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Tiêu đề A Novel Mechanism Design Following Augmented Objective with Flexible Energy Control
Tác giả Xuan Phu Do, Van Chi Le
Trường học Vietnam National University Ho Chi Minh City
Chuyên ngành Green Technology and Sustainable Development
Thể loại research paper
Năm xuất bản 2022
Thành phố Nha Trang
Định dạng
Số trang 509
Dung lượng 39,39 MB

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Nội dung

This proceedings contains the scientific contributions included in the program of the 6 th InternationalConference on Green Technology and Sustainable Development (GTSD2022), which was organized on July2930, 2022 in Nha Trang University, Khanh Hoa Province, Vietnam. The GTSD International Conferenceseries is a prestigious biannual event created to provide an international scientific research forum intechnologies and applications in the field of Green technology and Sustainable development in the Industrialrevolution 4.0. The areas of GTSD include but are not limited to energy engineering, environmentalengineering, education, digital transformation, new materials and solutions for sustainable development,advances in computational intelligence and their applications to the real world and so on.The conference is structurally organized in order to promote the active participation of all attendees andpresenters, via plenary presentation sessions, keynote addresses, interactive workshops and paneldiscussions, to find out how to further contribute to and solve various problems in life and manufacture. Theaim was to further increase the body of knowledge in this specific area by providing a forum to exchangeideas and discuss results.The program committee members of GTSD2022 come from various countries, and the 269 selected papers(out of more than 450 submitted papers) are from 27 countries and from 5 continents. This certainly attests tothe widespread and international importance of the theme of the conference. Each paper was carefullyreviewed on the basis of originality, novelty and rigorousness.We would like to take this opportunity to express our deep appreciation to all authors, participants, keynotespeakers, program committee members, session chairs, organizing committee members, steering committeemembers, as well as the organizers for their great efforts and contributions to making the GTSD2022successful, surging the global care about green technology research for sustainable development.

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PROCEEDINGS OF

TH 20226 INTERNATIONALCONFERENCE

ONGREENTECHNOLOGY

ANDSUSTAINABLEDEVELOPMENT

(GTSD)

VNUHCM PRESS

Trang 2

Proceedings of

and Sustainable Development (GTSD)

July 29-30, 2022 - Nha Trang City, Vietnam

VNUHCM PRESS

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Table of Contents

Editors Preface viii GTSD2022 Organizing Committee ix

A Novel Mechanism Design following Augmented Objective with Flexible Energy Control 1

Xuan Phu Do and Van Chi Le

Evaluating Green Marketing Trending Determinants by a Text Mining Approach 5

Phan-Anh-Huy Nguyen

A Simple Synthesis of Antibacterial and Antifungal ZnO Nanorods 8

Khanh Son Trinh and Vinh Tien Nguyen

An Assessment of Complementary Energy of HPFRCs under Tension 15

Duy-Liem Nguyen, Tien-Tho Do, Thi-Ngoc-Han Vuong and H T Tai Nguyen

A Study of the Scavenging Process in a Two-stroke Free Piston Linear Engine at Low Velocity Using CFD and DPM 21

Nguyen Huynh Thi, Nguyen Van Trang, Huynh Thanh Cong, Dao Huu Huy, Huynh Van Loc, Truong Hoa Hiep, Ngo Duc Huy and Vo Bao Toan

Investigating the Relationship between Workers’ Needs and Commitments to Garment Enterprise 27

Tu Tran

Optimization of Aggregates in Concrete Brick with Recycled Materials from Stone 32

Nguyen Thang Xiem, Ho Minh Chau, Tran Doan Hung and Truong Thanh Chung

A Comparison on the Flexural Capacity and Dynamic Performance of a Reinforced Concrete Beam and a Steel Beam in a High-rise Building 36

Tham Hong Duong

Optimization Model for Biomass Supply Chain Planning: A Case Study in Mekong River Delta – Vietnam 44

Thi-Be-Oanh Cao, Duc Duy Nguyen, Thanh-Tuan Dang and Chia-Nan Wang

Developing a Digital Competence Performance Assessment Platform for University Students Based on the DigComp Framework 50

Anh Tho Mai, Thi Kim Oanh Duong and Anh Tuan Ngo

The Performance of Geonet Reinforced Straw Rolls as a Flexible Waterbreaker for Riverbank Protection 57

Minh-Duc Nguyen, Le-Nhat-Huy Nguyen and Tran-Phuong-Thao Hua

SSD21, Educational Toolbox for Static, Stability, and Dynamic Analysis of Frame 63

Truong Thanh Chung, Le Nguyen Anh Vu, Le Cong Lap and Nguyen Thang Xiem

Digital Competence of University Students: A Comparative Study at Three Universities in Vietnam 67

Anh Tho Mai, Quynh Trang Mai and Anh Tuan Ngo

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ii

Load Capacity Evaluation of Simple Reinforced Concrete Girder Bridges with Considering the Corrosion of Reinforcement and Concrete 75

Tran The Truyen, Tran Thu Minh, Nguyen Dac Duc, Tran Duc Manh and Nguyen Quoc Cuong

Effect of Biodegradable and Metallic Mordants on Dyeing Cotton Fabric with Spent Coffee Grounds 80

Tuan Anh Nguyen

The Importance of Green Technology for Sustainable Development Education: A Case Study at Lac Hong University 85

Nga Hong Thi Doan and Truong Van Nguyen

Unique Competitive Advantages of Vietnam’s Garment Industry in the Sustainable Development Trend 89

Quang-Tri Tran, Thanh-Nhan Nguyen, Tho Alang, Tuyet-Anh Truong, Kim-Chi Le and Nguyen Thi Le

Driving Factors of Green Economy for Smart Cities in the Context of Developing Countries 95

Tiep Nguyen, Nghia Hoai Nguyen, Leonie Hallo and Bao Van Pham

Impacts of Green Training on Green Competencies of Employees: Empirical Case of Industrial Manufacturers in Dong Nai Parks 101

Thanh-Lam Nguyen, Doan Thi Chuyen, Nguyen Thi Phuong Thao and Doan Van Ly

Mathematical Modelling of Combined Infrared and Heat Pump Drying of Squid 107

Pham Van Toan, Phan Nhu Quan, Nguyen Hay and Le Anh Duc

Improving the Tensile and Compressive Strength of Cement-Based Materials by Hybrid Electrospun Nanofibers 114

Tri N M Nguyen, Xuan Tung Nguyen, Thanh Toan Dao, Huy Q Nguyen and Jung J Kim

Controlling Crystal Morphology via Crystallization Processes, Cases Studied of KDP and Zinc Lactate 118

Tam Le-Minh, Cuong Nguyen Van and Venkata Subbarayudu Sistla

A Green Solution for Kitchen Waste Treatment Using Earthworm, Experimental and Mathematical Approaches 122

Tam Le-Minh, Phuong Pham Thi Hong and Nhu Vo Thi Thu

Effect of Reinforcement Corrosion on Crack Development in Concrete Under Load 127

Vo Van Nam and Tran The Truyen

Study on Synthesizing and Size Controlling of Silver Nanoparticles by Using a System of Two Protectants Trisodium Citrate and Polyvinylpyrrolidone 132

Hien Chuc Mai, Quynh Nguyen Thi Nhu, Thuan Hoang Duc, Du Cao Van, Cuong Ngo Van and Dung Duong Thi Ngoc

Study on Chemical Composition and In-vitro Biological Activities of Salvia officinalis L in Lamdong,

Vietnam 137

Thao Tran Thach, Cuong Ngo Van and Xuan Nguyen Bang

Dynamic Analysis of Plates under Moving Discontinuous Impulsive Load on Viscoelastic Foundation 141

The Tuan Nguyen and Trong Phuoc Nguyen

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Isolation and Quantitative Determination of Geniposide from Gardenia jasminoides Ellis Using

High-Performance Liquid Chromatography 147

Vo Thi Nga, Truong Thi Khanh Van and Bui Trung Huu

Oxygen-LPG Torch for Thermal Spraying 152

Ngo Thanh Binh, Le Van Canh and Pham Huy Dong

Predicting Land Use Change in Buon Ma Thuot City, Dak Lak Province by Integrating GIS and Markov Chain 158

Nguyen Thi Ngoc Quyen, Nguyen Thi Tinh Au, Nguyen Cong Tai Anh and Tran Thi Xuan Phan

Dissimilar Friction Stir Welded Lap-joint of Aluminum Alloy 6061 and 316 Stainless Steel 165

Huy Huu Ho, Hao Dinh Duong, Nam Hoai Quach, Thuyen Van Phi, and Tra Hung Tran

A Stochastic Half-Car Model for Vibration Analysis with Uncertain Parameters 169

Nguyen Van Thuan

Sources of Payment Risks to Contractors in the Vietnam Construction Industry 173

Duong Vuong, Thao Huynh and Phu Tran

Pharmacognostic Assessment of Polyscias Fruticosa Leaves in Vietnam 180

Dao Phan Thi Anh, Hue Ha Thi, Trang Le Vu Khanh, Thanh Le Duc, Huong Nguyen Thi Thu and Trieu Ly Hai

Alkali-Activated Slag/Sugarcane Bagasse Ash Pastes Cured in Room-Air Ambient and in Saturated Lime Water: A Study on the Compressive Strength and Shrinkage 185

Duc-Hien Le and My Ngoc-Tra Lam

Production Efficiency Improvement Using Value Stream Mapping with Simulation: A Case Study in Vietnam 191

Xuan-Quang Bach, Thanh-Tuan Dang and Chia-Nan Wang

Study on the Effect of Mixing Ratio of Biodiesel Fuel Made from Animal Fat on Exhaust Emissions of the Fishing Vessel’s Diesel Engines 199

Pham Dinh Trung, Mai Duc Nghia and Ho Duc Tuan

A Study on Mechanical Properties of Ca-Alginate Hydrogels 204

Thanh Tan Nguyen, Van Tron Tran, Long Nhut-Phi Nguyen and Nguyen Thi My Le

Mechanical Characteristics of PBT Based Blend 208

Hoang-Khang Lu, Ngoc Tran-Nhu Nguyen, Huy Huynh-Nhat Do, Van-Huong Hoang, Van-Thuc Nguyen, Nga Thi-Hong Pham, Van-Tron Tran, Long Nhut-Phi Nguyen and Thanh-Tan Nguyen

An Evaluation of Corporation Social Responsibility Performance for Vietnamese Contractors 213

Nguyen Van Minh, Ha Duy Khanh, Soo Yong Kim and Chu Viet Cuong

Local Waste Seeds as Organic-Based Coagulant Aids in Water and Wastewater Treatment 218

Nhung Thi-Tuyet Hoang, Anh Thi-Kim Tran and Luu Hong Quang

The Implementation of 5C’s in Online-Foreign Language Teaching for Vietnamese Students in the 4.0 Era 222

Chau Le Thi Bao, Nhu Vo Hoang Nhu and Nhi Ho Yen

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iv

Antibacterial Activity of Aqueous Extracts from Marine Sponges Found in Vietnam’s Sea 229

Huynh Nguyen Duy Bao and Nguyen Khac Bat

Digital Competence of University Students: Developing Information and Data Literacy for IT Students at Ho Chi Minh City University of Technology and Education 233

Anh Tho Mai and Quynh Trang Mai

A Simple Design Method for Piled Raft Foundations 239

Tong Nguyen, Nhat Nguyen Le Anh and Dat Nguyen Thanh

Evaluating Performance of Petroleum Industry Using Data Envelopment Analysis: A Case Study in Vietnam 247

Kristofer Neal C Imperial, Chia-Nan Wang, Thanh-Tuan Dang and Nguyen Ngoc Hiep

Fire Resistance Properties and Geopolymer Coating 254

Van Su Le, Van Vu Nguyen, Artem Sharko, Doan Hung Tran, Petr Louda, Piotr Los, Thang Xiem Nguyen, Stanislaw Mitura and Katarzyna Buczkowska

Effects of Intake Air Temperature on Power and Emission Characteristics of the HCCI Engine Fueled with the Blends of 15% Ethanol and 85% Petrol Fuels 259

Minh Xuan Le and Thanh Tuan Nguyen

Linear Viscoelastic Characterization of an SMA Mixture Using Dynamic Indirect Tensile Test 263

H T Tai Nguyen, Hong Ha Mai and Van Hien Nguyen

Effect of the Limestone Powder Content on the Properties of Alkali–Activated Slag Mortar 268

