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Our most striking observation was that expression changes of genes involved in b-oxidation of fatty acids and glucose metabolism differentiate adaptive from maladaptive hypertrophy.. DNA

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expression between exercise-induced cardiac effects and maladaptive cardiac hypertrophy

Claes C Strøm1, Mark Aplin1, Thorkil Ploug2, Tue E H Christoffersen1, Jozef Langfort3,

Michael Viese2, Henrik Galbo2, Stig Haunsø1and Søren P Sheikh1

1 CHARC (Copenhagen Heart Arrhythmia Research Center), Department of Medicine B, H:S Rigshospitalet, University of Copenhagen Medical School, Denmark

2 Copenhagen Muscle Research Centre, Department of Medical Physiology, Panum Institute, University of Copenhagen, Denmark

3 Laboratory of Experimental Pharmacology, Polish Academy of Science, Warsaw, Poland

Keywords

adaptive; DNA microarray; gene expression;

hypertrophy; maladaptive

Correspondence

S P Sheikh, Laboratory of Molecular

Cardiology, Department of Medicine B,

H:S Rigshospitalet, University of

Copenhagen, 20 Juliane Mariesvej,

DK-2100 Copenhagen, Denmark

Fax: +45 3545 6500

Tel: +45 3545 6730

E-mail: sheikh@molheart.dk

(Received 10 October 2004, revised 15

March 2005, accepted 22 March 2005)

doi:10.1111/j.1742-4658.2005.04684.x

While cardiac hypertrophy elicited by pathological stimuli eventually leads

to cardiac dysfunction, exercise-induced hypertrophy does not This sug-gests that a beneficial hypertrophic phenotype exists In search of an under-lying molecular substrate we used microarray technology to identify cardiac gene expression in response to exercise Rats exercised for seven weeks on a treadmill were characterized by invasive blood pressure mea-surements and echocardiography RNA was isolated from the left ventricle and analysed on DNA microarrays containing 8740 genes Selected genes were analysed by quantitative PCR The exercise program resulted in car-diac hypertrophy without impaired carcar-diac function Principal component analysis identified an exercise-induced change in gene expression that was distinct from the program observed in maladaptive hypertrophy Statistical analysis identified 267 upregulated genes and 62 downregulated genes in response to exercise Expression changes in genes encoding extracellular matrix proteins, cytoskeletal elements, signalling factors and ribosomal pro-teins mimicked changes previously described in maladaptive hypertrophy Our most striking observation was that expression changes of genes involved in b-oxidation of fatty acids and glucose metabolism differentiate adaptive from maladaptive hypertrophy Direct comparison to maladaptive hypertrophy was enabled by quantitative PCR of key metabolic enzymes including uncoupling protein 2 (UCP2) and fatty acid translocase (CD36) DNA microarray analysis of gene expression changes in exercise-induced cardiac hypertrophy suggests that a set of genes involved in fatty acid and glucose metabolism could be fundamental to the beneficial phenotype of exercise-induced hypertrophy, as these changes are absent or reversed in maladaptive hypertrophy

Abbreviations

ACE, angiotensin converting enzyme; ALP, actinin a2 associated LIM protein; EST, expressed sequence tag; FABP4, fatty acid binding protein 4; FACL, fatty acid CoA ligase; FDR, false discovery rate; GCKR, glucokinase regulatory protein; HR, heart rate; LVEDP, left ventricular end diastolic pressure; MAP, mean arterial pressure; MBE, model based expression; MYL, fast myosin alkali light chain; PCA, principal component analysis; PDC, pyruvate dehydrogenase complex; PDP, pyruvate dehydrogenase phosphatase; Slc27a1, fatty acid transport protein 4; UCP2, uncoupling protein 2.

