residual Stress and Deformation of Steel, G.E Totten, M.A.H Howes, and T Inoue, Eds., ASM International, Materials Park, OH, 2002,

pp 248–295.)

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