Tai Tran Thanh, Chung Pham Duy, Tu Nguyen Thanh and Hyug-Moon Kwon

The Educational Philosophy of Existentialism with the Development of Personalized Learning for Learners in Massive Open Online Courses (MOOCs) – The Case of Ho Chi Minh City University of Technology and Education 273

Thi Thao Tran, Tran Phuong Thao Hua and Thi Chu Tran

Transportation Infrastructure Strategy for Sustainable Development: A Case Study of Vietnam Mekong Delta 281

Le Thu Huyen

Study on Behaviour of Short Pile Groups in Soft Ground with Sand Leveling on a Small Scale Model Using Schneebeli Analogue Soil 286

Sy Hung Nguyen and Thi Phuong Huyen Tran

Research and Preparation of Thinking Strategies for Quality of Textile and Garment Products Manufactured in Vietnam 292

Nguyen Phuoc Son, Nguyen Ngoc Chau and Nguyen Thi Tuyet Trinh

Building Students’ Self-Reliant on Problem-Based Learning by Embedding Mind of Engineering Design Concept at HCMC University of Technology and Education 296

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Fabrication of Graphene Oxide from the Graphite Rod of a Disposed Battery 305

Huy-Binh Do, Hoang-Trung Huynh, Thien-Trang Nguyen, Van-Cuong Pham, Tien-Luat Nguyen, Anh-Vu Phan-Gia and Maria Merlyne De Souza

Design and Optimization of a Compliant Mechanism for Vibration-Assisted Drilling 309

Hai-Thanh Nguyen, Van-Khien Nguyen, Phan-Khanh-Tam Nguyen, Huy-Tuan Pham, Quang-Khoa Dang and Pham Son Minh

Eco-friendly Adsorbent Formulated from Rubber Shell Biochar to Remove Chromium (Cr(VI)) from Aqueous Solutions 313

Linh My Nguyen

A Study on the Effect of the Shape of the Center Rib on Thermal Resistance on the Dual-Layer channel Heat Sink 317

Micro-Hung-Son Dang and Thi-Anh-Tuyet Nguyen

Experimental Study of the Effect of Heat Input on Tensile Strength and Microstructure of the Weld using the Orbital TIG Welding Process 321

Thien Tran Ngoc, Ngoc-Huy Dinh, An-Duong Tra, Kha-Duy Doan, Binh-Minh Ngo and Anh-Duc Pham Duc

A Study of Customer Satisfaction in Online Food Delivery Service Quality During the Covid-19 Pandemic: Baemin’s Case Study 326

Hong-Xuyen Thi Ho, Ngoc-Tra Tran Thi and Ngoc-Anh Ha Thi

Controllable Green Synthesis and Morphological Properties of Gold Nanostar 332

P Quoc-Duy Huynh, Van-Dung Le, Chi-Hien Dang, Radek Fajgar, The-Ha Stuchlikova, Jiri Stuchlik and Thanh-Danh Nguyen

Isolation, Selection and Identification of the Probiotic Properties of Lactobacillus spp from Shrimp

Ponds in Nhon Trach, Dong Nai 336

Doan Thi Tuyet Le, Le Thi Thu Huong, Phan Pham, Pham Minh Thinh, Vo Thi Lan Chi, Nguyen Phuoc Trung, Huynh Minh Hieu and Do Minh Anh

Production of Cheese from Reconstituted Milk and Soy Milk with the Addition of Microbial Transglutaminase 340

Pham Thi Hoan and Trinh Khanh Son

Studying the Effect of Biodiesel Blend Ratios Derived from Rubber Seed Oil on the Technical Characteristics of Diesel Engines without Modifying the Structure by Simulation and Experiment 349

Nguyen Manh Cuong and Huynh Phuoc Son

Work from Home during the Covid-19 Pandemic: A Qualitative Research with Women Taking Care

of Young Children 355

Hien Phan Thi Thanh, Thuy Nguyen Thi Thanh and Tram Nguyen Thi Mai

Study on Determining the Freezing Mode of Frozen Fillet Bigeye Tuna (Thunnus obesus) 361

Dzung Tan Nguyen, Linh Khanh Thuy Do, Chuyen Van Hoang and Tuan Thanh Chau

Numerical Investigation of the Optimum Operating Condition in Magnetically Confined Plasma with Sheared Slab Ion-Temperature-Gradient Model 367

Thanh Tinh Tran

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vi

Using Brake and Engine Torque to Control Traction on Either Side of the Drive Wheel 371

Tan Tai Phan and Van Nhu Tran

Fatigue Life of Accelerated Corroded Steel Plate 377

Dao Duy Kien, Nguyen Thanh Hung, Nguyen Thi Thu Hao, Nguyen Van Hung and Haidang Phan

A Study on Ultrasonic Shear Horizontal Waves in Composite Structures 381

Duy Kien Dao, Hoang Ngoc Quy, Truong Giang Nguyen, Ductho Le, Hoai Nguyen and Haidang Phan

Designing and Modeling Pipe Welding Machine 385

Tuong Phuoc Tho, Phan Phuc Khang, Tran Thanh Nhon and Pham Phi Long

Investigation of the Mechanical Properties of Lightweight Geopolymer Concrete Using Keramzite as Coarse Aggregate 390

Kiet Tran Tuan, Duc Nguyen Phan, Tuan Le Anh, Khoa Nguyen Tan and An Huynh Thao

Researching and Improving the Registration and Treatment Process in Health Care Facility with Lean Principles and Ergonomics Standards 394

Minh-Tai Le

Application of Lean and Six Sigma Tools to Improve Productivity and Product Quality at Dien Quang Company, Vietnam 401

Minh Tai Le, Hoang Khang Lu and Nhat Huy Do Huynh

Hydrogen Plasma Annealed Gallium and Aluminum co-doped Zinc Oxide Films Applied in emissivity Glass 408

Low-Shang-Chou Chang, Yun-Che Tsai, Huang-Tian Chan, Jian-Liang Lai, Jian-Syun Wu and Wei-Min Wang

Study on Pectinase Production by Bacillus subtilis in Molasses and Its Application for Coffee

Fermentation 412

Ngan K Le, Duy Q Nguyen, Nhi Y Dinh and Phu H Le

Environmental Sustainability: Exploring Managers’ Attitudes and Behaviours at High-End Accommodation Businesses in Vietnam 417

Thanh-Nhan Nguyen, Quang-Tri Tran and Tho Alang

Research on Optimal Algorithms Using Experimental Planning to Improve Shoe Production Line Productivity 425

Minh Tai Le, Thi Cam Duyen Doan and Huynh Thao Vy Nguyen

Application of Multivariable Linear Regression Algorithm to Support Inventory Management 431

Trung Tin Ngo, Minh Tai Le, Nguyen Kim Thoa Vo and Thanh Nam Luong

Ethanol in Gasoline Fuel Blends: Experimental Investigation Effects on Exhaust Emission of the Homogeneous Charge Compression Ignition Engine 437

Minh Xuan Le and Thanh Tuan Nguyen

The Impact of the Industrial Revolution 4.0 on Logistics Businesses: A Case in Mekong Delta 441

Ngo Hong Ngoc and Huang Ying Yin

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Enhancement in Dielectric Constant of Poly Vinyl Alcohol by Loading of Strontium Titanate for Supercapacitor Applications 447

Anju Yadav, Dinesh Kumar Yadav, Khushbu Meena, Kiran Devat, Narendra Jakhar, Rajesh Sahu, S K Jain and Balram Tripathi

Free Vibration Analysis of Smart FG Porous Plates Reinforced by Graphene Platelets Using Isogeometric Approach 451

Lieu B Nguyen and Duc-Thien Pham

Free Vibration of MSGT Porous Metal Foam Microplates Using a Moving Kriging Meshfree Approach 459

P T Hung

Impacts of Adverse Weather on Mode Choice Behavior: A case study in Hanoi City, Vietnam 469

Binh Nguyen Mai, Thi Anh Hong Nguyen, Akimasa Fujiwara and Canh Do

Travel Behavior on Ground Access Mode Choices by Introducing a New City Air Terminal: A Case Study of Vientiane Airport, Laos 474

Komack Keochampa, Canh Do, Akimasa Fujiwara and Thi Anh Hong Nguyen

A Study of The Tensile Strength for The Mixing Ratio of Eva in Pa6/Eva Blends 482

Minh-Nhat Nguyen, Quy-Long Nguyen, Ngoc-Thien Tran, Vinh-Tien Nguyen and Minh The-Uyen Tran

Cytotoxicity of Isoxazole/Pyrazole Curcuminoids against Human Oral Epidermal Carcinoma-KB Cell Line 486

Hoang Minh Hao, Ho Dung Manh and Vo Thi Nga

Modeling of Flow Mixed with Polymers in Open Channel Flow: Application on the Blumenau River in Brazil 491

Walid Bouchenafa, Airton Hoenicke, Bruna Luiza Cunico, Huyen Xuan Dang-Vu and Trong Dang-Vu

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viii

Preface

This proceedings contains the scientific contributions included in the program of the 6th International Conference on Green Technology and Sustainable Development (GTSD2022), which was organized on July 29-30, 2022 in Nha Trang University, Khanh Hoa Province, Vietnam The GTSD International Conference series is a prestigious bi-annual event created to provide an international scientific research forum in technologies and applications in the field of Green technology and Sustainable development in the Industrial revolution 4.0 The areas of GTSD include but are not limited to energy engineering, environmental engineering, education, digital transformation, new materials and solutions for sustainable development, advances in computational intelligence and their applications to the real world and so on

The conference is structurally organized in order to promote the active participation of all attendees and presenters, via plenary presentation sessions, keynote addresses, interactive workshops and panel discussions, to find out how to further contribute to and solve various problems in life and manufacture The aim was to further increase the body of knowledge in this specific area by providing a forum to exchange ideas and discuss results

The program committee members of GTSD2022 come from various countries, and the 269 selected papers (out of more than 450 submitted papers) are from 27 countries and from 5 continents This certainly attests to the widespread and international importance of the theme of the conference Each paper was carefully reviewed on the basis of originality, novelty and rigorousness

We would like to take this opportunity to express our deep appreciation to all authors, participants, keynote speakers, program committee members, session chairs, organizing committee members, steering committee members, as well as the organizers for their great efforts and contributions to making the GTSD2022 successful, surging the global care about green technology research for sustainable development

On behalf of GTSD2022 Organizing Committee

Assoc.Prof Hoang An Quoc

General Co-Chair of GTSD2022

and

Dr Nguyen Vu Lan

Publication Chair of GTSD2022

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GTSD2022 Organizing Committee

General Chairs

A/Prof Le Hieu Giang, HCMUTE, Vietnam

A/Prof Trang Si Trung, NTU, Vietnam

Prof Nguyen Ngoc Thanh, WUST, Poland

Prof Wen-June Wang, NCU, Taiwan

Prof Yo-Ping Huang, NPU, Taiwan

Honorary Chairs

A/Prof Thai Ba Can, HCMUTE, Vietnam A/Prof Do Van Dung, HCMUTE, Vietnam A/Prof Ngo Van Thuyen, HCMUTE, Vietnam

Dr Khong Trung Thang, NTU, Vietnam

General Co-Chairs

Dr Quach Hoai Nam, NTU, Vietnam

A/Prof Hoang An Quoc, HCMUTE, Vietnam

Prof Huann-Ming Chou, KSU, Taiwan

Prof Chang-Ren Chen, KSU, Taiwan

A/Prof Nguyen Vu Quynh, LHU, Vietnam

A/Prof Nguyen Thanh Lam, LHU, Vietnam

Program Chairs

A/Prof Nguyen Truong Thinh, HCMUTE, Vietnam A/Prof Do Thanh Trung, HCMUTE, Vietnam A/Prof Nguyen Minh Tam, HCMUTE, Vietnam