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Heart disease is a leading cause of death in the

West-ern world and is commonly associated with cardiac

hypertrophy Sustained cardiac hypertrophy leads to

cardiac dysfunction, heart failure, arrhythmia and

sudden death As a result, cardiac hypertrophy is an

independent risk factor for cardiac morbidity and

mortality [1]

Exercise-induced cardiac hypertrophy is distinct

from the hypertrophy seen in different pathological

settings, as it is not accompanied by cardiac

dysfunc-tion or increased morbidity [2,3] This intriguing

dis-tinction has led to the concepts of maladaptive and

adaptive forms of cardiac hypertrophy While gene

expression changes in maladaptive cardiac hypertrophy

have been extensively investigated, much less is known

about transcriptional regulation in exercise-induced

hypertrophy Identification of a set of genes unique to

this condition would enhance our understanding of the

molecular differences between maladaptive and

adap-tive cardiac hypertrophy

Exercise training increases the functional capacity of

the cardiovascular system The adaptations include

increases in cardiac mass and dimension, maximum

oxy-gen consumption and coronary blood flow [4] Also,

exercise results in a balanced growth of cardiomyocytes

with normal myofibril to mitochondrial ratio [5,6] In

the setting of maladaptive hypertrophy, a shift from

fatty acids to glucose as the main fuel in the

myocar-dium has been described, and is in part caused by

down-regulation of gene products involved in b-oxidation of

fatty acids [7] Whether this metabolic shift also occurs

in adaptive hypertrophy remains to be established

Although the physiological and morphological

chan-ges during cardiac adaptations to exercise are well

characterized, little is known about the underlying

molecular changes

Evidence that adaptive and maladaptive hypertrophic

cardiac phenotypes result from activation of distinct

sig-nalling pathways has come from studies demonstrating

that exercise-induced hypertrophy is not prevented by

angiotensin II receptor blockade or cyclosporine

treat-ment [8,9] Also, several authors have demonstrated that

expression of marker genes including atrial natriuretic

peptide, myosin heavy chain isoforms and thyroid

hormone receptor isoforms differ between adaptive

and maladaptive hypertrophy [10–12] A comprehensive

analysis of the gene expression changes in

exercise-induced cardiac hypertrophy, however, is lacking Such

an approach may identify shared and divergent

mole-cular networks between adaptive and maladaptive

hypertrophy and point to new therapeutic strategies

The microarray technology allows simultaneous

analysis of the expression level of thousands of genes

making this technology well suited for comprehensive analysis of gene expression changes in response to phy-siological challenges DNA microarrays have been use-ful in analysis of cellular responses to stimuli, animal models of human disease and cancer classification [13,14]

We used DNA microarrays to define gene expression changes that characterize exercise-induced cardiac hypertrophy We identified 305 genes with differential expression in response to cardiac exercise, the majority

of which have not previously been associated with exercise The most directly interpretable and poten-tially biologically important finding was a reversed metabolic shift in response to exercise suggesting that genes involved in fatty acid and glucose metabolism are key regulatory points that distinguish adaptive beneficial hypertrophy from more adverse maladaptive forms elicited by pathological stimuli

Results

Physiological response to exercise Several pieces of data indicated that exercised rats had cardiac hypertrophy as compared to the sedentary con-trol animals First, training resulted in an  25% increase in left and right ventricular masses when nor-malized to lean body weight (Table 1) and a 10% increase when compared to tibial length (data not shown) Other organ weights were unchanged (lungs, kidney and stomach) after normalization (Table 1) Absolute cardiac weights were increased but not signi-ficantly, while other organ weights were significantly

Table 1 Organ weights Values are mean ± SEM Weights (W) of heart (H), left ventricle (LV), right ventricle (RV), lungs (P), kidney (K) and stomach (S) divided by lean (L) body (B) weight (mgÆg 0.78 )1).

*P < 0.05.

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reduced A less intense training protocol resulted in

