Bsi bs en 15167 2 2006

www bzfxw com BRITISH STANDARD BS EN 15167 2 2006 Incorporating Corrigendum No 1 Ground granulated blast furnace slag for use in concrete, mortar and grout — Part 2 Conformity evaluation The European[.]

Incorporating Corrigendum No 1

Ground granulated

blast furnace slag for

use in concrete, mortar

and grout —

Part 2: Conformity evaluation

The European Standard EN 15167-2:2006 has the status of a

British Standard

ICS 91.100.15

This British Standard was

published under the authority

of the Standards Policy and

Strategy Committee

on 31 October 2006

© BSI 2006

National foreword

This British Standard was published by BSI It is the UK implementation of

EN 15167-2:2006 Together with BS EN 15167-1, it supersedes BS 6699:1992 which will be withdrawn on 1 May 2008

The UK participation in its preparation was entrusted by Technical Committee B/517, Cement and lime, to Subcommittee B/517/4, Additions for concrete

A list of organizations represented on B/517/4 can be obtained on request to its secretary

This publication does not purport to include all the necessary provisions of a contract Users are responsible for its correct application

Compliance with a British Standard cannot confer immunity from legal obligations.

Amendments issued since publication

16764

Corrigendum No 1 31 October 2006 Correction to national foreword

EUROPÄISCHE NORM August 2006

ICS 91.100.15

English Version

Ground granulated blast furnace slag for use in concrete, mortar

and grout - Part 2: Conformity evaluation

Laitier granulé de haut-fourneau moulu pour utilisation dans

le béton, mortier et coulis - Partie 2: Evaluation de la

conformité

Hüttensandmehl zur Verwendung in Beton, Mörtel und Einpressmörtel - Teil 2: Konformitätsbewertung

This European Standard was approved by CEN on 26 June 2006.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member.

This European Standard exists in three official versions (English, French, German) A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.

EUROPEAN COMMITTEE FOR STANDARDIZATION

C O M I T É E U R O P É E N D E N O R M A L I S A T I O N

E U R O P Ä I S C H E S K O M I T E E F Ü R N O R M U N G

Management Centre: rue de Stassart, 36 B-1050 Brussels

Contents Page

Foreword 4

1 Scope 5

2 Normative references 5

3 Terms and definitions 5

4 Tasks for the manufacturer 8

4.1 Factory production control 8

4.1.1 Concept 8

4.1.2 Works' quality manual 8

4.1.3 Management systems 9

4.1.4 System of documentation 9

4.2 Internal quality control 10

4.2.1 Process control 10

4.2.2 Measuring and testing 10

4.2.3 Handling, storage, packaging and delivery 11

4.3 Autocontrol testing of samples 11

4.3.1 Sampling and testing 11

4.3.2 Corrective action 11

4.3.3 Measuring and test equipment for autocontrol testing 11

4.3.4 Quality records 12

5 Tasks for the certification body 12

5.1 General 12

5.2 Surveillance, assessment and acceptance of the production control 12

5.2.1 Inspection tasks 12

5.2.2 Frequency of inspections 12

5.2.3 Reports 12

5.3 Evaluation of the results of autocontrol testing of samples 12

5.3.1 Evaluation tasks 12

5.3.2 Number and timing of evaluations 13

5.3.3 Control period 13

5.3.4 Evaluation of test results 13

5.3.5 Reports 13

5.4 Audit testing of samples taken at the factory/depot and initial type testing 13

5.4.1 Sampling 13

5.4.2 Number of samples 13

5.4.3 Properties and test methods 13

5.4.4 Testing 14

5.4.5 Evaluation of test results 14

5.4.6 Reports 14

5.4.7 Proficiency testing 14

5.5 Initial inspection of the factory and the production control 14

5.5.1 Inspection of a new factory 14

5.5.2 Inspection of an existing factory 15

5.5.3 Criteria for the assessment of the production equipment 15

5.5.4 Criteria for the assessment of laboratories 15

5.5.5 Reports 15

5.6 Evaluation of test results during the initial period 15

5.6.1 Initial period 15

5.6.2 Evaluation of test results 16

5.6.3 Reports 16

6 Actions in the event of non-conformity 16

6.1 Actions to be taken by the manufacturer 16

6.2 Actions to be taken by the certification body 16

6.2.1 Following surveillance, assessment and acceptance of the production control (see 5.2) and evaluation of the results of autocontrol testing (see 5.3) 16

