INTRODUCTION
Purpose
Using the extraction from some organic material for making organic lipstick, replacing toxic pigment, toxic flavour in industrial lipstick by pigment, essential oil from extractions of fruits.
Requirement
+ Extraction of yellow pigment from tumeric
Extraction of strong pink pigment from red dragon fruit
Extraction of red pigment from gac fruit
Extraction of essential oil from pomelo
Trial on mixing organic material and extractions for making lipstick.
OVERVIEW
Basic information about researching material
2.1.1.1 General introduction of red dragon fruit
The native plant species is originally found in Mexico, Central America, and South America, but it is now also cultivated in Southeast Asian countries, including Vietnam, Malaysia, Thailand, the Philippines, and Indonesia, particularly in the western part of Java Island, as well as in southern China and Taiwan.
Red dragon fruit is rich in lycopene and betacyanin, powerful natural antioxidants that combat cancer and heart disease while helping to lower blood pressure This vibrant fruit not only boasts a striking dark red exterior but also features a crimson red flesh that is more nutritious than conventional white dragon fruit With higher levels of Vitamin C and protein, red dragon fruit stands out as a beautiful and healthful choice.
A, Glucid, Lipit, red dragon fruit brings very high nutritional value Red flesh dragon fruit is a new, strange, delicious, nutritious product, a "made in Vietnam" product Currently, the United States has issued an export code for red flesh dragon fruit and with advanced production techniques, red flesh dragon fruit is a product that strictly complies with food safety, pesticide residue as well as some other requirements has been trusted by export partners from the US, Japan, and Europe
The characteristic of this dragon fruit is that it looks very small but weighs (~ 1kg /
Red flesh dragon fruit is a unique and high-end delicacy, known for its bright red flesh, crispy texture, and sweet flavor, packed with vitamins and minerals Although it is priced higher than white flesh dragon fruit, its exceptional taste appeals to both domestic and international consumers Recent scientific research highlights the presence of Lycopene in red fruits, including Gac and Carot, which is recognized for its anti-cancer and anti-aging properties, making red flesh dragon fruit a nutritious choice.
In addition, according to Mr Phung Nhat Phong, owner of the pilot production and processing facility and the first farmer to pilot red-flesh dragon fruits in Tay
Ninh stated that the fruit leaves a beautiful red color on natural lips and has a high natural color content, making it suitable for food coloring and cosmetics like lipstick and makeup powder Additionally, it has potential cancer treatment properties and can be used to produce health-beneficial wine for the elderly and women, as acknowledged by the Institute Pasteur Beyond its typical uses, dragon fruit juice can be enjoyed as a refreshing drink, and the process of extracting juice from the seeds adds fiber, which aids digestion and promotes laxative effects.
2.1.2.1 General introduction of gac fruit
Distribution: This is a type of perennial melon grown throughout Southeast Asian countries and Northeastern Australia
Gấc, known for its vibrant orange-reddish hue, is rich in beta-carotene and lycopene Research conducted by TS Phan Quoc Kinh and his team as part of the national key research program on nutrients (64D03) in 1988-1989 focused on Gấc fruit products as nutritional supplements Additionally, since 1941, the Medicine Department of Hanoi University of Pharmacy has identified that the red membrane surrounding Gấc seeds is a significant source of beta-carotene and herbal oils.
Researchers from Hanoi Medical University and Hanoi University of Pharmacy have found that the red film oil surrounding Gac seeds has effects similar to vitamin A and can promote weight gain in both animals and humans In 1951, Prof Nguyen Van Dan introduced this medicinal herb in Germany, discovering that it not only contains beta-carotene but also lycopene, a potent anti-aging compound Over the past 20-30 years, Vietnam's pharmaceutical industry has developed various products featuring Gac membrane oil, which are used as tonics and for treating malnutrition in children, as well as certain eye diseases Additionally, doctors in Vietnam have utilized Gac membrane oil for the prevention and treatment of various cancers.
To prepare the extraction, both the seeds and the Gac membrane must be thoroughly dried until the seeds can no longer be held in hand Once dried, a sharp knife is used to remove the red film This membrane is utilized to produce Gac oil, which is rich in essential nutrients such as beta-carotene, lycopene, and alpha-tocopherol Upon entering the body, beta-carotene is converted into vitamin A, providing numerous health benefits.
