Phổ gc sự o-metil hóa một số phenol sử dụng Carbonat Dimetil

Phổ gc sự o-metil hóa một số phenol sử dụng Carbonat Dimetil

PHO GC GC-MS

Analysis Date & Time: 5/17/2005 1:01:41 AM

Data Name : DAHUU CO\C.LAN PHUONG\Phenoliphenol.ged

Method Name : DAHUU CO\C.LAN PHUONG |Phenolianisol.gem Intensity

Analysis Date & Time: 5/16/2005 11:00:22 PM

Sample Name : EUGENOL CHUAN

Sample Type : Unknown

Injection Volume :

ISTD Amount

Data Name : DAHUU CO\C.LAN PHUONG\Eugenol\EUGENOL CHUAN ged

Method Name : DAHUU CO\C.LAN PHUONG\Eugenol\EUGENOL.gem

Analysis Date & Time

¡1

: SOECHUAN : ISOECHUAN : Unknown

: DAHUU CO\C.LAN PHUONG\EugenolISOEUGENOLASOECHUAN.gcd

Analysis Date & Time : 10/10/2005 3:37:44 PM

Data Name : DAHUU CO\C.LAN PHUONG\THYMOL\THYMOL gcd

Method Name : DAHUU CO\C.LAN PHUONG\THYMOLITHYMOL.s gem

Analysis Date & Time

tJ

: CARVACROL : CARVACROL : Unknown

: DAHUU CO\C.LAN PHUONG\Eugenol\CRA VACROL\CARVACROL.ged : DAHUU COAC.LAN PHUONGIEugenoEUGENOL.gem

Analysis Date & Time

: DAHUU CO\C.LAN PHUONG\O-CRECROL\O-CRECROL ged : DAHUU CO\C.LAN PHUONG\THYMOL\THYMOL.gem

Pile ` 2: \HPCHEM\ 1 \DATA\ LPHUONGS oD

Operator > NA ~ LAN PHƯƠNG

Acquired Instrument : : 5 May o5 3:35 pm using AcqMethod ACEBEN

TPE eT ery Tree

† OPE ATE Ey LTT ri Trị an Te ĩ 7 T rere err tàng —> “hận 350 400 450 600 5.50 6.00 650 7.00 750 800 851 900 9.50 10.00 10.50 141.00 11.50 1200 4

TMPLIBRP TXT

Information from Data File:

Integration Params: EVENTS.E

Minimum Quality Minimum Quality

Re£# CAS#

T1

2

3.96 52.16 C:\DATABASE\wiley138.1

Benzene, methoxy- 4.59 47.82 C:\DATABASE\wileyi38.1

File : C:\HPCHEM\1\DATA\LPHUONG? .D

Operator : NA ~ LAN PHUONG

Acquired : 5 May os 3:12 pm using AcqMethod ACEBEN

TMPLIBRP TAT

information from Data File:

File 2 C: \HPCHEM\ L\DATA\LPHUONG2 D

Operator : HA - LAN PHUONG

Acquired : =5 May 05 3:12 pm using AeqMethod ACEBEN

Sample Name: El

Mise Info :

Vial Number: 1

Integration Params: EVENTS.E

Time—> 4.60 6.00 550 600 650 7,00 750 800 8,

3 xrịc:-r?y'†-T"rr

900 950 1 LTO 920 1950 1100 1150 1200 1250 1200 13:TTT TTT TUTE TTI IIT TTT

TMPLIBRE TXT

Information from Data File;

Pile h C:\HPCHEM\1\DATA\P2.D

Operator : NA - LAN PHUONG

Acquired : 23 Oct 05 2:34 pm using AcqMethod ACEBEN

Misc Info

Vial Number: 1

C; \DATABASE\ UNIVER L

Integration Params: EVENTS

23 Aug 65 3:00 pm using AcqMethod ACEBEN - GC/MS Ins

Sample Name: THYMOL - T2

TMPLIBRP.TXT

Information from Data File:

File : C:\HPCHEM\1\DATA\LPHUONG6 D

Operator : NA - LAN PHUONG

Acquired + 29 Aug 05 3:00 pm using AcqMethod ACEBEN

Sample Name: THYMOL - T2

Misc Info

Vial Number: 1

C:\DATABASE\UNIVER.L

Unknown Spectrum: Apex

Integration Params: EVENTS.E

Library Searched : C: \DATABASE\WILEY138 L

fui» 36 40 50 60 70 80 $0 160 140 120 130 140 150 160 170 180 190 200 210 220 235 240 250 260 270 280 290 300

#123687: Phonol, 24neth-Š-{1-methyiethyfr 1%

Library Searched : C:\DATABASE\WILEY138.L

Bs \DATA\ DHKHTN\HPHUONG\TROSOS D5

If leading or trailing edge < 100 prefer < Baseline drop else tangent >

Method DB: \METHOD\CARVACROL.M

Title

Signal Tic

peak R&.T first max last PK peak corr Corr % of

# min scan scan scan TY height area $ max, total

1 5.850 916 929 1016 BY 7778505 197560408 43.41% 30.2728

2 6.316 1016 1044 1174 PV 2 7800619 455058573 100.00% 69.728%

Sum of corrected areas: 652628981 CARVACROL.M W ed May 10 15:26:30 2006

“* Search Report Page 1 of 4 Unknown: Average of 5.838 to 5.862 min THOS09.D

Compound in Library Factor = 229

CTIHIGO: MF: 911; RMF: 935; Prob 36.9%; CAS: 1076-56-8; Lib: mainiib; ID: 87664

Unknown: Average of 6.288 to'6.312 min.: THO509.D

Compound in Ubrary Factor = -107

Hit 1: Phenol, 2-methyt-5-(1-methylethyi)-

C10H140; MF: 926; RMF: 926; Prob 36.1%; CAS: 499-75-2; Lib: mainlib; ID: 79160

File : C:\HPCHEM\L\DATA\PS .p

Operator : NÀ - LAN PHUONG

Acquired Instrument ; : 8 Nov os 1:52 pm using AcqMethod ACEBEN

TMPLIBRP TXT

Information from Data File:

Acquired : 8 Nov 05 1:52 pm using AcqMethod ACEBEN

Sample Name: O-CRESOI

Misc Info :

Vial Number: 1

Unknown Spectrum: Apex

Integration Params: EVENTS.E