Dr Huynh Phuoc Son, HCMUTE, Vietnam

Dr Tran Thi My Hanh, NTU, Vietnam

Dr Pham Thi Thu Thuy, NTU, Vietnam

Program and Steering Committee

Prof Nguyen Trung Kien, HUTECH, Vietnam

Prof Surya Narayan Panda, Chitkara Uni., India

Prof Arun Patil, SGU, India

Prof Sid Nair, VIT, Australia

Prof Pracha Yeunyongkul, RMUTL, Thailand

A/Prof Atul Sharma, RGIPT, India

A/Prof Truong N Luan Vu, HCMUTE, Vietnam

A/Prof Le Chi Kien, HCMUTE, Vietnam

A/Prof Bui Van Hong, HCMUTE, Vietnam

A/Prof Nguyen Tan Dung, HCMUTE, Vietnam

A/Prof Chau Dinh Thanh, HCMUTE, Vietnam

A/Prof Vo Viet Cuong, HCMUTE, Vietnam

A/Prof Truong Dinh Nhon, HCMUTE, Vietnam

A/Prof Duong Thi Kim Oanh, HCMUTE, Vietnam

A/Prof Trinh Khanh Son, HCMUTE, Vietnam

A/Prof Ngo Dang Nghia, NTU, Vietnam

Dr Irma Kunnari, HAMK, Finland

Dr Lisa Donaldson, DCU, Ireland

Dr Lai Jiang, KULEUVEN, Belgium

Dr Manoj Kumar Dash, IIITM Gwalior, India

Dr Le Minh Nhut, HCMUTE, Vietnam

Dr Nguyen Xuan Vien, HCMUTE, Vietnam

Dr Diep Phuong Chi, HCMUTE, Vietnam

Dr Huynh Van Vu, NTU, Vietnam

Dr Mai Thi Tuyet Nga, NTU, Vietnam

Dr Tran Quang Huy, NTU, Vietnam

Dr Jari Jussila, HAMK, Finland

Dr Phan Gia Anh Vu, HCMUTE, Vietnam

Dr Tran Vu Tu, HCMUTE, Vietnam

Dr Dang Quang Vang, HCMUTE, Vietnam

Dr Nguyen Khac Hieu, HCMUTE, Vietnam

Dr Vu Van Phong, HCMUTE, Vietnam

Publication Chairs

Dr Nguyen Vu Lan, HCMUTE, Vietnam

Media and Publicity Chairs

Chau Ngoc Thin, HCMUTE, Vietnam

Nguyen Van Nguyen, HCMUTE, Vietnam

Local Arrangement Chairs

Tran Nhat Tan, NTU, Vietnam

Vu Thi Thanh Thao, HCMUTE, Vietnam

Do Thi Ngoc Dung, HCMUTE, Vietnam Phung Phuong Thu Thuy, HCMUTE, Vietnam Nguyen Thi Minh Ngoc, HCMUTE, Vietnam Nguyen Thi Hoa, HCMUTE, Vietnam

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A Novel Mechanism Design following Augmented

Objective with Flexible Energy Control

Xuan Phu Do

Mechatronics and Sensor Systems Technology

Vietnamese German University

Binh Duong, Vietnam phu.dx@vgu.edu.vn

Abstract: This study presents a newly proposed theory for

design of augmented structure, especially in exoskeleton

design A general model is proposed with basic elements of a

featured actuator related to mechanism The calculation

theory is based on dynamical analysis with new modifications

to obtain general equations for design The new theory is

different from the conventional theory, which always

assumed that the analyzed structure was zero in a static state

The augmented theory has broken out the barrier of the

classical model with a new added element related to the

accumulated energy in the structure, especially in the

mechanical spring After formulating, antagonistic variable

stiffness mechanism is chosen to evaluate the proposed

analysis The simulation results show that the proposed

theory can meet the requirement in the design of new

augmented mechanism

Keywords: augmented mechanism, exoskeleton design,

general augmented mechanism, upper exoskeleton, lower

exoskeleton

I INTRODUCTION

Design of exoskeleton with low power consumption and

high efficacy is always the ultimate objective The main

design is to develop special calculation and modified

mechanisms based on the conventional structure such as beam

deflection Normally, the trials in design are always the safe

choice to guarantee the performance of the proposed structure

when manufacturing However, this also leads to unexpected

results that the efficiency of the structure is lower than the

desired values This study presents a new view of design

mechanism based on the dynamical parameters to overcome

the disadvantage Generally, a view of the existing

publications related to the content of this study is carried out

A design of a low-power stiffness mechanism was presented

in [1] The ideal variable stiffness mechanism with its

potential energy was analyzed based on many assumptions

related to the consumption value To use the internal energy

to control the exoskeleton mechanism’s movement was

presented in [2] The internal energy [2] was from the muscle

states of a human, and this value belonged to the physical

health of every person The disadvantage of the internal

energy is its unstable value and can be attacked by the working

environment As mentioned above, the theory of beam

deflection is main analysis in any research of design

mechanism The review of this analysis was presented in [3]

An extension of the research [2] was studied in [4] The

infinity energy in the calculation of the exoskeleton was

presented in [4] The analyzed theories [1,2,4] are different

from the conventional analysis [5] The result [5] was the

background to interpolate the efficient area of the stiffness

mechanism The metabolic cost was studied in [6] This issue

is one of the problems when controlling the mechanism and directly affects the structure’s functions [6] New modification

of the structure [1] was presented in [7] This modification [7] concentrated on improving the mechanical function of the spring at the knee exoskeleton In addition, the movement of the centroid point in the robotic mechanism was studied in [8] When designing the structure, the centroid point is also a part

of soft compliance calculation The stiffness of the above mechanisms is different from the application of smart material

as shown in [9-13] with the same objective in control the movement

From the above summarization, stiffness control is still a state-of-art issue when controlling and designing the structure However, the conventional theory does not fully view the affection of the initial energy in the designed model Hence it needs support from the controllers to fulfil the desired requirements This is also the main objective of this research which is shown in the next sections

II CONVENTIONAL AND PROPOSED THEORY

Figure 1 Suddenly energy at the first time of vibration control

There exists a phenomenon as shown in Fig 1 in any system at the first state The energy at this state is always larger than other positions and also affects the control system

To analyze the phenomenon, two specific models are chosen

in this study The conventional model of the design mechanism is shown in Fig 2 In this figure, three main mechanism elements are listed: motor, transmission, and dynamic functions The output of the mechanism includes force, stiffness In some particular cases, the output force can

be replaced by the output torque belonging to the objective control This model is also similar to the featured model of an exoskeleton The potential energy of the structure is defined

as follows [1]:

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Where, fi is the ith force of the structure with its

equilibrium l 0 and the length l i at ith position It is noted that

Eq.(1) is the general model for any mechanism The value p

is angular position, and the value x is the translational

position of the system

Figure 2 The first model of Antagonistic Variable Stiffness

Mechanism (AVSM) Energy (1) includes the internal and external energies

Normally, the internal energies are always assumed zero

value for all calculations This assumption is used in the

conventional model to neglect the complicated analysis, and

the obtained results are acceptable From definition (1), the

official dynamic parameters related to the movement are

Where, fIN is the input force, fOUT is the output force, and

kOUT is the output stiffness In Fig (1), the transmission

element is normally the mechanical spring-like model In

some exceptional cases, the element is the beam and the

activated actuators The condition for an ideal elastic element

Where, K is a symbolized translational position In the

proposed equation (3), the condition energy for an ideal

mechanism is different from the classical definition This is

from the characteristic of the manufactured elements always

remains an initial power inside its model The energy can be

seen as lower power, but it is complete affection to combine

the external energy This combination brings an unexpected

phenomenon in dynamic response at the first time to apply a

controller The power motor can be defined as follows:

Where, the values of w w1, 2,w3are found based on the

experiment data corresponding to acceleration, velocity, and

initial power of the system; P0is the initial power of the

motor (W) Eq.(4) is designed based on the assumption in

Eq.(3) Eq (4) also satisfies the phenomenon in the first time

of vibration control as shown in Fig 1 This phenomenon

always exists in any system, especially in suspension The variation of the energy also leads to the changing stiffness of the system as follows:

flexible calculation for design progress

III APPLICATION TO ANTAGONISTIC VARIABLE STIFFNESS MECHANISMS AND DISCUSSIONS

A First modification of AVSM

The potential energy of the first model of AVSM as shown in Fig 2 is given by:

1( , )3

This research is funded by Vietnam National Foundation for Science and

Technology Development (NAFOSTED) under grant number

107.02-2020.13 Corresponding author: Dr Xuan Phu Do

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B Second modification of AVSM

Figure 3 The second model of AVSM

The second mode of AVSM is shown in Fig 3 The

potential energy of the first model of AVSM as shown in Fig

3 is given by:

1( , , x ) , , x

2

Where, k is the input stiffness of the structure, p is the

angular position, lis the deflection of the spring length, x 1

and x 2 are the position of the first and the second springs The

input force and the output stiffness are determined as follows:

, ,, ,

k R xx , where  is a constant related to the

proportionality of the force-deflection springs The input

force (14) can be written as follows:

The result (16) shows that the mechanism’s energy for

control is first order function with the input control and the

stiffness output This also points out that the movement is

independent when controlling

IV SIMULATION AND DISCUSSIONS

Simulation results of the first and the second AVSMs are

shown in Fig (4) and Fig (5) In the first model as shown in

Fig (4), the criterion for design follows the second-order

function of the input force and the output force This relation

is reflected clearly in Fig 4(a) It is shown that the increased

value of the output stiffness from 0 to 2 N/m corresponds to

the input force of approximately 100 N In this point, the

potential energy is nearly zero value However, the output

stiffness changes from 2 to 4 N/m with the potential energy 5

W as shown in Fig 4(b) It is remarked that the relation

between the input force and the potential energy is not linear

as shown in Fig 4(c) In Fig 4(c), it is shown that the

potential energy is not zero value if there exists internal energy of the structure as shown in Eq.(4)

The result of second AVSM is shown in Fig 5(a,b,c) The relation of the input force and the output stiffness is linear-like as shown in Fig 5(a) This response is from the connection of the first and the second mechanical springs as shown in Fig 3 The affection of the connection is also shown

in Fig 5(b) It is remarked that the values of the output stiffness are the actual value of the mechanical spring, which

is different from Fig 4 as the difference value when controlling The result in Fig 5(c) also points out that the potential energy will increase if there is internal energy in the structure

(a)

(b)

(c)

Figure 4 Result of the first AVSM: (a) input force versus output

stiffness, (b) potential energy versus output stiffness, (c) potential

energy versus input force

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4

(a)

(b)

(c)

Figure 5 Result of the second AVSM: (a) input force versus

output stiffness, (b) potential energy versus output stiffness, (c)

potential energy versus input force

In this study, a new view of the stiffness mechanism is

presented This proposed theory is designed from the mutation

energy at the first time to control the system This theory also

modifies the traditional mechanism theory that the energy is

always approximate zero value The proposed theory also

presents equations related to the stiffness, input energy, and

output energy These equations point out that the energy

cannot assume the zero value related to the design of the

mechanism Two AVSM models are used to apply the

proposed theory The simulation and its results show that the

proposed theory can be developed to design the augmented

mechanism for supporting the movement of the upper limb

and lower limb The theory also gives a new view of design mechanisms when the energy and the stiffness of the system cannot be predicted

REFERENCES

[1] Vincent Chalvet, David J.Braun, “Criterion for the design of low-power variable stiffness mechanisms”, IEEE Transactions

on Robotics, vol 33, no 4, pp 1002-1010, 2017

[2] Amanda Sutrisno, David J.Braun, “How to run 50% faster without external energy”, Science Advances, vol 6, no 13, eaay1950, 2020

[3] Ke Wu, Gang Zheng, “A comprehensive static modeling methodology via beam theory for compliant mechanisms”, Mechanism and Machine Theory, vol 169, pp 104598, 2022

[4] Amanda Sutrisno, David J.Braun, “Enhancing mobility with quasi-passive variable stiffness exoskeletons”, IEEE Transactions on Neural Systems and Rehabilitation Engineering,vol 27, no 3, pp 487-496, 2019

[5] C.E.English, D.Russell, “Mechanics and stiffness limitations

of a variable stiffness actuator for use in prosthetic limbs”, Mechanism and Machine Theory, vol 34, pp 7-25, 1999

[6] Daniel F.N.Gordon, Christopher McGreavy, Andreas Christou, Sethu Vijayakumar, “Human-in-the-loop optimization of exoskeleton assistance via online simulation of metabolic cost”, IEEE Transactions on Robotics, pp 1-20, DOI: 10.1109/TRO.2021.3133137

[7] Sung Y.Kim, David J.Braun, “ Novel variable stiffness spring mechanism modulating stiffness independent of the energy stored by the spring”, 2021 IEEE/RSJ International Conference

on Intelligent Robots and Systems (IROS), pp 1-6, DOI: 10.1109/IROS51168.2021.9636339, 2021

[8] Qiang Huang, Chencheng Dong, Zhangguo Yu, Xuechao Chen, Qingqing Li, Huanzhong Chen, Huaxin Liu, “Resistant compliance control for biped robot inspired by humanlike behavior”, IEEE/ASME Transactions on Mechatronics, pp 1-