significant body weight reductions but no increase in

ventricular weights (data not shown) Secondly,

echo-cardiographic examination of the cardiac phenotype

revealed that exercised rats had increases in both left

ventricular wall thickness and left ventricular cavity

dimensions (Table 2) Anterior and posterior wall

thicknesses were both increased by 14% and left

ven-tricular area indexed to lean body mass increased 9%

Cardiac function at rest, as determined by fractional

area of change (Table 2), left ventricular end diastolic

pressure (LVEDP), and maximal rate of isovolumetric

pressure development and decay (Table 3), was

identi-cal in the two groups, which is consistent with

pre-vious findings [15] Mean arterial pressure showed

no differences between exercised and sedentary rats

(Table 3), but resting heart rate decreased 10% in

response to exercise The decrease in resting heart rate

probably results from an increase stroke volume and

increased parasympathetic tone

Thus, our exercise protocol resulted in a phenotype

of eccentric hypertrophy without impairment of

car-diac function

Distinct global gene expression profiles between

exercised and sedentary animals

We first analysed the data for differences in global

gene expression patterns between exercised and

con-trol animals using a principal component analysis

(PCA) This type of analysis serves to reduce the

number of variables in multivariate data with mini-mal loss of information The PCA analysis based on all 8740 genes clearly distinguished the gene expres-sion profiles of hearts of exercised animals from those of controls (Fig 1) This finding indicated the existence of a distinct gene expression program induced by exercise

Identification of individual genes that are differentially expressed in response to exercise Next, individual genes regulated by exercise were iden-tified as described in Experimental procedures (Fig 2) The vast majority of genes were unchanged At the applied threshold [predefined to a false discovery rate (FDR) of 5% or less], 329 genes were identified as dif-ferentially regulated in response to exercise (marked with grey in the figure) Of these, 267 genes were upregulated while 62 genes were downregulated The upregulated genes represented 179 known genes, 66 expressed sequence tags (EST) and 22 replicate genes Among the downregulated genes were 43 known genes,

17 ESTs and two replicate probe sets A subgroup of the genes is listed in Table 4 and the full list of genes

is given in supplementary Table S1

To demonstrate the specificity of the gene expression changes, we randomly divided samples into two groups

of equal size and repeated the SAM analysis (see Experimental procedures) This procedure was repeated

Table 2 Echocardiography Values are mean ± SEM AWT,

Anter-ior wall thickness; PWT, posterAnter-ior wall thickness; d, diastole; LVA,

left ventricular area; BW, lean body weight; FAC, fractional area of

shortening.

AWTd

(cm)

PWTd (cm)

LVAd ⁄ BW (mm 2 Æg)0.78)

FAC (%) Exercised 0.205 ± 0.007* 0.195 ± 0.007* 4.97 ± 0.12* 77 ± 1

Sedentary 0.180 ± 0.003 0.171 ± 0.004 4.57 ± 0.09 78 ± 1

*P < 0.05.

Table 3 Left ventricular pressures Values are mean ± SEM.

dP ⁄ dt-max, Maximal rates of isovolumetric pressure development;

dP ⁄ dt-min, maximal rates of isovolumetric pressure decay.

LVEDP

(mm Hg)

dP ⁄ dt-max (m HgÆs)1)

dP ⁄ dt-min (mHgÆs)1)

MAP (mm Hg)

HR (min)1)

Exercised 6.0 ± 0.7 7.9 ± 0.3 ) 10.1 ± 0.4 113 ± 2 347 ± 8*

Sedentary 4.1 ± 0.5 9.3 ± 0.6 ) 11.0 ± 0.6 111 ± 6 383 ± 9

*P < 0.05.

Fig 1 Global gene expression in the hearts of exercised rats is dif-ferent from that of sedentary controls A principal component analy-sis was performed on all genes (n ¼ 8740) to find trends in the microarray data The two first components (PC1 and PC2) from the analysis are shown in the figure Exercised rats clearly cluster sep-arate from the sedentary controls indicating the existence of a dis-tinct gene expression program induced by exercise.

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several times No genes were identified as differentially

expressed in the randomized data sets as shown in

Fig 3

Confirmation of differential expression of

selected metabolic genes by quantitative PCR

From the interesting metabolic genes, six were chosen

for validation by quantitative PCR analysis CD36,

fatty acid binding protein 4 (FABP4), fatty acid

trans-port protein (Slc27a1), and glucokinase regulatory

pro-tein (GCKR) were upregulated and uncoupling propro-tein

2 (UCP2) was downregulated confirming the DNA

microarray data (Fig 4) Expression of fatty acid CoA

ligase (FACL) was not significantly upregulated in the

quantitative PCR analysis of exercise-induced

hyper-trophy

Expression of selected genes in maladaptive

hypertrophy

To compare expression of CD36 and UCP2 in

adap-tive and maladapadap-tive hypertrophy we analysed

expres-sion of CD36 and UCP2 in the noninfarcted region of

the left ventricle 3 weeks after myocardial infarction

as compared to sham-operated animals Contrary to

adaptive hypertrophy, where CD36 was upregulated

and UCP2 downregulated, CD36 expression was

unchanged and UCP2 expression increased (26%) in

maladaptive hypertrophy (Fig 5)