6.2.2 Following evaluation of the results of the audit testing of samples taken at the factory/depot (see 5.4 and Annex A) 16

7 Procedure for third party certification of conformity 17

8 Certificates of conformity and conformity mark 17

9 Requirements for dispatching centres 17

9.1 General requirements 17

9.2 Tasks for the intermediary 18

9.2.1 Measures to maintain the ground granulated blastfurnace slag quality 18

9.2.2 Confirmation autocontrol testing of samples taken at the dispatching centre 18

9.3 Tasks for the third party 18

9.3.1 Surveillance, assessment and acceptance of the measures to maintain the ground granulated blastfurnace slag quality and of the confirmation autocontrol 18

9.3.2 Audit testing of samples taken at the dispatching centre 19

9.3.3 Decisions to be taken 19

Annex A (normative) Evaluation of the representativeness and the accuracy of the 28 day activity index test results 22

A.1 General 22

A.2 Sets of results considered 22

A.3 Evaluation procedure 22

A.3.1 Introduction 22

A.3.2 Symbols 22

A.3.3 Evaluation of whether set A and set B belong to the same population (sampling error check) 23

A.3.4 Comparison between set B and set C in order to check the accuracy of the autocontrol testing (testing error check) 23

Bibliography 24

Foreword

This document (EN 15167-2:2006) has been prepared by Technical Committee CEN/TC 104

“Concrete and related products”, the secretariat of which is held by DIN

This European Standard shall be given the status of a national standard, either by publication of an

identical text or by endorsement, at the latest by February 2007, and conflicting national standards

shall be withdrawn at the latest by May 2008

The standard EN 15167, is composed of two parts:

 Part 1: Definitions, specifications and conformity criteria

 Part 2: Conformity evaluation

The preparatory work was carried out by WG15 of CEN/TC 104 since November 2003 in which the

following countries participated: Austria, Belgium, Czech Republic, Finland, France, Germany, Ireland,

Italy, Netherlands, Norway, Poland, Spain, Sweden, Switzerland and the United Kingdom

According to the CEN/CENELEC Internal Regulations, the national standards organizations of the

following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech

Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy,

Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia,

Slovenia, Spain, Sweden, Switzerland and United Kingdom

1 Scope

This European Standard specifies the scheme for the evaluation of conformity of ground granulated

blastfurnace slag according to EN 15167-1

The European Standard provides technical rules for the production control by the manufacturer,

including autocontrol testing of samples It also provides rules for actions to be followed in the event of

non-conformity, the procedure for the certification of conformity and requirements for dispatching

centres

The following referenced documents are indispensable for the application of this document For dated

references, only the edition cited applies For undated references, the latest edition of the referenced

document (including any amendments) applies

EN 196-1, Methods of testing cement — Part 1: Determination of strength

EN 196-7, Methods of testing cement — Methods of taking and preparing samples of cement

EN 15167-1:2006, Ground granulated blast furnace slag for use in concrete, mortar and grout — Part

1: Definitions, specifications and conformity criteria

3 Terms and definitions

For the purposes of this document, the following terms and definitions apply

3.1

autocontrol

continual statistical quality control of the ground granulated blastfurnace slag based on the testing of

samples taken by the manufacturer or their agent at point(s) of release from the ground granulated

blastfurnace slag factory

[EN 15167-1:2006]

NOTE This testing corresponds also to the “further testing of samples” mentioned in Annex III Section 2 point

(i) of the Construction Products Directive 89/106/EEC

3.2

certificate of conformity

document issued under the rules of a certain scheme for the evaluation of conformity indicating that

adequate confidence is provided that ground granulated blastfurnace slag is in conformity with

3.4

certification body

impartial body, governmental or non-governmental, possessing the necessary competence and

responsibility to carry out conformity certification according to given rules of procedure and

management

3.5

certified ground granulated blastfurnace slag

ground granulated blastfurnace slag for which a certificate of conformity has been issued