11, DOI: 10.1109/TMECH.2021.3139332, 2022

[9] Do Xuan Phu, Kruti Shah, Seung Bok Choi, “A new magnetorheological mount featured by changeable damping gaps using a moved-plate valve structure”, Smart Materials and Structures, vol 23, pp 125022, 2014

[10] D X Phu, S B Choi, Y S Lee, M S Han, “Design of a new engine mount for vertical and horizontal vibration control using magnetorheological fluid”, vol 23, pp 117001, 2014

[11] Do Xuan Phu, Seung Bok Choi, “Vibration control of a ship engine system using high-loaded magnetorheological mounts associated with a new direct fuzzy sliding mode controller”, vol 24, pp 025009, 2014

[12] Xuan Phu Do, Huy Ta Duc, Le Tran Huy Thang, Seung Bok Choi, Dalseong Yoon, “Design of a new inside multi-coil clutch for knee-exoskeleton structure based on Helmholtz phenomenon and magneto-rheological fluid”, Proceedings Volume 10598, Sensors and Smart Structures Technologies for Civil, Mechanical, and Aerospace Systems 2018, 105983M,

2018, 105983M, 2018

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Evaluating Green Marketing Trending Determinants by a Text Mining Approach

Phan-Anh-Huy Nguyen

Faculty of Economics HCMC University of Technology and Education

Ho Chi Minh City, Vietnam huynpa@hcmute.edu.vn

Abstract: Green Marketing can also refer to the

production and marketing of goods based on environmentally

friendly products made from renewable materials This

approach attracted many companies in recent years

Identifying the trending factors influencing green marketing

is a complicated task This paper proposed a novel

approach based on text mining techniques to figure out the

new determinants in green marketing activities The results

of this paper can be applied to enterprises in their selecting

business strategy development to boost their business

performance

Keywords: text mining, green marketing, marketing

strategy, data mining

I INTRODUCTION

Green marketing is an important topic in recent years

since more entrepreneurs focus on the environmental impacts

on society Furthermore, it is getting more concerns from

many organizations in the era of industrial revolution 4.0 In

current years, there are several studies investigating green

marketing issues in business [1 - 8] However, most of the

previous papers have not found the main themes which are

affected by green marketing Figuring out the trending

determinants is critically important to solve those problems

Therefore, this paper implemented a text mining approach in

order to help the organizations to have better conversations in

the new situation

The contributions of this study are as follows:

1) A new text mining approach is adopted to analyze the new

dataset

2) Four main themes with some related factors have been

discovered

3) The implications are proposed to support the business to

solve the green marketing issues

The remaining sections of the study are organized as follows:

in section 2, the reviews of related works are presented

Section 3 proposed the methodology Section 4 shows the

experimental results and implications

II LITERATURE REVIEW

Green marketing has been defined and analyzed in many

studies in recent years In [1], Peattie and Ken reported the

concepts of green marketing and its main features Dalton et

al drilled down about management techniques when

applying green marketing [2] In [3], Jain, Akansha, et al

used MCDM to select a suitable green marketing strategy under fuzzy environment Suki et al investigated the impacts

of corporate social responsibility on the links between green marketing concerns and consumer purchase intentions [4] Chung, Kuo Cheng reported the green marketing orientation

to achieve sustainable development in hospitality management [5] Mujahid, M., et al analyzed the link between green marketing and performance in small businesses [6] In [7], Mohd Noor et al tried to understand the consumers and green product purchase decision in Malaysia using a structural equation modeling-partial least square (sem-pls) approach In [8], Amaliana, Luthfatul, et al analyzed the consistency of bootstrap resampling in structural model with PLS-PM approach with the technology acceptance model to evaluate in green marketing management strategy In [9], Said, Syahnur, et al applied green marketing practice in purchasing decision home care product The results of the study showed that the attribute of environmentally friendly product design with the green label

is a variable that dominates the selections of consumers when purchasing the products Furthermore, preference attribute weight is having the smallest influence on making the purchasing decisions To the best of our knowledge, there is

a lack of paper applying text mining to figure out the trends

in green marking in recent years Hence, this paper proposed

a new approach to handle this issue by evaluating the green marketing determinants

A Dataset description

In this study, we use a dataset which is collected from

4000 related articles from newspapers recently The following keywords are used for the query to get access to the data: business, experience, data, analysis, technology, skills, work, management

B Text mining method

We use text mining software to visualize word cloud with co-occurrences of term extracted from the main text dataset

In this paper, we use topic modeling by co-word analysis The frequency of keywords is utilized to create the co-occurrences matrix and the clusters of related topics Then, the network visualization is also conducted to show the relationships between topics The algorithm is:

Step 1: Similarity Matrix construction From the co-occurrence matrix by normalizing the latter matrix, the similarity matrix is constructed on differences in the total number of occurrences

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6

Step 2: Mapping technique:

The aim of mapping technique is to minimize a weighted

sum of distances between all pairs of items by the squared

Euclidean

Step 3: Translation, Rotation, and Reflection

The objective of three transformation techniques is to

transform the solution obtained for the optimization problem

Hence, it can create consistent results

The text mining results with discovered topics and

implications are described in this section

Figure 1 The word-cloud

From the resulting data in the word-cloud, it can be seen

that the keyword "Green" has been updated with a lot of tools,

maybe 5023 from green issues is seen as an issue that many

people care about and talk about The whole issue is updated

as “Marketing” with 2194 occurrences for marker work in

today's society is very important, especially the Green

Marketing trend Around the keywords when it comes to this

issue are: product, environment, consumer, company,

enterprise, energy, market and new

The keywords related to Green Marketing show that

consumers are interested in the company's environmentally

friendly products, affect the market, how is the energy

problem The keywords related to the issue show that

consumers are now interested in environmentally friendly

green products and new products or new energy sources to

help protect the environment, and companies should grasp

this green trend to influence the company's marketing to help

the company understand the market and develop better

The results obtained after performing data set analysis on

Green marketing appeared 4 main color clusters In each

cluster, there will be a particular factor that is larger than the

others because it appears more and has a strong association

with other clusters

Figure 2 Results for cluster 1 (red)

The factor “climate change” appears 134 times, although

it is not the factor with the highest frequency, it is an important factor that shows the relationship with other factors

in the same cluster 1 such as person, government, planet, effort This shows that climate change is an issue that the whole world needs to pay attention to Climate change will lead to many serious consequences for our planet, so people and governments are both working to limit and prevent climate change by saving resources, based on research and development technology to create new alternative energy

Figure 3 Results for cluster 2 (green)

The “market” element appears with the highest frequency

620 times among the elements in cluster2 It is not surprising that the element “market” appears a lot in the analysis results because the market is the place where marketing strategies are implemented In addition, in this cluster 2, we see the appearance of these factors such as strategy, research, firm (company), country, The appearance of these factors shows that if companies want to understand the market or dominate the market, it is essential to do research to analyze and come

up with appropriate strategies for each market in different countries and different families In a market where consumers are increasingly concerned about the environment, companies need to make changes in product strategies to meet consumer needs

Figure 4 Results for cluster 3 (blue)

Product is the element that appears the most with 1837 times and has many close links with factors inside and outside the cluster to create a strong linked system The reason that

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products are mentioned so many times in the topic of green

marketing is because plastic waste is currently a factor that

has a serious impact on the environment However, most of

the plastic waste discharged into the environment today

comes from product packaging, so in order to implement

green marketing campaigns, the first thing that needs to be

mentioned must be the change Product packaging becomes

more environmentally friendly

Through the links between product elements (product)

and factors inside and outside the cluster such as consumers,

technology, brands, strategies, etc., we see that brands should

start making changes to their products by applying new

technologies to research alternative materials in order to

change the product packaging to be more environmentally

friendly by capturing the green living trend that consumers

are aiming Certainly, this change will also consume time and

money of businesses, but if businesses have specific and

properly executed strategies, they will bring good results such

as gaining advantages in the market as well as building value

for the brand in the hearts of consumers

Figure 5 Results for cluster 4 (Yellow)

In this cluster, we focus on analyzing the green product

factor Like the analysis mentioned above, green product is a

trend in the current market However, creating green and

environmentally friendly products will cost many times

higher than conventional products Therefore, at present,

green and environmentally friendly products are still very

expensive compared to other common products That also

creates a huge impact on sales of green products Hence,

businesses need to have more strategies, learn to apply

technologies, and cooperate with suppliers to minimize the

cost of producing green products From there, it is possible to

optimize the price to compete in revenue with other

conventional products

V CONCLUSION

In this study, a novel text mining approach has been

implemented to find the green marketing trends There are

four main clusters which are the themes that have been

discovered From that, we have also analyzed the meanings

of each topic with some related determinants Then some business implications have been reported from the results The limitation of this research is the number of text documents in the dataset is not quite huge For future work,

we could get more data to solve some bias problems We could also apply sentiment techniques for implementing those tasks

[4] Suki, Norazah Mohd, Norbayah Mohd Suki, and Nur Shahirah Azman "Impacts of corporate social responsibility

on the links between green marketing awareness and consumer purchase intentions" Procedia Economics and Finance, vol 37, pp 262-268, 2016

[5] Chung, Kuo Cheng "Green marketing orientation: Achieving sustainable development in green hotel management" Journal of Hospitality Marketing & Management, vol 29.6, pp 722-738, 2020

[6] Mujahid, M., et al "Linking green marketing with performance: Environmental marketing model for small business" IOP Conference Series: Earth and Environmental Science vol 737 No 1 IOP Publishing, 2021

[7] Mohd Noor, Mohd Nazri, et al "Understanding consumers and green product purchase decision in Malaysia: a structural equation modeling-partial least square (sem-pls) approach" Asian Social Science , vol 12.9, pp 51-64, 2016

[8] Amaliana, Luthfatul, et al "The consistency of bootstrap resampling in structural model with PLS-PM approach: technology acceptance model in green marketing management strategy" IOP Conference Series: Earth and Environmental Science Vol 239 No 1 IOP Publishing,

2019

[9] Said, Syahnur, et al "Green Marketing Practice In Purchasing Decision Home Care Product" International Journal of Scientific & Technology Research, vol 9.06, pp 893-896,

Trang 21

8 Copyright © authors This work is licensed under a Creative Commons

Attribution-NonCommercial-NoDerivatives 4.0 International License

A Simple Synthesis of Antibacterial and Antifungal

ZnO Nanorods

Khanh Son Trinh

Faculty of Chemical and Food Technology

Ho Chi Minh City University of Technology and

Education

Ho Chi Minh City, Vietnam

sontk@hcmute.edu.vn

Vinh Tien Nguyen

Faculty of Chemical and Food Technology

Ho Chi Minh City University of Technology and

Education

Ho Chi Minh City, Vietnam tiennv@hcmute.edu.vn

Abstract: ZnO nanorods were prepared by precipitation

method with Zn(CH3COO)2 as the precursor, NaOH as the

precipitating agent and soluble starch as the capping agent

X-ray diffraction analysis showed that the ZnO nanoparticles

(NPs) were structured in the wurtzite lattice with an average

crystallite size of 11.38 nm Field-emission scanning electron

microscopy coupled with energy-dispersive spectroscopy

showed that the material was mostly nanorods with an

average size of 28 nm UV-vis absorption spectra showed that

ZnO-NPs strongly absorb UV radiations The ZnO NRs

demonstrate typical dose-dependent antimicrobial activities

and inhibited Escherichia coli, Staphylococcus aureus, and

Salmonella sp 99.7, 99.96, and 100% respectively at 184

ppm ZnO-NPs At 553 ppm concentration, ZnO-NPs

demonstrated 100% inhibition for the three bacterial strains

Gram-positivity and Gram-negativity seemed to be

unimportant for the resistance of bacteria toward ZnO NRs

ZnO NRs at 14740 ppm showed a weak 98.2% growth

inhibition against the fungi Colletotrichum gloeosporioides

FESEM and EDS analyses showed that the cells of bacteria

were distorted and damaged when being in contact with ZnO

NRs in dispersion The fungal cells in these conditions turned

into spores and were also damaged The synthesized ZnO

NRs can find a wide range of applications as an antibacterial

and antifungal component in inks, paints, coatings,

cosmetics, and pharmaceutics

Keywords: ZnO nanoparticles, antibacterial, antifungal,

UV absorption, Staphylococcus aureus, Salmonella

I INTRODUCTION

In recent years, the synthesis and antimicrobial activities

of ZnO nanomaterials are gaining much attention due to their

low cost, chemical stability, biocompatibility and

biodegradability Recent research on ZnO nanomaterials

focused on green methods of their syntheses using natural

sources of reagents For example, plant extracts were used to

synthesize ZnO nanoparticles and their antibacterial activity

was tested on E.Coli, Streptococcus sp, Enterococcus sp, and

Klebsiella sp [1] Another study used the powder of leaves of

S multiflorus to prepare ZnO nanomaterials and tested their

antifungal activity on Aspergillus niger and Aspergillus flavus

[2] ZnO nanomaterials were also synthesized using

diethylene glycol and triethylene glycol and incorporated into

an antimicrobial film against Staphylococcus aureus and

Proteus vulgaris [3]

