Tiêu chuẩn iso 03216 1997 scan

Foreword IS0 the Interna tional O rga niza tion f or S ta nda rdization is a worldwide fed- a nd non-governmental, in la ison with ISO , also ta e pa rt in the work.. IS0 c ola borates c

STA NDA RD

19 7-0 -01

Huie es entiele de ca nneler, typ Chine (Cin amomum a roma tic rn

Foreword

IS0 (the Interna tional O rga niza tion f or S ta nda rdization) is a worldwide fed-

a nd non-governmental, in la ison with ISO , also ta e pa rt in the work IS0

c ola borates c losely with the Interna tiona l Elec trotec hnic al Commis ion

(IEC ) on a ll maters of elec trotec hnical sta nda rdiza tion

c ircula ted to the memb r b dies f or votin Publcation as an Interna tiona l

Stan ard req ires a pprova l by a t lea st 7 % of the memb r b dies c astin

a vote

lSO/ T C 5 , Es ential ois

T his sec on edition c anc els an re lac es the first edition (IS0 3 16:19 4)

whic h has b en tec hnic aly revised

Annexes A an B of this Interna tional Stan ard a re for information only

0 IS0 197

All rig ts re erved Unle s oth rwis spec ifie , n pa rt of this publc atio may be

repro uc ed or utiz d in an form or by an mean , elec tro ic or mec hanic al inc lu in

ph toc opyin a nd microfim, with ut permisio in writin fom th publser

Interna tio a l O rganizatio f or Stan ardizatio

Cas Po tale 5 l C H-121 Ge eve 2 l Switz rlan

Intern t c entalQis c h

x 40

c=c ; a 40 n t; p is ; o=is c ; s=c ental

Printe in Switz rlan

O il of c assia, Chinese type (Cinnamomum arornafkurn

rela tive den ity at 2 “C (R eferenc e method)

T his Interna tiona l Stan ard sp c ifies certa in charac -

teristic s of the oi of c as ia, C hinese ty pe (Cin amomum

Blume) in order to fa cilta te as es ment of its q a lity

refra ctive in ex

IS0 8 5:19 1, Es ential ois - Evaluation of misc i-

bi ty in etha nol

IS0 12 2:19 3, Es ential ois - Determination of the

ac id value

throu h referenc e in this tex t, con titute provision

agre ments b sed on this Interna tiona l Stan ard a re

enc ouraged to in estigate the p s ibi ty of a ply in

curently vald Interna tiona l Stan ard

IS0 1 0 4-I :- 31, Es ential ois - Genera/ g idanc e

c hromatogra hic profies f or presenta tion in sta n-

dard

on c hromatogra hic profies - Part 2: Uti za tion of

ois

IS0 1 0 5:- 3) O il of c as ia, C hinese ty pe - Deter

c hromatogra hic method on ca pi a ry c olumn

3 Definitio

IS0 212:19 3, Es ential ois - Sampln

For the purp ses of this Interna tiona l Stan ard, the

1) T o b publsh d (R ev isio of IS0 210:19 1)

2) T o b publsh d (R ev isio of IS0 21 : 9 1)