Discussion

In this work, we present a comprehensive analysis of transcriptional changes in response to exercise-induced cardiac hypertrophy, thereby for the first time provi-ding an overview of molecular clues to the adaptive cardiac phenotype We identified a distinct global gene expression pattern of myocardium adapting to the physiological challenge of exercise, and statistical ana-lysis identified 267 upregulated and 62 downregulated gene transcripts, providing a host of potential novel diagnostic and therapeutic targets for further investiga-tion

The exercise resulted in a relatively small increase in left ventricular mass (6%), which was in the same range as that found by others after isotonic exercise [10,16] When normalized to body weight or tibial length the increase in left ventricular mass was larger and significant Taken together with the fact that the absolute weights of all other organs were significantly reduced in the exercised animals, these data do support that the exercise regime elicited cardiac hypertrophy The reduction in body weight seen in the exercised animals most likely resulted from a combination of reduced body fat and growth retardation In line with this, a pilot series of less intense exercise resulted in a reduction in body weight (exercise 313 g vs sedentary

403 g), concurrent reductions in absolute cardiac weights, and no hypertrophy after normalization to body weight or tibial length

Fig 2 Identification of differentially

expres-sed genes A scatter plot of the observed

relative difference in gene expression vs.

the expected difference based on

permuta-tion of samples At the solid line, observed

values are identical to expected values The

applied threshold (delta ¼ 1.20) is shown as

dotted lines Corresponding values of

signifi-cance threshold (delta), FDRs, number of

genes identified as differentially expressed

and the expected number of false positives

are listed in the lower right quadrant.

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Table 4 Expression changes in response to exercise Gene names are listed with GenBank accession number; SAM score, fold change (FC) and P-values calculated by a Welch t-test are listed for comparison.

Metabolism

Extracellular matrix

Cytoskeletal

Non-muscle myosin alkali light chain, new-born, heart ventricle (MYL4) S77858 4.1 1.2 2.08E-03

Growth

Inflammation

Signalling

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Overall, gene expression patterns in adaptive cardiac

hypertrophy were quite similar to previously published

data from maladaptive cardiac hypertrophy A general

upregulation of signalling, cytoskeletal and extracellular

matrix genes was evident and the isoform shifts in

sarcomeric proteins resembled those of maladaptive

hypertrophy The most prominent difference from the

maladaptive response was differential expression of a set

of metabolic genes not previously associated with

exer-cise-induced cardiac hypertrophy While

downregula-tion of genes involved in lipid oxidadownregula-tion is typical of

maladaptive hypertrophy, we found upregulation of

sev-eral of these genes in adaptive hypertrophy Expression levels of glycolytic enzymes indicated both enhanced glycolysis and glucose oxidation to contrast the impair-ments of glucose oxidation in maladaptive hypertrophy

We also identified several differences in expression of

Fig 3 A scatter plot of the number of differentially expressed

genes compared to the number of false-positive genes at different

levels of delta The black line represents the actual data while the

three grey lines represent data from three random divisions of

samples into two groups The dotted black line represents unity,

where the number of called genes is identical to the number of

false positives.

Fig 4 Expression of selected metabolic genes by quantitative PCR confirming the microarray data Expression was normalized to GAPDH Bars represent SEM and *P < 0.05.

Table 4 (Continued).

Guanine nucleotide binding protein, alpha inhibiting polypeptide 3 AI228247 3.3 1.1 8.47E-03