Most of the methods using natural sources such as plant

extracts are relatively complicated due to involving the extract

preparation and hence increasing the production costs In this study, we used a simple chemical method to prepare the ZnO nanoparticles (NPs) using inexpensive and commercially available reagents including zinc acetate as the precursor, sodium hydroxide as the precipitating agent, and soluble starch as the capping agent to control the size of NPs The produced ZnO NPs were then tested for antibacterial and antifungal activity against different species

II EXPERIMENTAL METHODS

A Synthesis and characterization of ZnO NPs

ZnO NPs were synthesized based on a reported method [4] Soluble starch (1.5 g) was completely dissolved in 250 mL

of distilled water by stirring at 90oC for 10 min After cooling the solution to room temperature, 5.4875 g of Zn(CH3COO)2.2H2O (0.025 mol) was added and stirred until complete dissolution After that, 250 mL of 0.2 M NaOH solution was added dropwise under continuous stirring The solution was then left stirred for 2 h to complete the reaction The reaction mixture was then filtered and the solid was washed with 3x 500 mL of distilled water and dried at 80oC The dried solid was then ground into a powder

UV-vis spectra were recorded using a UH5300 (Hitachi, Japan) spectrophotometer

X-ray diffraction spectra were recorded using a D8 Advance platform (Bruker, Germany) with  = 0.15406 nm at

nm was the wavelength of the X-ray, K = 0.9 was a constant, and D (nm) was the crystallites size

Field Emission Scanning Electron Microscopy (FESEM) was conducted using an S–4800 (Hitachi, Japan) electron microscope Energy Dispersive Spectra (EDS) were recorded using a 7593-H spectrometer (Horiba, Japan) Before FESEM and EDS measurements, the ZnO sample was sputtered with

a thin layer of Pt to enhance the electrical conductivity of ZnO

B Antimicrobial tests of ZnO NPs

Antibacterial activity of ZnO NPs was evaluated based on

a reported method with some modifications [6] The E.coli

bacteria were first activated in a Nutrient Broth medium at

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37oC for 24 h The ZnO NPs were dispersed in a nutrient agar

medium with different concentrations from 0 to 737 ppm The

nutrient agar medium was poured into Petri dishes and when

the agar solidified, 100 l of the bacteria suspension was

spread on the surface of the agar The Petri dishes were then

incubated at 37oC for 24 h After that, the density of survived

bacteria was determined by counting the number of bacterial

colonies The antibacterial activity was calculated using the

formula

%inhibition=𝐴1 −𝐴2

𝐴1 × 100, where A1 was the bacterial density in the Petri dish without

ZnO NPs (CFU/mL), and A2 was the bacterial density in the

Petri dish with ZnO NPs (CFU/mL)

One-way Analysis of Variance (ANOVA) was conducted

to test the statistically significant difference between the

means with a confidence level of 95%

Antifungal activity of the ZnO NPs was evaluated using a

reported method [7] A PDA medium was autoclaved at 121oC

for 15 min and then ZnO NPs were added with different

concentrations from 0 to 14740 ppm The medium was poured

into Petri dishes and left for solidification The spores of the

fungi were then put in the centre of each Petri dish The size

of the fungal colony was measured every day The percent

inactivation was calculated using the following formula [8]:

Where So was the area of the fungal colony (cm2) in the

control Petri dish without ZnO NPs (cm2) and Ss was the area

of the fungal colony (cm2) in the Petri dish with ZnO NPs

(cm2)

To evaluate the effect of the presence of ZnO NPs on the

bacterial cells, the microorganisms were first activated (in

Nutrient Broth medium for bacteria and in Potato Dextrose

Broth medium for fungi) at 37oC for 24 h After that, 30 mL

of the bacteria suspension was added to 30 mL of a sterilised

Nutrient Broth medium containing ZnO NPs of 184 ppm for

bacteria and 3685 ppm for fungi After 24 h of stirring, the

bacterial cells were centrifuged at 2000 rcf for 30 min, put on

a silicon wafer and left for drying under ambient conditions

The morphology of the cells was observed using the FESEM

and EDS equipment which was used for ZnO NPs described

above [9]

In this reaction, zinc ions were first precipitated into Zn(OH)2 and then dissolved in the presence of excessive hydroxide ions:

Zn2+ + 2OH- → Zn(OH)2 Zn(OH)2 + 2OH- → Zn(OH)42- + 2H+

The complex was unstable and gradually turned into ZnO NPs according to the reaction [10]:

Zn(OH)42- → ZnO +H2O + 2OH- The presence of excessive OH- ions turned soluble starch into a negatively charged form and hence stabilized the ZnO NPs by interacting with the positively charged Zn ions in the ZnO crystallites [11]

A Characterization of ZnO NPs

XRD spectrum of the synthesized material (Figure 1) shows characteristic peaks with corresponding planes of ZnO: 31.8424o (100), 34.3866o (002), 36.2351o (101), 47.4113o (102), 56.605o (110), 62.9608o (103), and 68.0339o (112), which were also reported in another study [12] These peaks indicated the wurtzite structure of ZnO based on the standard JCPDS number 36–1451

Figure 1 XRD spectum of ZnO NPs

The peaks at 2θ of 33.5334o and 59.5205o belong to Zn(OH)2, according to JCPDS number 38–0356 [13] This result indicated that the temperature of 80oC was not high enough to fully convert Zn(OH)2 to ZnO

The crystallites sizes of ZnO NPs were calculated using the Debye – Scherrer equation for different XRD peaks The average of these sizes was 11.38 nm, which is close to the size

of the ZnO NPs determined from the SEM images

Figure 2 FESEM micrograph of ZnO NPs at 50 000 magnification (A) and frequency distribution of particle sizes from

the FESEM micrographs (B)

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10

Figure 2A shows that there were several shapes of ZnO

NPs, including nanorod, nanowire, and nanotube, with the

majority being nanorods The nanorod shape of ZnO NPs in

this study was due to the usage of precursor zinc acetate It

was shown that the acetate precursor of zinc produced mainly

nanorods, while the chloride and sulfate precursors produced

nanoprims [14] Besides, in this study we used dilute 0.1 M

solution of zinc ions, thus facilitating the formation of

nanorods instead of nanoplates [15]

Figure 2B shows that the sizes of nanorods ranged from 10

to 57 nm with an average of 27.7 nm This result demonstrated

that the soluble starch effectively protected the NPs from

aggregation and growing in diameter [16]

The Energy dispersive spectrum (Figure 3) shows that zinc and oxygen were the main elements in the synthesized material The presence of carbon and the higher atomic percentage of oxygen compared to zinc were possibly due to the presence of soluble starch absorbed on the surface of ZnO NPs Because the size of ZnO NPs was small, the surface interaction between the capping soluble starch and the ZnP was strong, therefore it was difficult to completely remove the soluble starch by washing with water The presence of Al was due to the aluminum holder of the ZnO sample and the presence of Pt was due to the platinum sputtering process before SEM and EDS measurements

Figure 3 EDS spectrum (left) and element composition (right) of the synthesized ZnO NPs

UV-vis spectrum of the ZnO NPs dispersion in water

(Figure 4) shows a broad absorption peak near 366 nm This

result is similar to that of another study that reported an

absorption band of ZnO NPs from 355 to 380 nm [17] The

strong absorption of UV radiations by ZnO NPs can have

several applications such as in sunscreens or anti-aging

coatings

B Antibacterial activity

Table 1 shows that a concentration of 185 ppm of ZnO

NPs inhibited at least 99.0% of the growth of the three

bacteria ZnO NPs exhibited a dose-dependent antibacterial

activity, which was also reported in other studies [18, 19] The

high antibacterial effect was due to ZnO NPs because an

equivalent amount of Zn(CH3COO)2 exhibited significantly

lower antibacterial activity [19]

Figure 4 UV-vis spectrum of the dispersion of synthesized ZnO

NPs in water

Table 1 shows that the antibacterial effect of ZnO NPs

against negative E.coli was lower than against positive S.aureus, similar to other reports [20-22] In Gram-

Gram-positive bacteria, the cell is protected by a thick peptidoglycan membrane composed of teichoic acid, lipoteichoic acid, and surface proteins, while in Gram-negative bacteria, the cell is protected by a membrane composed of lipopolysaccharide,

porins and a thin peptidoglycan layer [23] Although E.coli and Salmonella are both Gram-negative, E.coli is more resistant while Salmonella is less resistant than S.aureus to

ZnO NPs This result indicated that the Gram type of bacteria might not be a significant factor in their resistance toward ZnO

369 ppm

553 ppm

737 ppm

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Figure 5 Area growth of C gloeosporioides treated with ZnO NPs with different concentrations for 7 days

C Antifungal activity

Figure 5 shows that the fungi C gloeosporioides

continuously grew even in the presence of ZnO NPs

However, the presence of ZnO NPs significantly inhibited the

fungal growth in all 7 days of the experiment Increasing the

ZnO NPs concentration resulted in higher growth inhibition

After 7 days, with ZnO concentrations from 3685 to 14740

ppm, the percent inhibition ranged from 82.8% to 98.2%,

which is similar to the results of 93% inhibition against C

gloeosporioides [24] and 84.5% inhibition against

Erythricium salmonicolor [8]

The high antifungal activity of ZnO NPs was due to the

small size of the synthesized material [25] The mechanism of

antifungal activity was found to be the formation of reactive

oxygen species with high oxidative activity, hence lead to the

alteration of membrane permeability and subsequent cell

death [26, 27]

We used FE-SEM and EDS methods to observe the

microbial cells without and with the presence of ZnO NPs in

the nutrient agar in the previous antimicrobial tests

D Morphology and elemental analysis of microbial cells after ZnO NPs treatments

Comparing sub-figures (A) and (B) in Figures 6, 7, and 8 shows that the bacterial cells were shrinkled and distorted after the treatment with ZnO NPs On the cells in sub-figures (B) there were white dots that contained 3-10% zinc atoms based

on the EDS analysis (data table not shown), which are similar

to other studies [28-31]

It was found that the dispersion of ZnO NPs in the nutrient medium produced reactive oxygen species (ROS) such as hydroxide, superoxide, and hydrogen peroxide [29] These ROS with high reactivity would then react with components

of bacterial cell walls including proteins, lipids, and DNA, hence leading to cell death Hydrogen peroxide penetrates the cell wall into the cell, while superoxide ions attack the cell [32, 33] Another antibacterial mechanism of ZnO NPs was the direct attachment of the NPs on the cell wall and subsequent interaction with the membrane components such as proteins and enzymes, which also lead to the dysfunction of the cells and their death [34]

Figure 6 E.coli cells before (A) and after (B) treating with 184 ppm of ZnO

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12

Figure 7 S.aureus cells before (A) and after (B) treating with 184 ppm of ZnO NPs

Figure 8 Salmonella cells before (A) and after (B) treating with 184 ppm of ZnO NPs

Before treating C.gloeosporioides with ZnO NPs, one can

easily find the fungal cell in the FESEM micrograph (Figure

9A) However, after treating the fungi with ZnO NPs for 24 h,

we found only their spores (Figure 9B), with the presence of approximately 6.5% zinc atoms on the surface

Figure 9 A cell of C gloeosporioides before ZnO NPs treatment (A) and a fungal spore after treating the cells with ZnO NPs (B)

The antifungal mechanism of ZnO NPs is different from

their antibacterial mechanism and is attributed to the attack of

Zn2+ ions on N-acetylglucosamine or β-1,3-D-glucan synthase

(FKs1p) [8] N-acetylglucosamine plays a vital role in the

synthesis of chitin, and β-1,3-D-glucan synthase takes part in the synthesis of β-1,3-D-glucan [35] Both chitin and β-1,3-D-glucan are important components in the structure of fungal cell walls [8]