NOTE A single factory can manufacture more than one certified ground granulated blastfurnace slag, where

each is subject to separate autocontrol and declaration of conformity

3.6

confirmation autocontrol testing

continual testing carried out by an intermediary which consists of testing of samples taken by the

intermediary at the point(s) of release from the dispatching centre

bulk ground granulated blastfurnace slag handling facility (not located at the factory) used for the

dispatch of ground granulated blastfurnace slag (whether in bulk or bagged) after transfer or storage

where the manufacturer has full responsibility for all aspects of the quality of the ground granulated

blastfurnace slag

3.10

dispatching centre

bulk ground granulated blastfurnace slag handling facility (not located at the factory) used for the

dispatch of ground granulated blastfurnace slag after transfer or storage where an intermediary has

full responsibility for all aspects of the quality of the ground granulated blastfurnace slag

3.11

existing factory

factory which is already producing ground granulated blastfurnace slag certified under this scheme

3.12

factory production control

permanent internal control of ground granulated blastfurnace slag production exercised by the

manufacturer consisting of internal quality control and autocontrol testing

3.13

factory

facility used by a manufacturer for the production of ground granulated blastfurnace slag using

equipment which is suitable for continuous mass production of ground granulated blastfurnace slag, in

particular equipment for adequate grinding and homogenisation and the necessary silo capacity for

the storage and dispatch of each ground granulated blastfurnace slag produced This equipment and

the production control applied allow the control of production with sufficient accuracy to ensure that

the requirements of EN 15167-1 are met

impartial body having the organization, staffing, competence and integrity to perform according to

specified criteria functions such as assessing, recommending for acceptance and subsequent audit of

manufacturers’ quality control operations, and selection and evaluation of products on site or in

factories or elsewhere, according to specific criteria

[Construction Products Directive, 89/106/EEC]

3.16

intermediary

natural or legal person who takes from the manufacturer ground granulated blastfurnace slag certified

according to EN 15167-2 and bearing the conformity mark, who undertakes full responsibility for

maintaining in a dispatching centre all aspects of the quality of the ground granulated blastfurnace

slag and who supplies the ground granulated blastfurnace slag onwards to a further natural or legal

single result limit value

value of a mechanical, physical or chemical property which – for any single test result – in the case of

an upper limit is not to be exceeded or in the case of a lower limit is, as a minimum, to be reached

[EN 15167-1:2006]

3.21

specified characteristic value

characteristic value of a chemical or physical property which in the case of an upper limit is not to be

exceeded or in the case of a lower limit is, as a minimum, to be reached

[EN 15167-1:2006]

3.22

spot sample

sample taken at the same time and from one and the same place, relating to the intended tests It can

be obtained by combining one or more immediately consecutive increments (see EN 196-7)

[EN 15167-1:2006]

laboratory which measures, examines, tests, calibrates or otherwise determines the characteristics or

performance of materials or products

[Construction Products Directive, 89/106/EEC]

works’ quality manual

document providing information on the production control that a manufacturer applies at a particular

factory to ensure conformity of the ground granulated blastfurnace slag with the requirements of

EN 15167-1

4 Tasks for the manufacturer

4.1 Factory production control

4.1.1 Concept

Production control means the permanent internal control of ground granulated blastfurnace slag

production exercised by the manufacturer and consists of internal quality control (see 4.2) and

autocontrol testing1) of samples of ground granulated blastfurnace slag taken at the point of release

(see 4.3)

NOTE The requirements of EN 15167-2 as regards the production control take account of those clauses of

EN ISO 9001 which are relevant to the production, process control and testing of ground granulated blastfurnace

slag

4.1.2 Works' quality manual

The manufacturer's documentation and procedures for the production control shall be described in a

Works' quality manual, which shall adequately describe, among other things:

a) the quality aims and the organisational structure, responsibilities and powers of the responsible

staff with regard to product quality and the means to monitor the achievement of the required product quality and the effective operation of the internal quality control (see 4.1.3);