3) T o b publsh d

3.1 oi of c as ia, Chinese ty pe: Es ential oi

o tained by ste m disti a tion of the le v es, lea f

mainly growin in the South of C hina

Mo ie lq id

4.2 C olo r

C ha rac teristic, resembln odour of c in amaldehy de

4.4 R elativ e den ity at 2 “C / 20 “C

Minimum: 1,0 2

Minimum: 1,6 0 0

2 “C s a ll b req ired to give a cle r solution with

1 v olume of es ential oi

4.7 Ac id v alue

c in amaldehy de

Analy sis of the es ential oi s a ll b ca rried out by

s own in ta le 1 s a ll b identified T he pro ortion

of these c omp nents, in ic a ted by the integra tor,

s a ll b as s own in ta ble 1 T his c on titutes the

c hromatogra hic profie of the es entia l oi

T able 1 - Chromato ra hic profie

Comp n nt

Van -C in amaldehy de

-

0,5

C oumarin

1,5

4

O -Methoxy c in amy l ac etate

-

2

Ben aldehy de

0,5

2

-

O ,l

Salc y lic aldehy de

0

1

Pheny lethy l alc ohol

-

0,5

C in amy l ac etate

-

6

C in amic a lcohol

-

1

Sty rene

-

0,15

Pheny lethy l aldehy de

-

0,7

c is-C in amaldehy de

-

a 7

NOT - T he c hromatogra hic prof ile is normative, c on-

tra ry to ty pic a l c hromatograms given f or informa tion in

an ex A

Information on the fla shp int is given in an ex B

NOT - T his v olume alows e c h of the tests sp c ified

in this Interna tiona l Stan ard to b ca rried out a t le st

onc e

6 T est meth ds

2 9

6.2 R efra c tiv e in ex a t 2 “C

6.4 Acid v alue

Test p ortion: ‘I2 g to I5 g

R ela tiv e

M, = 13 ,2

c lumn

storage

Annex A

Pe k identifica tion

O pera tin c on ition

Column: fu e si c a c api ary ; le gth 5 m; diameter

2 Salc y lic ald hyd

3 Aceto h n n

4 Ph nylethyl alc oh l

5 tra sCin amald hyd

6 Cin amic alc oh l

7 Eu e ol

8 Coumarin

9 Cin amyl acetate

10 cis-0meth x cin amald hyd

4

Statio ary p ase: p ly dimethyl sioxa e (OV 101)

Ov n temp rature: from 10 “C to 2 0 “C at a rate

of 3 Wmin

Injec tor temp rature: 2 0 “C

Detector temp rature: 2 0 “C

Detector: flame io izatio

C arier gas: nitroge

C arier gas flow rate: n t k nown

V olume injecte : a out 0.2 ~1

Splt ra tio: l/l 0

4

Pe k id ntifica tio

2 Aceto h n n

3 S a lic ylc ald hyd

4 Ph nylethyl a lco ol

5 tra s-Cin am ald hyd

6 Cin am yl acetate

7 Eu e ol

8 Cin amic alco ol

9 Vans-O -M eth x cin amald hyd

10 Coumarin

1 O -M eth x cin am yl a cetate

Colum n: fu e si c a c a pi a ry; le gth 5 m; diam eter 0,2 mm

Sta tio a ry p ase: p lyethyle e gly ol 2 0 0 (CWA X 2 M)

Ov n tem perature: 5 “C for 3 m in, th n up to 19 “C a t a ra te of I4 “Urnin

Injec tor tem perature: 2 0 “C

Detector tem perature: 2 0 “C

D etector: flam e io iza tio

C a rrier gas: hydroge

Injecte v lum e: n t k own

C a rrier gas flow ra te: 1 m l/m in

C hart sp e : 0,2 cm /m in

6

8

9

0

1

Fig re A.2 -Ty pic a l c rom atogram ta en on a p la r colum n

Annex B

servic es, etc req ire information a out the fla sh-

p int of es entia l ois, whic h in most cases a re

sta ndardiza tion purp ses, given tha t

-

es entia l ois a re varied an their c hemic al c om-

p sition diff er to a la rge ex tent

-

price of es ential ois;

-

satisfy the desired o jec tive, but u ers c an ot

b o lged to u e one ty pe of eq ipment ra ther

than another

C on eq ently , it was dec ided to give a me n value

interested pa rties

o tained s ould b sp c ified

For further information, se ISO/ T R 1 018 4)

NOT - T he lower value was o ta ined with “L uc haire”

4) lSO/T R 1 018:19 7, Es e tial ois.- Ge eral g id nce o th d termin tio of flash oint

6

K S 71.10 60

De c riptors: fuit a nd veg ta le pro uc ts, e s ntial ois, c in amo ,

casia, spec ific atio s, c harac teristic s, c emical c mpo itio ,