Trang 26

IV CONCLUSION

In this study, we synthesized ZnO NPs in the shape of

nanorods with sizes mostly lower than 60 nm due to the

capping role of soluble starch The ZnO NPs demonstrate a

dose-dependent antibacterial activity toward different bacteria

and fungi Gram-positivity and Gram-negativity seemed to be

unimportant for the resistance of bacteria toward ZnO NPs

FESEM and EDS analyses showed that the cells of bacteria

were distorted and damaged when being in contact with ZnO

NPs in dispersion The fungal cells in these conditions turned

into spores and were significantly inhibited With the low cost

of zinc acetate precursor and the ease in the synthesis of ZnO

NPs, the material can find a wide range of applications as an

antibacterial and antifungal component in inks, paints,

coatings, cosmetics, and pharmaceutics

ACKNOWLEDGEMENT

The authors acknowledge Ho Chi Minh City University of

Technology and Education for the facility and equipment

required for this study We thank Mr Nguyen Duc Manh

(student ID 15116030) and Mr Nguyen Quoc Tuan Anh

(student ID 15116002) for their helpful technical support

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[6] S S Shinde, "Antimicrobial activity of ZnO nanoparticles

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3, p 1033, 2015

[7] M Al‐Hetar, M Zainal Abidin, M Sariah, and M Wong,

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f sp cubense", Journal of applied polymer science, vol 120,

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[8] P Arciniegas-Grijalba, M Patiño-Portela, L

Mosquera-Sánchez, J Guerrero-Vargas, and J Rodríguez-Páez, "ZnO

nanoparticles (ZnO-NPs) and their antifungal activity against

coffee fungus Erythricium salmonicolor", Applied

Nanoscience, vol 7, no 5, pp 225-241, 2017

[9] R K Dutta, P K Sharma, and A C Pandey, "Assessing the

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E Ali, "Synthesis of ZnO nanostructures using sol-gel

method", Procedia Chemistry, vol 19, pp 211-216, 2016

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nanoparticles with controlled morphology", Journal of Materials Chemistry, vol 9, no 11, pp 2871-2878, 1999 [16] G Krithika et al., "Zinc oxide nanoparticles—Synthesis, characterization and antibacterial activity", Journal of Nanoscience and Nanotechnology, vol 17, no 8, pp 5209-

5216, 2017

[17] N M Shamhari, B S Wee, S F Chin, and K Y Kok,

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99-101, 1957

Trang 28

An Assessment of Complementary Energy of

Ho Chi Minh City University of Technology and Education

Ho Chi Minh City, Vietnam thodt@hcmute.edu.vn

Thi-Ngoc-Han Vuong

Faculty of Civil Engineering

Ho Chi Minh City University of Technology and Education

Ho Chi Minh City, Vietnam hanvtn@hcmute.edu.vn

H T Tai Nguyen

Faculty of Civil Engineering

Ho Chi Minh City University of Technology and Education

Ho Chi Minh City, Vietnam tainht@hcmute.edu.vn

Abstract: This paper deals with the complementary

energy of HPFRCs under tension through an experimental

study The HPFRCs were prepared from an identity matrix

but with different fiber types or volume contents The fiber

used in this research is long twisted with a length of 30 mm

and a diameter of 0.3 mm There were four levels of fiber

volume content as follows: 0.5 vol.%, 1.0 vol.%, 1.5 vol.%

and 2.0 vol.% to investigate the effect of fiber volume content

on the energy parameters of HPFRCs The complementary

energies of the HPFRCs were evaluated and correlated to a

number of microcracks as the dosage of the fiber was

changed

Keywords: HPFRC, Complementary energy,

First-cracking, Post-First-cracking, Energy absorption capacity

High-performance fiber-reinforced concretes (HPFRCs)

have been classified as one of the sustainable construction

materials, which can enhance structure resistance and avoid

ruinous disasters [1-3] The term “high-performance” of

HPFRCs refers to strain-hardening behavior accompanied by

multiple micro-cracks This property can be identified with an

increase of stress after the first crack due to the crack-bridging

mechanism of reinforcing fibers, and consequently leads to

high strain capacity and large energy absorption capacity of

HPFRCs HPFRCs only produce strain-hardening behavior

with suitable fiber type/content mixed in the plain concrete

[1-5] The interfacial bond between the fiber and HPFRC matrix

is strongly dependent on fiber type/content, which will govern

the mechanical properties of HPFRCs

On the other hand, a strain hardening HPFRC with lower

crack spacing, is characterized as a more ductile material This

is because the fracture strain beyond the first crack is mainly

due to microcracks, which were generated during

strain-hardening [1-3] Complementary energy is defined as the area

above the stress versus strain response curve of a material The

ratio of complementary energy to the crack tip toughness of

the mortar concrete will represent the capability of producing

many microcracks, as illustrated in Fig 1 [6-10] It is clear that

complementary energy is a key engineering property of

HPFRCs that should be evaluated Based on the test data of

the previous studies of the first author [11,12], this paper

focuses on the effect of fiber content on the complementary

energy of HPFRCs, which has been not assessed yet Better

understanding mechanical properties of HPFRCs, including their complementary energy, is highly expected to widen the application of HPFRCs

scc

Hardening energy (G hd )

epc ecc

Multiple microcracks

Crack Localization

Complementary energy (CE)

to evaluate in the discussion part

- The elastic energy (named G el) is the zone under the stress versus strain relationship curve within the elastic stage and calculated using Eq (1) It characterizes the energy absorption capacity per unit volume during extending a tensile specimen from 0 to ecc

- The hardening energy (named G hd) is the zone below the stress versus strain relationship curve with the strain range from 0 to epc The Ghd indicates the energy absorption capacity per unit volume during extending a tensile specimen from 0 to epc, it can be derived using Eq (2)

- The crack tip toughness (named CT ) is the zone above

the stress versus strain relationship curve in the elastic stage and given using Eq (3) It is noted that this expression is

equivalent to the result obtained by Li et al [13] The CT

reveals the energy per unit volume can not be absorbed during extending a tensile specimen from 0 to ecc

Trang 29

16

- The complementary energy (named CE ) is the area

above the stress versus strain relationship curve with the strain

range from 0 to epc [13,14] The CE represents the energy

per unit volume can not be absorbed during extending a tensile

specimen from 0 to epc, it can be derived using Eq (4)

0

( )

cc el

pc hd

e e e

It is noted that the Ghd and Gel are the true energies

absorbed by a tensile specimen under loading whereas the CE

and CT are the virtual energies only

A Materials and preparation of specimens

Lmm dmm

Figure 2 Photo of the twisted fiber type in this research

Table 1 Composition and compressive strength of Mortar Matrix

Materials Weight ratio

Compressive strength (MPa) 89

Table 2 properties of six fiber types

Fiber type

(Notation)

Tensile strength (MPa)

Length (mm)/

Diameter (mm)

Density (g/cm 3 )

Long twisted

The HPFRCs used an identical mortar matrix, whose composition is provided in Table 1 according to weight ratio The partial materials are sand, fly ash, cement and silica fume, water and superplasticizer The amount of superplasticizer was 0.07 by weight ratio of the cementitious materials It is noted that the sand in the mixture plays an engineering role as coarse filler material whereas the fly ash and silica fume play

a role as fine filler materials to densify the concrete mixture The compressive strength of the mortar matrix using a cylindrical specimen with a size of 100×200 mm was 89 MPa

at 18-day age Table 2 provides the properties of long twisted fiber (T30/0.3) used in this research Photos of the fiber were presented in Fig 2

All constituent materials of HPFRC were blended using a 20-L laboratory mixer (Hobart type) Sand, fly ash, cement and silica fume were dry-mixed for about 10 min at first After dry-mixing, water and then superplasticizer were added

to the mixture and wet-mixed for about 10 min Because the plain mortar showed appropriate flow capability and, the steel fibers were gradually added to the mortar mixture by hand and further blended for 5 min After demolding, all specimens were cured in water at the temperature of 25oC for 14 days The detail of mixing work can be referred to in previous studies [11,12]

Hinge mechanism

Hinge mechanism

b) Experiment setup for direct tensile test

Figure 3 Tensile specimen detail and experimental setup

Trang 30

Dog-bone-shaped specimens were used in the direct

tensile test The working section over the gauge length of 100

mm is rectangular with a dimension of 50 × 25 mm2 To

prevent failure beyond the gauge length, both specimen ends

were reinforced by employing steel wire meshes, as described

in Fig 3a All the prepared specimens were tested through a

universal testing machine (UTM) with

displacement-controlled loading The standard displacement rate of 1.0

mm/min was applied to the movable crosshead of the UTM

The data collecting rate during loading was 1 Hz The

specimen elongation under tension was measured by two

linear variable differential transformers (LVDTs), as shown in

Fig 3b Besides, the hinge mechanism was designed at both

specimens Response curves of tensile stress versus strain of the HPFRCs were built and their complementary energies were derived and evaluated

A Tensile responses of HPFRCs with different fiber contents

Fig 4 presents the direct tensile responses of the HPFRCs using the same fiber type T30/0.3 but fiber content varying from 0.5 to 2.0 vol.% As can be seen in Fig 5, all these HPFRCs also exhibit strain-hardening behaviors, although the fiber contents were significantly different

Figure 4 Tensile responses of HPFRCs with different fiber contents

Table 3 Tensile parameters with different fiber contents

cc

s(MPa)

0.28 (0.077)

4.86 (0.69) 1.0 (0.003) 0.016 (0.47) 2.56 (0.092) 0.52 (0.78) 7.48

(0.002)

3.41 (0.03)

0.49 (0.035)

9.99 (1.22)

(0.005)

3.41 (0.27)

0.55 (0.013)

12.53 (0.36)

Note: The standard deviations are delivered within parentheses

Table 3 shows the tensile parameters of the HPFRCs using T30/0.3 type with different fiber contents, varying from 0.5 vol.% to 2.0 vol% The tensile parameters in Table 4 were averaged from three tested specimens for each series, the values in the brackets were standard deviations As presented

in Table 4, all the tensile parameters increased with the increase in fiber content The content of 2.0 vol.% generated the best performance in terms of scc, ecc, spc and epc

B Energy parameters of HPFRCs

Table 4 gives the results of four energy parameters of

HPFRCs, including CE , CT , Ghd and Gel of HPFRCs These results were averaged from three specimens tested for each series Fig 5 graphically displays the comparisons of the

Trang 31

18

energy parameters of HPFRCs using different fiber contents

As can be seen in Fig 5, all the four energy parameters of

HPFRCs generally increased as fiber volume content

increased As the fiber volume content was changed from 0.5

to 2.0 vol.%, the range values of the energy parameters were

observed as follows: from 0.381 to 1.609 kJ/m2 for the CE ,

from 0.014 to 0.027 kJ/m2 for the CT , from 0.981 to 5.419

kJ/m2 for the Ghd, and from 0.019 to 0.051 kJ/m2 for the Gel

Regardless of fiber content, the CT was observed to be lower

than the Gel at the first crack At the post crack, the CE was

significantly lower than the Ghd This means the material

capability of HPFRCs was utilized significantly The ratio

Figure 5 Comparison of energy parameters of HPFRCs

Table 4 Energy parameters of HPFRCs

Fiber content

(vol.%)

CE

(kJ/m 2)

hd G

(kJ/m 2)

CT

(kJ/m 2)

el G

(kJ/m 2)

hd

G CE

el

G CT

0.5 0.381 0.981 0.014 0.019 2.6 1.3

1.0 0.579 3.324 0.014 0.027 5.7 1.9

1.5 0.862 4.086 0.018 0.049 4.7 2.8

2.0 1.609 5.419 0.027 0.051 3.4 1.8

Note: Definition of energy parameters can be referred to Fig.1

C Correlation between complementary energy and number

of microcracks in hardening stage of HPFRCs

As illustrated in Fig 1, multiple microcracks (N ) are cr

generated during the hardening stage According to Naaman [14], the average crack spacing (

av L

 ) of a strain hardening composite can be predicted using Eq (5) Eq (5) relates to a number of fibers within cross-section (Nf), which is possibly estimated using Eq (6) Finally, Ncr within the gauge length

of a tensile specimen can be obtained using Eq (7) Mathematically, Eq (7) describes a linear relationship between Ncr and fiber volume content (Vf)

of 1D, 2  for case of 2D, and 0.5 for the case of 1, 2 and 3D fiber orientation; Ag is the cross-section area of tensile specimens; L is the gauge length of tensile specimen;  is the crack spacing factor, its value ranging from 1 to 2 It is highlighted that the author investigated the number of cracks using experiment only and did not calculate the number of cracks through theoretical equations proposed by Naaman Since the ratio of the complementary energy to the crack tip toughness (CE CT ) of a composite represents capability /

of producing multiple microcracks (

cr

N ), in this section, the

ratio CE CT was correlated to / N of HPFRCs, which were cr

Generally, as the ratio CE CT is higher than 1, the multiple /microcracks possibly occur in the composite Kanda and Li [15] stated that the conditions for surely producing multiple microcracks are ratio CE CT >2.7 and ratio / spc/scc>1.3