Gac fruit is a rich source of beta-carotene, containing twice the amount found in carrots, and its oil is known to prevent vitamin deficiency, boost immunity, and provide anti-aging and skin care benefits Additionally, Gac is exceptionally high in lycopene, with levels 70 times greater than those in tomatoes Epidemiological studies in the U.S indicate that higher consumption of lycopene-rich fruits correlates with a lower incidence of digestive tract cancers, reducing cancer mortality rates by up to 50% A 12-year study revealed that individuals consuming ketchup at least twice a week had a 35% lower risk of prostate cancer, with even more significant effects observed in advanced cancer cases Furthermore, lycopene is beneficial for treating hepatitis, cirrhosis, and conditions like high blood pressure and dry eyes.
Distribution: This is plant native to the Indian subcontinent and Southeast Asia, that requires temperatures between 20 and 30 °C (68 and 86 °F) and a considerable amount of annual rainfall to thrive
Turmeric root is composed of 4-6% light yellow essential oils, with fresh turmeric containing 2.24% aromatic compounds Its chemical makeup includes 25% terpenic carbons, zingiberene, and 65% sesquiterpenic ketones such as turmerone and ar-turmerone Additionally, turmeric contains curcuminoids, primarily curcumin, which ranges from 0.3% to 1.5%, along with desmethoxycurcumin Curcumin is characterized as a reddish-purple crystal that is insoluble in water but soluble in both acidic and alkaline environments.
Turmeric is known for its bitter and pungent taste, along with a warm aroma, and is effective in breaking stasis and detoxifying the body Curcumin, a key component of turmeric, promotes skin health by enhancing bile secretion from liver cells and reducing blood cholesterol levels Additionally, turmeric essential oil exhibits fungicidal properties on the skin, while curcumin also demonstrates antibacterial effects.
The pomelo is believed to have originated in the Malesian region and has been cultivated in Southeast Asia, particularly in countries like Indonesia, Thailand, Malaysia, and Vietnam Various species of pomelo have emerged through selection, propagation, and natural hybridization.
Pomelo flowers positively impact the respiratory system, with their fragrance promoting relaxation, stress reduction, and enhanced alertness The essential oil derived from pomelo flowers contains key components such as Nerolidol (30.9-40.04%), Farnesol (14.3-23.47%), and Linalool (9.23-23.76%).
Pomelo flowers are small and white, with occasionally resinous stalks While pomelo trees are generally smaller and greener than the fruit itself, they can reach heights exceeding 1 meter above the average pomelo tree Historically, pomelo has been a significant fruit in many rural areas of Vietnam.
Pomelos are increasingly favored for their delicious fruit and early production, leading many farmers to transition to pomelo cultivation The process of transplant breeding has made it harder to distinguish the original characteristics of the fruit, with many consumers focusing primarily on its appearance in the market Pomelo trees typically reach heights of 3–4 meters, featuring pale yellow bark that may exude sap from cracks They have long, pointed spines on their branches and gill-shaped, ovoid leaves measuring 11–12 cm in length and 4.5-5.5 cm in width, characterized by large winged stalks The flowers are double, red, and fragrant, growing in clusters of 6-10 The fruit itself is large and globose, with thick skin that varies in color depending on the variety.
2.1.5 Organic materials compound lipstick base [8]
Cosmetic trendy nowaday
In today's cosmetic trend, many users prioritize color, effectiveness, and price over the ingredients in lipsticks However, they may be unaware of the toxic chemicals and heavy metals present in industrial products that can directly impact their health One such harmful ingredient commonly found in lipsticks is propylparaben.
These are ingredients that can irritate the skin, especially for people with a history of allergies Some studies also show that propylparaben disrupts the endocrine system b Lead
Many cosmetic brands incorporate lead into their lipstick formulations, leading to potential health risks for women who use these products regularly The continuous use of lead-containing lipsticks can result in the accumulation of lead in the bloodstream, which is linked to serious health issues such as brain damage, neurological disorders, infertility, hormonal imbalances, and an increased risk of cancer.