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signalling proteins between adaptive and maladaptive

hypertrophy including important modulators of

adren-ergic signalling

Perhaps the most striking and potentially

physiologi-cally meaningful observation was the shift in metabolic

gene expression This finding is especially interesting as

it differentiates adaptive from maladaptive

hypertro-phy and could be the molecular mechanism underlying

earlier findings of a balanced growth of

cardiomyo-cytes with a normal ratio of mitochondria to cell

num-ber [10,17] and normal myofibril to mitochondrial

ratio [5,6] in adaptive hypertrophy

In our study, several genes involved in b-oxidation

of lipids (CD36, FACL, fatty acid binding protein)

were upregulated Genes involved in b-oxidation are

downregulated in maladaptive cardiac hypertrophy

[18,19] One gene, CD36 or Fat, encoding a fatty acid

translocase, was upregulated in response to exercise

but not regulated after maladaptive hypertrophy

CD36 has recently been shown to be responsible for

the defect in fatty acid metabolism seen in

spontane-ously hypertensive rats [20], and myocardial recovery from ischaemia is impaired in CD36 knockout mice [21] Thus the differential expression of CD36 between maladaptive and adaptive hypertrophy might be of key importance for the difference in clinical outcome in the two conditions

Glucose utilization through glycolysis is enhanced in hypertrophic hearts [22,23] However, there is no cor-responding increase in rates of glucose oxidation [22,23] The consequent low coupling of glucose oxida-tion to glycolysis is funcoxida-tionally relevant, as it contri-butes to the contractile dysfunction in hypertrophic hearts [23] The multienzyme pyruvate dehydrogenase complex (PDC) catalyses the oxidative decarboxylation

of pyruvate and contributes strongly to flux control of myocardial glucose oxidation The activity of PDC is continuously regulated by balance of inhibiting pyru-vate dehydrogenase kinase and activating pyrupyru-vate dehydrogenase phosphatase (PDP) reactions [24] We found upregulation of the PDP gene, thus, suggesting

an increased glucose oxidation in exercise-induced hypertrophy GCKR was upregulated; this has been shown to increase both glucokinase protein and enzy-matic activity levels, leading to improved glucose toler-ance and lowered plasma glucose in diabetic mice [25]

In accordance with these data, we found upregulation

of glucokinase (hexokinase 1) in hearts of exercised rats Further evidence of enhanced glycolysis came from the upregulation of 6-phosphofructo-2-kinase⁄ fructose-2,6-bisphosphatase that stimulates 6-phospho-fructo-1-kinase [26], a key enzyme of glycolysis, which was also upregulated in our experiments Collectively, these findings support the notion that cardiac capacity for glucose utilization is in fact increased by adapta-tion to exercise and that a transcripadapta-tional explanaadapta-tion for this aspect of functional improvement exists

We found significant downregulation of UCP2 in response to exercise, while UCP2 was upregulated in maladaptive hypertrophy Uncoupling proteins dissipate the proton electrochemical gradient formed during mito-chondrial respiration and generate heat production instead of ATP [27] Thus, ATP production through oxidative phosphorylation might be more effective in adaptive than in maladaptive hypertrophy due to differ-ences in UCP2 expression In line with this, UCP2 was recently found to be upregulated in several different transgenic models of cardiomyopathy induced by chro-nic b-adrenergic receptor signalling [28] The upregula-tion of UCP2 was partly reversed by b-adrenergic receptor blockade In response to volume overload, UCP2 expression was increased and this increase was partly reversed by an angiotensin converting enzyme (ACE)-inhibitor [29] UCP2 has previously been found

Fig 5 Expression of UCP2 and CD36 by quantitative PCR in

mal-adaptive hypertrophy 3 weeks after myocardial infarction (mi).

UCP2 was significantly upregulated while CD36 expression was

unchanged contrasting the findings in adaptive hypertrophy

Expres-sion was normalized to GAPDH Bars represent SEM and

*P < 0.05.

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to be downregulated in response to exercise [30] Thus,