Trang 32

Table 5 supplies the ratio CE CT and / N As shown in cr

Table V, the ratio CE CT increased with the increase in fiber /

content The value of CE CT was from 26.3 to 58.8 while /

the value of spc/scc was from 1.9 to 3.7 These ratios

completely satisfy the conditions according to Kanda and Li

[14] The value of N was observed from 2.00 to 16.67 cr

Table 5 Capability in producing multiple microcracks of HPFRCs

cr N

Figure 6 Photos of multiple microcracks of HPFRCs within

the gauge length

Figure 7 A linear relationship between ratio CE CT/ and

number of multiple microcracks of HPFRCs

Figure 8 A linear relationship between fiber content and

number of multiple microcracks of HPFRCs

A linear relationship was supposed in this study for ratio /

CE CT versus N and cr Vf versus

N response curve was performed in Fig 7 with the

regression function Eq (8) Similarly, the fiber volume content versus N response curve was shown in Fig 8 with cr

the regression function Eq (9) The regression functions are useful for the prediction work of microcrack number and ratio /

CE CT with a changed fiber volume content

- The complementary energy, crack tip toughness, and the ratio between them of HPFRCs clearly increased with increasing fiber volume content

- The hardening energy of HPFRCs was much higher than the complementary energy, regardless of fiber content This means the material capability in terms of energy absorption was utilized significantly Also, the elastic energy was higher than the crack tip toughness of HPFRCs

- Relationship of microcrack number versus ratio complementary energy to crack tip toughness as well as the relationship of microcrack number versus fiber volume content were analytically modelled based on the test result and regression analysis The regression functions are useful for the prediction work of microcrack number and complementary energy as the fiber volume content in HPFRCs is changed

ACKNOWLEDGMENT

This research was supported by Ho Chi Minh City University of Technology and Education, the authors are grateful to the sponsor The opinions expressed in this paper are those of the authors and do not necessarily reflect the views of the sponsor

REFERENCES

[1] D L Nguyen, J Song, C Manathamsombat, D J Kim,

“Comparative electromechanical damage-sensing behavior

of six strain-hardening steel-fiber-reinforced cementitious composites under direct tension”, Compos Part B, 69 (2015), pp 159–168

[2] D L Nguyen, G S Ryu, K T Koh, D J Kim, “Size and geometry dependent tensile behavior of ultra-high-performance fiber-reinforced concrete”, Composites: Part

B, 58 (2014), pp 279-292

[3] S H Park, D J Kim, G S Ryu, K T Koh, “Tensile behavior of Ultra-high Performance Hybrid Fiber Reinforced Concrete,” Construction and Building Materials,

2012, 34(2), pp 172-184

[4] K Wille, D J Kim, A E Naaman, “Strain hardening FRC with low fiber contents,” Mater Struct, 44 (2011), pp 583-598

Trang 33

UHP-20

[5] N T Tran, D L Nguyen, D J Kim, T T Ngo, “Sensitivity

of various fiber features on shear capacities of

ultra-high-performance fiber-reinforced concrete”, Magazine of

Concrete Research, Vol 74, No 4, 2022, pp 190-206

[6] V C Li, and H C Wu, “Conditions for Pseudo Strain

Hardening in Fiber Reinforced Brittle Matrix Composites”,

Journal of Applied Mechanics Review, Vol 45, No 8, 1992,

pp 390-398

[7] V C Li, and C K Y Leung, “Theory of Steady State and

Multiple Cracking of Random Discontinuous

Fiber-Reinforced Brittle Matrix Composites”, ASCE Journal of

Engineering Mechanics, Vol 118, No 11, 1992, pp

2246-2264

[8] V C Li, “On Engineered Cementitious Composites (ECC):

A Review of the Material and its Implications”, Journal of

Concrete Technology, Japan Concrete Institute, Vol 1, No

3, 2003, pp 215-230

[9] D B Marshall and B N Cox, “A J-Integral Method for

Calculating Steady-State Matrix cracking Stresses in

Composites”, Mechanics of Materials, North-Holland, No

7, 1988, pp 127-133

[10] A E Naaman, “Tensile strain-hardening FRC composites:

Historical evolution since the 1960”, Advances in

Construction Materials 2007, Springer Berlin Heidelberg,

pp 181-202, Stuttgart, Germany

[11] J Song, D L Nguyen, C Manathamsombat, D J Kim,

“Effect of fiber volume content on electromechanical behavior of strain-hardening steel-fiber-reinforced cementitious composites”, J Compos Mater 2015, doi:10.1177 /0 021998314568169

[12] D L Nguyen, M N -T Lam, D J Kim and J Song, “Direct tensile self-sensing and fracture energy of steel-fiber-reinforced concretes”, Composites: Part B 183 (2020)

107714, pp 1-19, doi:10.1016/j.compositesb.2019.107714 [13] V.C Li, S Wang, C Wu, Tensile strain-hardening behavior

of polyvinyl alcohol engineered cementitious composite (PVA-ECC), ACI Mater J., 98(6) (2001), pp 483-492 [14] Yoo, D.-Y., Kim, S.-W., & Park, J.-J (2017) Comparative flexural behavior of ultra-high-performance concrete reinforced with hybrid straight steel fibers Construction and Building Materials, 132, pp 219-229 doi:10.1016/j.conbuildmat.2016.11.104

[15] A E Naaman, “Ferrocement & laminated cementitious composites,” Techno Press 3000, Ann Arbor, Michigan,

2000

[16] T Kanda, V C Li, “Practical design criteria for saturated pseudo strain hardening behavior in ECC,” J Adv Concr Technol 2006, 4, p 59

Trang 34

A Study of the Scavenging Process in a Two-stroke Free Piston Linear Engine at Low Velocity Using CFD

and DPM

Nguyen Huynh Thi

Faculty of Vehicle and Energy

Engineering

Ho Chi Minh City University of

Technology and Education

Ho Chi Minh City, Vietnam

nguyenhuynhthi@tgu.edu.vn

Nguyen Van Trang

Faculty of Vehicle and Energy

Huynh Thanh Cong

Vietnam National University - Ho Chi

Minh City

Ho Chi Minh City, Vietnam htcong@hcmut.edu.vn

Dao Huu Huy

Faculty of Vehicle and Energy

Engineering

Ho Chi Minh City University of

Technology and Education

Ho Chi Minh City, Vietnam

dhhuy2310@gmail.com

Huynh Van Loc

Faculty of Industrial Engineering Tien Giang University

My Tho City, Vietnam

Truong Hoa Hiep

Faculty of Industrial Engineering Tien Giang University

My Tho City, Vietnam

Ngo Duc Huy

Faculty of Vehicle and Energy Engineering

Ho Chi Minh City University of Technology and

Education

Ho Chi Minh City, Vietnam

Vo Bao Toan

Faculty of Vehicle and Energy Engineering

Ho Chi Minh City University of Technology and

Education

Ho Chi Minh City, Vietnam

Abstract: A free-piston linear engine (FPLE) does not

use a crankshaft to control piston motion The gas exchange

and piston movement are closely related to each other and

directly affecting to the engine performance In this study, a

numerical simulation using Computational Fluid Dynamics

(CFD) and the Discrete Phase Model (DPM) has been

performed to investigate the scavenging process in a

two-stroke free piston linear engine during warm up The

characteristics of the reciprocating motion can be

determined based on the dynamics model and the piston

motion profiles are imported into commercial CFD software

(Ansys Fluent V.21) Both models have been applied the

initial conditions such as the velocity of the piston, piston

displacement, and inlet pressure to assess the effect of the

trapping efficiency The results show that the trapping

efficiency ±5% difference in the two models was able to

achieve at piston of 0.32 m/s – 1.25 m/s In addition, the

change in gas at each displacement position of the piston

and different inlet pressures is also shown through the

simulation results

Keywords: free piston linear engine, scavenge

efficiency, piston motion, Computational Fluid Dynamics

(CFD), Discrete Phase Model (DPM)

I INTRODUCTION

The free-piston engine generator (FPLE) is a linear

internal combustion engine that is removed the crank and

piston moves freely in the cylinder With the advantages of

compactness, high efficiency [1], variable compression ratio

should be suitable for many different fuels [2], reducing friction compared to conventional heat engines [3] Visibly, FPLE is a research trend to improve the performance of hybrid vehicles The FPLE considered in the present research is the two-stroke dual-piston type The piston assembly has a free linear motion between the top dead center (TDC) and bottoms dead center (BDC) and the piston assembly motion is controlled by gas and load forces acting upon it Cancelling the crank mechanism allows the piston

to move freely between the two cylinders, giving the engine the advantage of flexible characteristics, but also poses a challenge to the stability of the engine The destabilization here is controlling the position of TDC before the combustion process; different positions of TDC produce different end-compression pressure that affects the power of the engine There are so many related researches on the stability control of FPLE, and proposed various control methods [4-7] These studies focus only on controlling the motion of the piston Although considerable progress has been made, the way FPLE is controlled remains one of the problems preventing its commercialization Another factor

is the mass of air and fuel trapped inside the combustion chamber The trapped mixtures that are affected by the gas exchange process in there have scavenging process That can be key to realizing the engine's combustion efficiency and emissions potential [8] But the stability of gas exchange is unpredictable and difficult for measurement techniques

CFD (Computational Fluid Dynamics) is a very useful tool to analyze the exchange gas through the motion process

of FPLE as well as the scavenging process Blarigan et al.,

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22

at Sandia National Laboratories, studied the effects of

design parameters such as gas pressure in box, inlet

position, and tilt angle on scavenging efficiency and

trapping efficiency of FPLE through CFD [9] Their results

indicate that during the early stages of gas exchange, some

gas travels from the scavenging port to the exhaust port,

causing direct trapping losses Blarigan et al., at Sandia

National Laboratories They introduced a non-dimensionally

modeled piston movement configuration into the KIVA-3V,

simulating it to obtain the basic FPLE scavenging

performance with constant intake pressure using the model

CFD [10] The results show that a gas exchange system with

continuously low-rise pressure maximizes efficiency and

reduces unclean emissions In addition, several other studies

show that FPLE has a faster piston speed than a

conventional engine, which results in shorter gas exchange

duration of FPLE, lower scavenge efficiency but higher trap

efficiency [11-12]

The studies above show that the gas exchange process

has been simulated and optimized the effects of design

parameters to FPLE However, these studies omitted the gas

exchange in the start process of FPLE, this process usually

operates at low speed but must ensure the trapping

efficiency This study presents a CFD simulation to

investigate scavenging structure and parameters on the

FPLE gas exchange process The dimensional parameters

are chosen based on a prototype FPLE, the motion of the

free piston is built based on a dynamic model to calculate

the piston’s motion profiles In this study, the key

parameters such as displacement piston, operating

low-frequency and inlet pressure are inlet parameters Two

methods CFD and the Eulerian-Lagrangian discrete phase

model (DPM) are used to track the ratio of particles trapped

and escape from the cylinder then find out trapping

efficiency and compare the accuracy with each other

II MODELING AND SIMULATION

A Dynamic model

The mechanical forces acting on the piston include the

gas force in the left and right cylinder, mechanical friction

and inertia force, and traction of the actuator Piston

dynamics can be determined by Newton II's law

P cyl , P cyr is the pressure in the left and right cylinders; S

is the area of the piston crown F f is the friction force, m is

the mass of the translator, d 2 x/dt 2 is the acceleration of the

piston, F sl , F sr are respectively the spring forces in the left

and right Fst the force is received from the starting device

The velocity of piston is calculated by the equation:

In the actual model, the initial speed V0 is based on

the mechanical starter Fig 1 This speed is hindered by the

spring forces on the left or right The piston velocity of the

BDC to TDC form is determined by:

V = V0 − 𝐹.𝑡

Figure 1 A prototype of two-stroke free piston engine [15]

1- Cylinder 1; 2- Activation mechanism; 3- Compressor;

4-Carburetor, 5- Compressed air chamber; 6-Cylinder 2

B CFD model

The piston model and main parameters of FPLE are shown in Fig 2 and Table 1 The parameter of the FPLE is imported into commercial CFD software Ansys Fluent v.21

to define the calculating surfaces and volumes as well as to generate the mesh Then there is the meshing process, the cylinder mesh is generated in a multi-zone method, and the others have generated the mesh in the sweep method The velocity of the piston is calculated by a program written in Microsoft Visual C++ before importing it into the Ansys software as an input database, the input database is a user-defined function (UDF) In the dynamic mesh, the layering

is used to add or remove layers of cells according to the piston position In addition, the dynamic mesh changes according to the piston position to change the compression ratio, pressure The position of the piston can be changed step by step with a step of 0.5mm, from which it is possible

to control the pressure at the end of the compression stroke

in different locations

In order to investigate the effects of intake pressure on the scavenging process and the pressure at the end compression, the inlet pressures are adjusted from 1.05bar to 1.2bar; initial speeds are 0.32m/s and 1.25m/s The inlet and outlet temperatures are set at 300 K during the simulation process The inlet mixture is assumed to be an ideal gas In addition, the 𝑘 − 𝜀 turbulent model is employed to capture turbulence Input parameters are provided for the computational fluid dynamic (CFD) model to calculate the trapping efficiency In two-stroke, the trapping efficiency is defined as follows [13]:

t= mass of delivered fresh charge retained in cylinder

mass of delivered fresh charge through all scavenging ports

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Figure 2 a) Parameter of the FPLE, b) Computational mesh of the

Inlet pressure Pin (bar) 1.05 - 1.25bar

Inlet temperature Tin (K) 300K

The discrete Phase Model (DPM) is used to

co-track particles’ motion DPM is based on a

Euler-Lagrangian framework, the forces such as viscous drag, lift

force acting on the particles along their trajectories and

stochastic behaviour of the turbulent flow are taken into

account Based on tracking the particles throw discrete

phases in boundary areas to escape, trap and reflect Escape

condition is assumed in the inlet and outlet ports, the trap

condition is considered the cylinder and reflects condition is

being a wall of intake and exhaust pipes Fig 3 To shorten

the computational time and the approach become much

simpler, assumptions in particle motion calculations will be

simplified: all particles have the same size, and the flow

around the particles and particle-particle interaction is

neglected in the simulation In the Lagrangian reference

frame, the trajectory is predicted by integrating the force

balance on each individual particle and can be written as

where F is an additional acceleration (force/unit particle

mass) term; is the particle density and p is the continuum

phase density; u is the local fluid phase velocity and up is the

velocity of the particle phase, respectively; g is the gravity

of the particle The first item on the right is the drag force

per unit particle mass, r is the droplet or particle relaxation

time The initial parameters of the particle such as velocity,

mass flow inlet… similar to the CFD model; the trap

efficiency in the DPM is replaced by the number of

particles The trapping efficiency is defined: as the number

of particles entering the cylinder divided by the number of particles supplied from the scavenging ports

Figure 3 DPM calculation model III RESULTS AND DISCUSSION

A CFD simulation results

Pressure changes at the inlet port and open/closed position affect the scavenging process At an initial speed of 0.32m/s, the initial pressure gradually increases from 1.05bar to 1.2bar Trapping efficiency is increased but not significantly since the mass flow in/out of the cylinder is almost stable Fig 4 When the piston is close to fully closing the inlet, the mass flow drops suddenly at the 3.5 mm position and at the 4mm position the scavenge port fully close At 1.05bar pressure due to high mass flow at the scavenge port but at the exhaust mass flow no significant difference with the case other so trapping efficiency still tends to increase; at 1.1bar pressure due to mass flow at the scavenge port low but high mass flow at exhaust port making the exhaust port high so trapping efficiency still tends to reduce The flow velocity at the exhaust port is based on the flow velocity at inlet port, the flow velocity at the higher inlet the higher exhaust The results of the flow velocity simulation De = 0mm; De =2mm; De =3.5mm at 1.05bar Fig 6 and the rest of the cases are shown in Fig 7

Figure 4 Trapping efficiency from 1.05bar to 1.25bar

4045505560

1.05 bar 1.1 bar 1.15 bar 1.2 bar

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24

Figure 5 Mass flow versus piston displacement at piston speed

0.32m/s

Figure 6 Velocity Streamline at A) De = 0mm; B) De = 2mm; C)

De = 3.5mm with initial pressure = 1.05 bar and initial velocity of

piston = 0.32m/s

Figure 7 Flow velocity versus piston displacement at piston speed

of 0.32m/s When increasing the speed to 1.25m/s the trapping

efficiency increases at 1.05bar pressure, more mass flows

into the cylinder and out to the cylinder roughly equal to the

other pressure curves Through the two results, the speed of

0.32m/s still gives trapping efficiency higher than 1.25m/s,

the reason is a lot of new charge going out of the exhaust

port but new charge into cylinder low, as shown in the mass

flow Fig 8 and the velocity simulation De = 0mm; De

=2mm; De =3.5mm at 1.05bar Fig 9, the rest of the cases

are shown in Fig 10

Figure 8 Mass flow versus piston displacement at piston speed

1.25m/s

Figure 9 Velocity Streamline at A) De = 0mm; B) De = 2mm; C)

De = 3.5mm with initial pressure = 1.05bar and initial velocity of

in the cylinder, the number of trapped particles corresponds

to the amount that is lost through the exhaust port and trapped due to the obstruction of the piston wall at the scavenging ports Fig 12

Trang 38

Figure 11 Trapping efficiency from 1.05 bar to 1.25 bar (DPM)

Figure 12 A) Particle residence time at De = 0mm, B) Particle

residence time at De = 4mm, C) Particle residence time at De =

6mm With a low piston speed of 0.32m/s, the amount of

particles trapped in the cylinder is high and stable When the

scavenging ports are completely closed, the number of

trapped particles is reduced, causing large air escape

through the exhaust port Fig 13 With a piston speed of

1.25m/s, the fast-closing time of the scavenging ports causes

the number of particles not to catch up to the cylinder, but

the number of particles retained is higher due to the

fast-closing time of the exhaust port Fig 14 However, at

0.32m/s the trapping efficiency is still higher

Figure 13 Amount of particle versus piston displacement at piston

ACKNOWLEDGMENT

This work belongs to the project grant No:

B2019-SPK-08 funded by Ministry of Education and Training, and hosted by Ho Chi Minh City University of Technology and Education, Vietnam

[3] B Jia, R Mikalsen, A Smallbone, and A Paul Roskilly, “A study and comparison of frictional losses in free-piston engine and crankshaft engines,” Applied Thermal Engineering, 2018

[4] R Mikalsen, A.P Roskilly, The control of a free-piston engine generator Part 1: Fundamental analyses, Appl Energy, 87 (2010), 1273–1280

[5] R Mikalsen, A.P Roskilly, The control of a free-piston engine generator Part 2: Fig 15 In-cylinder gas pressure and temperature of each combustion duration C Yuan, et al Applied Thermal Engineering 173 (2020) 115201 10 Engine dynamics and piston motion control, Appl Energy, 87

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(2010), 1281–1287

[6] B.R Jia, Z.X Zuo, H.H Feng, G.H Tian, A Smallbone,

A.P Roskilly, Effect of closed-loop controlled resonance

based mechanism to start free piston engine generator:

simulation and test results, Appl Energy, 164 (2016), 532–

539

[7] B.R Jia, G.H Tian, H.H Feng, Z.X Zuo, A.P Roskilly, An

experimental investigation into the starting process of

free-piston engine generator, Appl Energy 157 (2015), 798–804

[8] Goldsborough SS, Blarigan P V Optimizing the scavenging

system for a two-stroke cycle, free piston engine for high

efficiency and low emission: A computational approach

SAE Paper 2003-01-0001, 2003

[9] A Sofianopoulos, Y.C Zhou, B Lawler, S Mamalis, Gas

exchange processes of a small HCCI free piston engine - A

computational study, Appl Therm Eng., 127 (2017), 1582–

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[10] S Goldsborough, P Blarigan, Optimizing the scavenging

system for a two-stroke cycle, free-piston engine for high

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[11] C Yuan, H Ren, X Jing, Comparison of the gas exchange

of a loop scavenged free piston engine alternator and the conventional engine, Appl Therm Eng., 127 (2017), 638–

649

[12] Nguyen Ba Hung, Sung Jaewon, Ocktaeck Lim (2017) A study of a scavenging process in a two-stroke free piston linear engine using CFD 9th International Conference on Applied Energy (pp 1354-1360) Cardiff, UK: Elsevier Ltd

[13] Grljuši´c, M.; Tolj, I.; Radica, G.; Sciubba, E An Investigation of the Composition of the Flow in and out of a Two-Stroke Diesel Engine and Air Consumption Ratio Energies 2017, 10, 1

[14] A Vakhrushev, M Wu, A Ludwig, G Nitzl, Y Tang, & G Hackl, “Verification of a Discrete Phase Model with Water-Particle Flow Experiments in a Tundish,” in 5th Int Conf

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[15] [N H Thi et al., "An Investigation on Power Generation Characteristics of Linear Generator Driven by a Free-piston Engine," 2021 International Conference on System Science and Engineering (ICSSE), 2021, pp 495-499, doi: 10.1109/ICSSE52999.2021.9538476

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Investigating the Relationship between Workers’

Needs and Commitments to Garment Enterprise

Tu Tran

Faculty of Fashion and Tourism

Ho Chi Minh City University of Technology and Education

Ho Chi Minh City, Vietnam camtuspkt@hcmute.edu.vn

Abstract: This paper analyzes the relationship between

workers’ needs and commitments to garment enterprises

Data are collected from the direct survey through the

questionnaire will determine the level of satisfaction of

garment workers’ needs based on the Hierarchy of Needs

(Maslow, 1943), and the commitment between the worker

and the garment enterprise Then, through statistical analysis

to review and test the influence of each factor on worker

commitment to the enterprise The research results show that

factors affecting workers’ commitment to garment

enterprises include: social needs; physiological needs related

to business policies and the lives of workers; safety and

respect needs

Keywords: needs of garment workers, commitments with

garment enterprises, social needs, physiological needs, safety

and respect needs

I INTRODUCTION

From the beginning of 2021 until now, textile and garment

enterprises have prospered in terms of orders and export

markets, so the need to recruit more workers is quite large

However, many businesses are currently facing difficulties in

recruiting and facing a shortage of human resources [1]

In the report on the recruitment demand for mid-and

senior-level personnel in the Vietnamese market in the first

quarter of this year, Navigos Search Company stated that the

effectiveness of Free Trade Agreements (FTAs), especially

EVFTA (FTAs) Vietnam - EU), although it has not been able

to offset the decrease in export turnover caused by Covid-19,

it has brought significant effects in increasing export orders

for textile and garment enterprises in Vietnam Besides, the

tense situation in Myanmar has caused more orders to flow to

Vietnam, leading to an increase in demand for positions in the

textile and garment industry These advantages have helped

recruitment demand in the textile industry increase by 50-60%

over the same period in 2020, especially for middle and senior

management positions However, according to the Vietnam

Textile and Apparel Association (Vitas), after the 2020 labor

cuts, the textile and garment industries are now struggling to

re-hire because of workers who have returned to their

hometowns or online selling [1]

In the labor structure of the garment industry, workers

account for the highest proportion and the job-hopping rate is

also high This study is conducted to help understand the

factors affecting the commitment between workers and

garment enterprises by surveying workers about their needs

and level of engagement with their company With the data obtained from the survey and through processing and analyzing statistical data, it is hoped that the research results will provide managers with a deeper insight into the factors that connect employees and businesses Thereby drawing out several measures and recommendations to help the manager have better human resource management policies to connect workers with their company, and improve labor fluctuations

in the garment enterprises

1 The scale of satisfaction of needs

Maslow's hierarchy of needs (Maslow, 1943) [2] is a motivational theory in psychology comprising a five-tier model of human needs, often depicted as hierarchical levels within a pyramid

From the bottom of the hierarchy upwards, the needs are: physiological (food and clothing), safety (job security), love and belonging needs (friendship), esteem, and self-actualization (presented in figure 1)

Figure 1 Maslow's hierarchy of needs (1943)

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