Mineral oil, commonly found in color cosmetics, has a molecular structure that prevents it from being absorbed by the skin Instead, it clings to the skin's surface, leading to blocked pores and the potential for acne.
This is a fake form of vitamin A and is considered dangerous for pregnant women e Aluminum and manganese
Lipstick has also been found to contain a certain amount of aluminum and manganese, which can cause Alzheimer's disease and problems with brain function f Parafin wax:
This specialty is frequently found in lipsticks, foundations, and moisturizers While it is not classified as high-risk, it can still trigger reactions like burning, itching, blistering, and enlarged pores.
Triclosan, commonly utilized in the food and lipstick industries, disrupts calcium ion flow in the body, affecting communication between the brain and muscle tissue Research indicates that just 20 minutes of exposure to triclosan can lead to a 25% reduction in heart function.
Ph.D Sean Palfrey, Medical Director of the Lead Poisoning Prevention Program in Boston, emphasizes that even minimal lead absorption can negatively impact IQ and cognitive abilities, particularly in women who frequently use lipstick, leading to behavioral disorders and reduced learning capacity Additionally, fruity scents in products are primarily due to esters, which are key chemical compounds that define the characteristic odors of various fruits While esters can be naturally sourced or synthesized, the food, cosmetic, beverage, and confection industries predominantly rely on chemical synthesis due to cost considerations These esters, derived from mono-alcohols and mono-acids, are typically volatile liquids that emit pleasant fruity aromas, contributing significantly to product appeal.
12 have characteristic odors of fruits, essential oils and natural aromas But the chemicals synthesis aroma is not good for health
A brief examination reveals harmful ingredients in many lip products, which can pose health risks to consumers Despite the availability of various lip balms and natural lipsticks, most still rely on artificial colorants and chemical compositions Therefore, it is essential to find ways to satisfy women's growing beauty demands while minimizing the negative effects associated with lipstick use.
The thesis "Researching Using Some Organic Extraction to Compound Lipstick" aims to explore methods and dosages for creating cosmetics from natural ingredients It evaluates the working time and economic efficiency of these products compared to traditional cosmetics, as well as consumer opinions on their effectiveness This approach seeks to reduce the use of chemicals in the cosmetic industry and minimize chemical exposure for users By leveraging the benefits of natural preparations, the research promotes health safety and enhances beauty care, while also being economically viable and environmentally friendly.
The product mirrors the shape, color, quality, usage, and preservation of similar items available in the market Users can safely apply it in generous amounts without health concerns Notably, lipstick is particularly prone to ingestion, but with a formulation free from harmful ingredients, users can feel confident and at ease while using it.
Application of researching materials
This is an important part that determines the unique characteristics of each lipstick
To effectively blend with the lipstick base, pigments should be in gel or dry powder form The primary ingredients for lip color are derived from natural sources, such as fruits and other organic products The key color components analyzed include:
Lycopene and betacarotene from Gac fruit (red pigment)
Betacyanin from red dragon fruit (strong pink pigment)
Cucurminoid from tumeric (yellow pigment)
We select these ingredients for their safety and historical use as spices, supported by extensive research on their beneficial compounds For instance, beta carotene in Gac enhances eye health, reduces myopia, and supports heart function, while curcuminoids in turmeric effectively aid in managing stomach ailments.
Flavor refers to ingredients or combinations used to impart taste in cosmetics and personal care products, primarily in items like lipsticks and oral hygiene products that may be ingested Many fragrance components also serve as flavor compounds The U.S Food and Drug Administration defines "flavor" on product labels as any natural or synthetic substance used solely for taste enhancement In Europe, this is labeled as Aroma Flavors enhance or mask specific tastes in a variety of cosmetics and personal care items.
Certain chemical aromas can lead to skin irritation, rashes, and accelerated aging, and their prolonged use may impact the central nervous system or disrupt endocrine function This research aims to investigate the use of essential oils derived from pomelo flowers as a natural alternative to the synthetic essential oils typically found in lipsticks, thereby minimizing health risks for consumers.