1) This testing corresponds also to the "further testing of samples" mentioned in Annex III Section 2 point (i) of

the Construction Products Directive 89/106/EEC

b) the production and quality control techniques, processes and systematic actions that will be used

(see 4.2.1, 4.2.3 and 4.3.2);

c) the inspections and tests that will be carried out before, during and after production, and the

frequency with which they will be carried out (see 4.2.2, 4.3.1 and 4.3.3)

The Works' quality manual prepared by the manufacturer for each factory shall include an adequate

system of documentation (see 4.1.4 and 4.3.4)

The Works' quality manual shall address and document the procedures operated to ensure that the

ground granulated blastfurnace slag conforms to the technical specifications The manual may

reference associated documents which provide further details of the autocontrol testing of samples

and the internal quality control For the purpose of this scheme, the term Works' quality manual shall

be considered to include these associated documents

NOTE In the case of an existing quality management system according to EN ISO 9001, the certification

body may examine if the corresponding quality manual meets all the requirements of EN 15167-1 which are

relevant to the production control of ground granulated blastfurnace slag Provided all the requirements are

included, this quality manual may also be applied for product certification

The Works' quality manual shall include a statement by the management of the manufacturer defining

its quality policy, objectives and commitments to the attainment of product quality

4.1.3 Management systems

4.1.3.1 Management representative

The manufacturer shall appoint a management representative who, irrespective of other

responsibilities, shall have defined authority and responsibility for ensuring that the requirements of

this European Standard for the evaluation of conformity are implemented and maintained

4.1.3.2 Internal audits and management review

In order to ensure the continuing suitability and effectiveness of the Work’s quality manual to meet the

requirements of EN 15167-1, the manufacturer shall perform at least once per year:

a) internal audits covering the scope of Clause 4 and 6.1;

b) management review of the production control, taking into account records of the internal audits

4.1.3.3 Training

The Works' quality manual shall describe the measures taken to ensure that all the personnel

involved in operations that can affect internal quality control and product quality have appropriate

experience or training Appropriate records shall be retained

4.1.4 System of documentation

4.1.4.1 Document control

The management representative of the manufacturer shall be responsible for the control of all

documents and data related to the production control and to this scheme for the evaluation of

conformity

This control shall ensure that the appropriate issues of all documents are available at essential

locations, that obsolete documents are withdrawn and that changes or modifications to any document

are effectively introduced

A master list shall be established to identify the current version of documents in order to prevent the

use of non-applicable documents

4.1.4.2 Quality records

The manufacturer shall retain records of production control for at least the period required to comply

with relevant legislation

4.2 Internal quality control

4.2.1 Process control

4.2.1.1 General

The Works' quality manual shall describe the parameters for process planning, process control and

testing, inspection, corrective action, verification, dispatch and the associated records

Where a factory uses more than one source of granulated blastfurnace slag, measures shall be

provided for them to be separately and adequately stored, and for controlled proportioning and

homogenisation

Where a factory produces more than one certified ground granulated blastfurnace slag, measures

shall be provided to store each product separately, enabling proper sampling, identification and

despatch

4.2.1.2 Constituents and composition of ground granulated blastfurnace slag

The manufacturer shall establish documented procedures and appropriate test methods to ensure

that the constituents meet the requirements of EN 15167-1 and are suitable to enable ground

granulated blastfurnace slag to be produced meeting the technical specification The following shall

be part of this documentation:

a) the source of the granulated blastfurnace slags;

b) confirmation that the granulated blastfurnace slags and any grinding aids are in accord with

Clause 4 of EN 15167-1:2006

NOTE X-Ray Diffraction or optical-microscopy may be used to assess the content of glassy material in

granulated blastfurnace slag

4.2.1.3 Control of off-specification production

The Works' quality manual shall contain procedures to ensure that off-specification production is

adequately managed

4.2.2 Measuring and testing

4.2.2.1 Inspection, measuring and test equipment

The equipment for in-process inspection and testing shall be regularly checked and calibrated in

accordance with the procedures and frequencies laid down in the Works' quality manual

4.2.2.2 Inspection and test status

Procedures for the inspection and test status through the stages of production shall be detailed in the