upregulation of UCP2 seems a general feature of

mal-adaptive cardiac remodelling, and the well documented

beneficial effects of ACE-inhibitors and b-adrenergic

receptor-blockade are accompanied by decreased UCP2

expression These findings indicate that the

downregula-tion of UCP2 in adaptive hypertrophy constitutes a

molecular feature of ‘adaptiveness’ and that

upregula-tion of UCP2 may be a key factor underlying defective

energetics in diseased hearts

In accordance with previous reports we did not find

activation of the typical neonatal gene expression

pat-tern found in pathological hypertrophy, which includes

uprelation of atrial natriuretic peptide, B-type

natriure-tic peptide, a-skeletal and smooth muscle actin, and

b-myosin heavy chain [16] However, exercise-induced

hypertrophy was accompanied by a marked

upregula-tion of genes involved in extracellular matrix

remode-ling (biglycan, matrix gla protein, cathepsins, cystatins,

integrin a7 and laminin receptor) These genes are

con-sistently upregulated in pathological models of cardiac

hypertrophy indicating that these genes are necessary

to the cardiac growth response [18,31,32] In contrast

to pathological models of cardiac hypertrophy we

found no increase in collagen mRNA expression

We found upregulation of a number of cytoskeletal

genes Several of these genes were previously described

to be upregulated in pathological hypertrophy

(MYL 1, 4 and 6, sarcosin, talin, actin-related protein

complex 1b and ArgBP2) [31,33] Upregulation of

acti-nin a2 associated Lim11/rat Isl-1/Mec3 (LIM) protein

(ALP) in cardiac hypertrophy has not been described

previously but ALP–⁄ – mice develop cardiomyopathy

[34] In the only microarray study on exercise-induced

cardiac hypertrophy reported to date, MYL 4

upregu-lation was also found and confirmed by 2D gel

electro-phoresis [35] The study only employed three DNA

microarrays in each group and did not use a statistical

method to identify differentially expressed genes

We found prominent upregulation of proteins

involved in protein synthesis (eukaryotic translation

elongation factor 1 alpha 1, eukaryotic translation

elongation factor 2, RNA polymerase II polypeptide G

and several ribosomal proteins) These findings are

consistent with the increased demand for protein

syn-thesis in response to cardiac hypertrophy

In accordance with previous studies on

maladap-tive hypertrophy [18,36] we found upregulation of

inflammatory genes (superoxide dismutase 3,

comple-ment component 1qb and 1c, lysozyme and others)

indicating that inflammation is a general feature of

cardiac hypertrophy We cannot exclude the

possibil-ity that the strong physical stress induced by the

exercise contributed to the inflammatory response and exercise of more moderate extent with slower and continuous time course may induce hypertrophy without inflammation

Several of the differentially regulated signalling pro-teins have also been reported to change in maladaptive hypertrophy (Cbp⁄ p300-interacting transactivator, pro-tein tyrosine phosphatase 4a1, annexin 1 and cyclic nucleotide 3¢-phosphodiesterase) [18,32,33] Adrenergic signalling is important in cardiac hypertrophy and we found differential expression of several genes involved

in adrenergic signal transduction (catechol-O-methyl transferase, GRK2, AKAP4 and Gai3) GRK2 desen-sitizes G-protein coupled receptors and is upregulated [37] in maladaptive hypertrophy We found downregu-lation of GRK2 in adaptive hypertrophy pointing to a potentially important difference in adrenergic signal-ling between maladaptive and adaptive hypertrophy

In conclusion, we have used DNA microarrays to map gene expression in adaptive hypertrophy While expression of extracellular matrix proteins and sarco-meric proteins was similar to the changes known to occur in maladaptive hypertrophy, we found striking differences in expression of genes involved in metabo-lism between adaptive and maladaptive hypertrophy

Experimental procedures

Animal handling and training procedure

Twenty-four male Wistar rats (Taconic M & B, Ejby, Denmark) weighing 285 ± 10 g (mean ± SD; n¼ 24) were randomly assigned to either a seven-week treadmill running program (n¼ 12) or served as sedentary controls (n ¼ 12) The animals had free access to food (standard rodent pel-lets) and water Rats in the running group were exercised

on a custom-built 12-lane treadmill with an 8 inclination for 2 hÆday)1, 5 daysÆweek)1, for 7½ weeks between 12 : 00 and 17 : 30 Each training session started with a 20-min warm-up at 11 mÆmin)1 the first week gradually increasing

to 18 mÆmin)1 the last 3 weeks Running speed was set to

15 mÆmin)1 the first week, gradually increasing to level at 32.5 mÆmin)1 the final 2½ weeks, while the duration was reduced from 100 min to 80 min for the final 2½ weeks After 1 week of training one rat had a small injury to one

of its feet and was therefore withdrawn from further exer-cise and excluded from the study The experiments were approved by the Animal Experimentation Inspectorate of the Danish Ministry of Justice and the investigation con-forms to the Guide for the Care and Use of Laboratory Animals published by the US National Institutes of Health (NIH publication no 85-23, revised 1996) The day after completion of the training protocol, all animals were