MATERIALS AND METHODS
Materials, contents and method
The materials were provided by Faculty of Enviroment in Vietnam National University of Agriculture: red dragon fruit, gac fruit, turmeric and Pomelo
The experiment was conducted with three main subjects: red dragon fruit, gac and tumeric The ingredients should be:
- Lipstick base: Beewax; Soybean wax; Coconut oil; Olive oil
- Lipstick pigment: Red dragon fruit; Tumeric; Gac
- Place: Inviromental faculty in Vietnam National University of Agriculture
Machine: System of Sohlets experiment, thermostat tank, machine Vacuum, magnetic stirrer, vortex, system of steam attractive distillation
Chemical: Ancohol, Na 2 SO 4 , n-hexane, ethyl acetate/ ethanol solvent, food alcohol…
There are also tools such as glass chopsticks, glass cups, lamp flares, solution straws, filter cotton
Methods
3.2.1 Experiments of extraction from fruit and flower
3.2.1.1 Extracting pink pigment from red dragon fruit
This experiment utilized an alcohol method to extract a vibrant pink pigment from red dragon fruit, which is considered safe for human health and is currently used in cosmetics The progress of the experiment was summarized as follows:
Step 1: Add V (milliliter) of food alcohol to the container which have m (gram) of dragon fruit (the ratio of them is 1:1), cut into pomegranate seeds
Step 2: Soak the mixture on to the thermostat tank at 40°C (the thermostat tank is tightly closed ensure that the extraction of betacyanin is carried out in the dark) Proceed to soak and extract the clear mixture about n hours [9]
Step 4: The mixture is then filtered to remove residue by vacuum cleaner
Step 5: The obtained extract is further anhydroused with 15g Na 2 SO 4 on magnetic stirrer for 30 minutes Let the mixture settle for about 5 minutes and filter by machine Vacuum [10] Part of the filtered solution brings evaporation in low pressure obtained betacyanin pigment
Experiments were performed using four different formulas at a consistent solid-to-solvent ratio of 1g to 1ml and a temperature of 40°C to assess the quantity of pigment produced.
Table 3.1 Experimental arrangement of color extraction from red dragon fruit
3.2.1.2 Extracting yellow pigment from tumeric
This experiment was carried with Soxhlet method to extacting yeallow pigment from Tumeric And the progress was summary as:
Step 1: Preparing material: Clean up solids such as soil, sand, dust Slice, expose or dry at 40 – 50 0 C until the mass does not change After letting it cool in a cool place, put in the blender into powder This is used for an extractor
Step 2: Extract curcuminoid from tumeric power by Sohlet method:
After cleaning, slicing, and steam-distilling the sample to eliminate essential oils, it was dried and powdered The powdered sample was then subjected to Soxhlet extraction using n-hexane to remove hydrocarbons and fats The resulting residue was dried and further extracted with a mixture of ethyl acetate and ethanol at 80°C for varying durations, yielding crude curcuminoids.
Table 3.2 Experimental arrangement of color extraction from tumeric
Figure 3.1 Tumeric powder Figure 3.2 Tumeric powder stored in box
Experiments were conducted with 5 flomulas with different time (all of experiments were carried with the raw material is 1 kg and temperature is 80⁰C) to evaluate the amount pigment obtained
3.2.1.3 Extracting red pigment from gac fruit
This experiment was carried with using Sohlet method to extacting red pigment from Gac fruit and it is suitable for using in cosmetic And the progress was summary as:
Step 1: Preparing material: Split the core from fruit and dry at 45°C in 19h (remove the black seed before drying) until the mass does not change After letting it cool in a cool place, put in the blender into powder
Figure 3.5 Drying gac Figure 3.6 Dried gac powder
Step 2: Extracting pigment by using Sohlet method
The Soxhlet method is a continuous extraction process utilizing a specialized kit In this method, 500 grams of gac powder is wrapped in filter paper and placed in an extraction tube The solvent, heated to 80°C, vaporizes and travels through a steam pipe to the condenser in the extraction tube Initially, n-hexane is used to extract hydrocarbons and fats, after which the residue is dried and further extracted with a mixture of ethyl acetate and ethanol The solvent circulates back to the flask until the extraction is complete To determine if the extraction is finished, the condenser tube is removed, and a few drops of the solution are pipetted from the sample container for analysis.