Works' quality manual These shall include procedures for the control of off-specification intermediate

materials

For the manufacturer’s control of the grinding process, spot samples for the determination of fineness

should be taken at an appropriate point that is between the grinding equipment and the storage silos

4.2.3 Handling, storage, packaging and delivery

The Works' quality manual shall describe the precautions taken for the protection of the quality of the

ground granulated blastfurnace slag while under the responsibility of the manufacturer It shall include

a description of the procedures used at depots Delivery documentation shall allow traceability to the

producing factory

4.3 Autocontrol testing of samples

4.3.1 Sampling and testing

The manufacturer shall operate a system of autocontrol testing for each certified ground granulated

blastfurnace slag This system shall be used to demonstrate conformity to the requirements in

Clause 8 of EN 15167-1:2006 The properties to be tested, the testing methods, the minimum

frequency of autocontrol testing during routine testing and initial period of testing and the conformity

criteria shall be in accordance with the requirements given in Clause 8 of EN 15167-1:2006 For

ground granulated blastfurnace slags not being dispatched continuously, the frequency of testing and

the point of sampling shall be as specified in the Works' quality manual

All test data shall be documented

4.3.2 Corrective action

The Works' quality manual shall document procedures for the review and adjustment of the

production control in case of non-conformity (see 6.1)

The actions taken in the event of non-conformity shall be recorded in a report subject to inspection

during the management review

In the event of ground granulated blastfurnace slag yielding a test result not conforming to the single

result limit value conformity criteria specified in EN 15167-1, the manufacturer shall immediately

determine the affected quantity, take appropriate action to prevent the dispatch of this quantity and

inform the affected customer if such ground granulated blastfurnace slag has been released In

addition, the manufacturer shall immediately determine the causes of such non-conformity, take

corrective actions and undertake a review of all relevant production control procedures All such

actions and findings shall be appropriately recorded in a report subject to inspection during the

management review

NOTE The certification body may require to be kept informed of these actions and findings

4.3.3 Measuring and test equipment for autocontrol testing

The equipment used for autocontrol testing shall be regularly checked and calibrated in accordance

with procedures and frequencies laid down in the Works' quality manual These procedures may

include comparison of strength test results by proficiency testing with another laboratory designated in

the Works' quality manual

The Works' quality manual shall document procedures to ensure that all personnel involved in

autocontrol testing have appropriate experience and training Appropriate records shall be retained

4.3.4 Quality records

The manufacturer shall retain records of the autocontrol test results and appropriate records on test

equipment for at least the period required to comply with relevant legislation

5 Tasks for the certification body

5.1 General

The certification body (see 3.4) has responsibility for three separate functions - certification, inspection

and testing These three functions may be carried out by one body or by more than one body The

inspection function may be carried out by an inspection body (see 3.15) and the testing function by a

testing laboratory (see 3.24) Reference to the certification body includes reference to any sub-bodies

it has

5.2 Surveillance, assessment and acceptance of the production control

5.2.1 Inspection tasks

The inspection tasks include surveillance, assessment and acceptance of the production control

operated by the manufacturer Inspection shall include checking that any major change in the Works'

quality manual, relevant to the production control of ground granulated blastfurnace slag, has been

reported to the certification body by the manufacturer within one month of its implementation

Inspection shall verify that the production control complies with the requirements as described in

Clause 4 and has been carried out according to the Works' quality manual

5.2.2 Frequency of inspections

The inspections shall normally be carried out at least once per year and the certification body shall

inform the manufacturer in advance when an inspection is to be made

5.2.3 Reports

Following each inspection, a confidential report shall be prepared and sent to the manufacturer

The manufacturer shall, if appropriate, advise the certification body of any corrective actions taken or

planned to be taken following receipt of the report

The certification body shall then make a decision on its final assessment

5.3 Evaluation of the results of autocontrol testing of samples

5.3.1 Evaluation tasks

Surveillance, assessment and acceptance of the production control includes evaluation of the test

results of the manufacturer's autocontrol testing to check conformity to the statistical conformity

criteria and single result limit values in EN 15167-1