The extraction process is complete when the solvent has fully evaporated, leaving no residue If traces remain, further extraction is necessary Conducted under standard conditions, the time factor significantly influences the test results, prompting the experiment to be repeated five times with varying time intervals.
Table 3.3 Experimental arrangement of color extraction from Gac
Formula 1 Formula 2 Formula 3 Formula 4 Formula 5
Figure 3.7 Pigment obtained from Gac 3.2.1.4 Extracting essential oil from pomelo flower
This experiment was carried with using steam attractive distillation method to extacting aroma from pomelo flower And the progress was summary as:
(Source: Internet) Step 1: Weigh 100 grams of flowers and then puree
Step 2: Soak in 250ml of 10% NaCl solution for 3 hours
Step 3: Then attract through steam distillation method in 90 minutes to collect crude white essential oil [15]
Step 4: The crude oil is processed, extracted and anhydrous with diethyl ether, NaCl, and Na 2 SO 4 The ether solution is evaporated to collect essential oil [13]
High temperatures can decompose essential oils, so superheated steam above 100°C should only be used in the final stage of distillation, after all volatile components have been absorbed In our experiment, we tested five formulas at different temperatures to determine the optimal temperature for extracting essential oil from pomelo flowers.
Table 3.4 Experimental arrangement of essential oil extraction from pomelo flower
3.2.2 Experiments combining organic material and extractions making lipstick 3.2.2.1 Making lipstick base by organic material
This experiment utilized a diffusive heating method to formulate a lipstick base using beeswax, soybean wax, coconut oil, and olive oil In these formulations, beeswax and soybean wax contribute to the hardness of the lipstick, as they share the same melting point Meanwhile, coconut oil and olive oil enhance the softness and smoothness of the lipstick due to their identical melting point The amounts of beeswax and soybean wax were fixed at 1g each per formulation.
Step1: Weight beewax and soybean wax
Step 2: Heat the mixture in 80°C and diffusive by glass chopstick
Step 3: Add coconut oil and olive oil into the mixture
Experiments were conducted using five different formulas, each containing varying amounts of oil, while maintaining a consistent ratio of 1g of beeswax and soybean wax at a temperature of 80°C The objective was to evaluate the texture, specifically the smoothness and hardness or softness, of the lipstick base.
Table 3.5 Experiment evaluate the smooth and hard or soft of lipstick base
Formula 1 Formula 2 Formula 3 Formula 4 Formula 5
Olive oil and coconut oil
Figure 3.9 Weight beewax and soybean wax
Figure 3.10 Mixture after adding oil
3.2.2.2 Finding out the best formulation
Proper lipstick storage is crucial, as it should be kept below 45 degrees in a well-ventilated environment To assess the melting properties of two formulations that have shown the best results in terms of smoothness and hardness, tests will be conducted at various temperatures over a duration of 5 hours.
Table 3.6 Experiment evaluate the storage condition of lipstick base
3.2.2.3 Application of pigment extractions on coloring lipstick
Once the optimal lipstick base formulation is established, the next crucial step is to add color to the lipstick This involves utilizing the pigments extracted from previous experiments and thoroughly dispersing them into the melted lipstick base mixture.
In these experiments, we utilize glass chopsticks or a magnetic stirrer to blend pigment with the lipstick base The evaluation criteria, including pigment coverage, pigmentation, smoothness, and stickiness, are assessed with sensitivity.
RESULTS AND DISCUSSION
Results
4.1.1.1 Extraction result of pigment from red dragon
To extract pigment from red dragon fruit, we focus on the fruit's flesh rather than the peel, as the peel contains oily substances that do not dissolve well in common lipstick bases like coconut oil, olive oil, beeswax, and soybean wax This limitation prevents effective mixing of ingredients for lipstick production, making the flesh the preferred choice for pigment extraction.
The vibrant color of dragon fruit primarily comes from its pigment rather than its fiber, necessitating the removal of fiber through filtration during the experiment Once the pigment is extracted as a powder, it can be dissolved in oily lipstick, offering a natural alternative to the synthetic mineral pigments currently used in commercial lipsticks.
In this extraction experiment, time is the most important factor So we carried out each experiment with 4 fomulas with diferent time Then, we have the results as in table 4.1
Figure 4.1 Concerntrating mixture Figure 4.2 Concerntrated mixture
Table 4.1 Extraction result of pigment from red dragon fruit
The experiments conducted revealed the optimal conditions for betacyanin extraction, resulting in the highest betacyanin content of 1.403 grams The ideal parameters identified include an extraction time of 4 hours, an extraction temperature of 40 °C, and a solids/solvent ratio of 1 gram per 1 milliliter.
Figure 4.3 Pigment obtained from red dragon fruit 4.1.1.2 Extraction result of pigment from tumeric
Curcuminoids extracted from turmeric possess a vibrant yellow color and are fully soluble in oil, making pure extraction unnecessary This allows curcuminoids to effectively serve as a complete replacement in various applications.
Curcumin, the yellow pigment derived from turmeric, is recognized for its beneficial effects on young skin, promoting bile secretion from liver cells and aiding in cholesterol breakdown Additionally, turmeric essential oil exhibits fungicidal properties, while curcumin also demonstrates antibacterial effects, making it valuable in various industrial applications.
In this extraction experiment, time is the most important factor So we carried out each experiments 5 fomulars with diferent time Then, we have the results as in talbe 4.2
Table 4.2 Extraction result of pigment from tumeric
The experiments revealed key factors affecting the performance of curcumin extraction, identifying optimal conditions for maximum curcumin content The ideal extraction parameters include a duration of 10 hours, a temperature of 80°C, and a raw material quantity of 1 kg, resulting in a curcumin yield of 104 grams.
Formula 1 Formula 2 Formula 3 Formula 4 Formula 5
Figure 4.4 Color pigment obtained from tumeric 4.1.1.3 Extraction result of pigment from gac fruit
The Sohlet method is an efficient extraction technique that minimizes solvent usage, requiring only a few solvents for sample extraction Unlike other methods, it eliminates the need for filtering and refilling solvents By simply connecting to electricity to activate the circulating water, the machine autonomously carries out the extraction process.
The primary benefit of this method is its ability to effectively extract the desired compound However, a significant drawback is the necessity of conducting multiple timelines, as the extraction time plays a crucial role in influencing the results.
Beta-carotene and lycopene share the same red color, making it unnecessary to extract each separately Both compounds are soluble in lipstick formulations This experiment involved five formulas tested at different time intervals, with results presented in Table 4.3.
Figure 4.5 Color pigment obtained from gac fruit
Table 4.3 Extraction result of pigment from Gac
The experiments revealed significant effects on the performance of lycopene and beta-carotene extraction rates The optimal conditions for achieving the highest content of these compounds were identified as an extraction time of 10 hours and a specific extraction temperature.
80 0 C; Mount of raw material is 500gr; Mount of lycopene and betacarotene is 112gr
4.1.1.4 Extraction result of pomelo flowers
The steam attractive distillation method closely resembles direct water storage in terms of raw materials This technique utilizes its own steam source, allowing the steam to interact with the material to extract essential oils, which then undergo a transformation in a cooling and removable section Key advantages of this method include its straightforward implementation, ease of equipment creation, operational simplicity, and cost-effectiveness.
Various heat sources, including electricity, dock, and coal, can be utilized for distillation processes This method conserves water compared to direct distillation and produces clear water However, high temperatures can decompose essential oils, so superheated steam (above 100°C) should only be applied during the final stage of distillation, after all volatile components have been extracted In our experiment, we tested five formulas, each at a different temperature, and the results are presented in Table 4.4.
Table 4.4 Extraction result of pomelo flower
Formula 1 Fomula 2 Formula 3 Formula 4 Formula 5 Mixture of material (ml) 350 350 350 350 350
The optimal temperature for extracting progress is 100°C, yielding a total of 61.2 ml of essential oil after a 90-minute extraction period with 350 ml of material.
4.1.2 Trial combining material and extrction making lipstick results
4.1.2.1 Result of using organic materials making lipstick base
In these formulations, all of evaluation criteria is base on assessed sensitively And the results is appeared in below table:
Figure 4.6 Essential oil obtained from pomelo flower
Table 4.5 Evaluation result of character of lipstick base
Formula 1 Fomula 2 Formula 3 Formula 4 Formula 5 Olive oil and coconut oil
From the result in this table, the formulas which show the better result are formula
4.1.2.2 Result of finding out the best formualation of lipstick base
Proper lipstick storage requires temperatures below 45 degrees in a well-ventilated environment Formulations 4 and 5, made from organic materials, exhibit the ideal characteristics of industrial lipsticks These formulations will be tested to assess their melting properties at various temperatures over a duration of 5 hours.
Table 4.6 Evaluation result of storage condition of fomualtion 4 and 5
20 0 C 25 0 C 30 0 C 35 0 C 40 0 C 45 0 C 50 0 C 55 0 C 60 0 C Formula 4 Nomarl Nomarl Nomarl Nomarl Nomarl Oily Oily Melt Melt Formula 5 Nomarl Nomarl Nomarl Nomarl Nomarl Nomarl Oily Oily Melt
From the above results, the best formulation in these experiment is formula 4 and the best formulation of lipstick base contains 1g of bee wax, 1g of soybean wax and
2,5 ml of coconut oil and olive oil.
4.1.2.3 Result of application of pigment extractions on coloring lipstick
The evaluation criteria for these formulations, including pigment coverage, pigmentation, smoothness, and stickiness, are based on sensitive assessments, with the results presented in the tables below.
Table 4.7 Coloring lipstick results with yellow pigment (cucurminoid)
Table 4.8 Coloring lipstick results with strong pink pigment (betacyanin)
Table 4.9 Coloring lipstick results with red pigment (lycopene and beta carotene)
Because with each a mount of essential oil will make different fragrance concentrationins And the flavoring progress results will be assessed sensitively in table 4.10:
Table 4.10 Flavouring lipstick results with essential oil from pomelo flower
Result No flavor Perfumed Very Perfumed Too perfumed
From the results of these 3 experiments, the amount of pomelo essential oils which is suitable is 0.2% because it does not make people uncomfortable to smell.
Discussion
The product replicates the design and appearance of market lipsticks while maintaining standard usage and preservation methods Utilizing an optimal formula, it combines 2g of wax, 2.5ml of oil, approximately 2-2.5g of pigments, and 0.2% flavoring, adjusted according to the desired lipstick color This allows for the creation of high-quality lipsticks that mirror the characteristics of industrial options available today, albeit with reduced beeswax content.
Lipsticks come in various functional types, including traditional lipstick, lip balm, and creamy liquid options, offering a wide range of colors such as magenta, wine red, light pink, dark pink, orange red, and purple rose Additionally, they are available in diverse designs, including stick, liquid, roller, and jar formats.
This formula offers numerous advantages, including an aesthetically pleasing design and a variety of colors It ensures guaranteed quality with smooth, bright, and durable colors at a more affordable price, making it accessible to a wide range of users The raw materials are simple, contributing to high economic efficiency Its usage and preservation are comparable to other market products, with a shelf life of 6 months to 1 year without toxic chemical preservatives, as beeswax serves as an organic preservative, ensuring safety for user health.
This product significantly reduces the use of chemicals in the cosmetic industry and minimizes chemical exposure for consumers By utilizing natural preparations, it ensures safety for health while providing numerous benefits for beauty care Embracing nature's resources promotes both economic efficiency and environmental sustainability.
The product mirrors the shape, color, quality, usage, and preservation of similar items available in the market Users can safely apply it in generous amounts without health concerns Notably, lipstick is particularly prone to ingestion, making it essential that it is free from harmful ingredients, allowing users to feel confident and at ease during use.
After analyzing lipstick ingredients, we find that they contain safe components that offer both health benefits and aesthetic advantages The careful combination of these ingredients does not lead to adverse reactions, as their chemical properties are compatible However, since lipstick is primarily made from fruit, it is susceptible to spoilage, rancidity, and mold.
Coconut oil and olive oil, commonly used in food, contain acceptable levels of preservatives, allowing lipsticks made from them to be stored at room temperature while maintaining a long-lasting color The process of creating these lipsticks is straightforward, with a high success rate, minimal time investment, and significant cost-effectiveness.
Due to time constraints in the research, the formulas could not be tested multiple times with varying ingredient ratios, which may lead to potential drawbacks in the selected formulation Additionally, the limited availability of research materials and factors restricts the diversity of the thesis, highlighting this as the primary disadvantage of the study.
CONCLUSION AND PROPOSAL
Conclusion
Found out a method to prepare trial lipstick with the main raw material is natural color, flavour and base And made 3 lipstick products with 3 different colors: red, yellow, pink
With pink pigment: Extraction time is 4 hours; Extraction temperature: 40 ⁰ C;
Solids / Solvent ratio: 1gr / 1ml; Mount of Betacyanin: 1,403gr
With yellow pigment: Extraction time is 10 hours; Extraction temperature is 80
⁰ C; Mount of raw material is 1kg; Mount of cucurminoid is 104gr
With red pigment: Extraction time is 10 hours; Extraction temperature is 80⁰C; Mount of raw material is 500gr; Mount of lycopene and betacarotene is 112gr
With flavour extraction: Extraction temperature is 100°C, total amount of essential oil after extracting is 61,2ml in time interval is 90 minutes with the a mount of material is 350ml
With trial complete lipstick fomula: 2gr of wax, 2,5ml of oil with about 2-2,5gr of pigments and 0.2% flavour
The products mentioned offer the same benefits as industrial alternatives, utilizing raw materials to reduce chemical usage in cosmetics They highlight innovative applications of natural ingredients, particularly red dragon fruit, turmeric, and Gac By transforming simple materials into increasingly valuable products, they ensure both safety and economic efficiency.
Proposal
The pursuit of natural resources for the development of diverse beauty products, including chalk and lotions, is ongoing There is a particular focus on researching additional materials to extract a wider range of colors and fragrances, which will benefit the organic lipstick industry.
Continue to find new and more superior lipstick formulas, complete the old recipe and test those recipes to see if they are completely safe for the user
1.http://www.trieuthanhweeklymagazine.com/suutam/st1/nhungkienthucthuvi.html 2.http://www.webtretho.com/forum/f3270/7-chat-doc-hai-trong-my-pham-lam-dep-
3.http://www.hoahocngaynay.com/vi/nghien-cuu-giang-day/hoa-hoc-nha-truong/1098- mui-cua-cac-este.html
4.http://www.ifrj.upm.edu.my/18%20%2801%29%202011/%2828%29%20IFRJ-
5 https://thaythuocvietnam.vn/tac-dung-cua-qua-gac-va-nhung-khuyen-cao-khi-dung/
6 http://vi.wikipedia.org/wiki/Ngh%E1%BB%87
7 http://tracuuduoclieu.vn/buoi.html
8 http://vi.wikipedia.org/wiki/Ong
9.https://fr.scribd.com/doc/283541869/Nghien-C%E1%BB%A9u-Chi%E1%BA%BFt-
Xu%E1%BA%A5t-Ch%E1%BA%A5t-Mau-Betacyanin-T%E1%BB%AB- V%E1%BB%8F-Qu%E1%BA%A3-Thanh-Long-Hylocereus-Spp
10.http://umpir.ump.edu.my/id/eprint/2711/1/YUNI_KHALIDA_BT_RIAZUDDIN.P
11 http://www.udn.vn/app/webroot/svnckh2012/PDF/TB18-05.pdf
12 Shurook Mohammad Kadhim Saadedin1, Iqbal Harbi Mohammed Al-Zaidi1, 2 and Salwa Jaber Abdullah AL-Awadi (2007) Solvents extraction efficiency for lycopene and β- carotene of GAC fruit (Momordica cochinchinensis, Spreng) cultivated in Iraq Page 27-28
13 Lê Thị Anh Đào, Đặng Văn Liếu (2005), Thực hành Hóa học hữu cơ, NXB Đại học Sư phạm
14 Hélène de Clermont-Gallerande1,* , Sarah Abidh1,2 , Alexandre Lauer1 , Séverine
Navarro1 , Gérard Cuvelier2 and Julien Delarue2 (2018) Relations between the sensory properties and fat ingredients of lipsticks
15 https://naturesense.vn/so-sanh-tinh-dau-va-huong-lieu/