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sub-jected to echocardiography and hemodynamic examination

under isoflurane anesthesia before being killed Hearts were

excised, rinsed in ice-cold saline, weighed, dissected into left

and right ventricles, frozen in liquid nitrogen and stored at

)80 C until mRNA extraction

As exercise resulted in a significantly reduced body

weight (BW) when compared to sedentary controls,

normal-ization of organ weights to BW would result in apparent

hypertrophy of all organs in the training animals For valid

comparison of experimental groups, organ weights were

instead normalized to lean body mass, estimated as BW0.78

[38], rendering only weights of total heart and left and right

ventricles different between groups, while lung, kidney and

stomach were not

Echocardiography

Echocardiography was performed during anesthesia with

1–1.5% isoflurane using a Vivid Five Echocardiograph

(GE Medical Systems Ultrasound, Little Chalfont, UK)

Recordings were stored digitally for off-line analysis Left

ventricular cavity and wall dimensions were measured in 2D

short axis recordings at the level of the papillary muscles

Hemodynamic examination

A microtip transducer catheter (Millar Instruments,

Hous-ton, TX, USA) was introduced from the right carotid

artery and placed in the left ventricle for measurements of

LVEDP and maximal rates of isovolumetric pressure

devel-opment (dP⁄ dtmax) and decline (dP⁄ dtmin) After retraction

from the left ventricle, mean arterial pressure (MAP) was

measured Simultaneous elecrocardiography was performed

from subcutaneously placed needle electrodes and heart rate

(HR) was calculated

Myocardial infarction

Myocardial infarction was induced by ligating the left

cor-onary artery Sham-operated animals served as controls

[39] After 3 weeks, animals were killed and total RNA was

isolated from the noninfarcted part of the left ventricle as

described in [36] Despite large thinned fibrotic scars, the

weight of the left ventricle was increased in infarcted ani-mals compared to controls, indicating left ventricular hypertrophy of the noninfarcted ventricle

Gene expression profiling

The GeneChip RGU34A from Affymetrix containing 8740 probe sets (and 59 control probe sets which were excluded from further analysis) was used for all hybridizations The probe sets represent approximately 6000 known rat genes, the rest being ESTs (see http://www.affymetrix.com for a more detailed description) Standard protocols for chip hybridizations available at http://www.affymetrix.com were used Briefly, cDNA was synthesized from total RNA extracted from the tissue samples by Trireagent (Molecular Research Center, Inc., OH, USA) cDNA was then used for in vitro transcription to produce biotin-labelled cRNA The cRNA was fragmented before hybridization RNA from individual animals was hybridized to each chip and six randomly chosen samples were analysed from each group Chip hybridizations were performed at a core facil-ity with ample experience in microarray handling to ensure quality Raw data are available at http://www.ncbi.nlm nih.gov/geo as series number GSE739 (access by username: revstro90, password: revstro90)

Array data analysis

Array data were normalized using the nonlinear invariant rank fitting method of Li and Wong available at http:// www.dchip.org [40] Model based expression (MBE) values were calculated for each gene using dChip (perfect match only model) Differentially expressed genes were identified using SAM available at http://www-stat stanford.edu⁄ tibs ⁄ SAM ⁄ [41] Briefly, SAM is a statistical approach to identify differentially expressed genes by con-trolling the FDR The FDR is the percentage of genes iden-tified by chance SAM identifies the differentially regulated genes by assimilating a set of gene specific t-tests Each gene is assigned a score by dividing the average difference

in gene expression between groups by the pooled SD Genes with scores greater than threshold delta (Fig 2, grey) are deemed potentially significant By permutation of the

Table 5 Primer sets used in quantitative PCR Sequences are shown in the 5¢)3¢ orientation.

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samples and recalculation of the scores, the FDR is

estima-ted at different values of delta Log2MBE values were

ana-lysed using a two-class unpaired approach with an FDR of

less than 5% For comparison, we calculated P-values for

each gene by a Welch t-test, which allows for inequality of

variances between groups P-values ranged from 2.0· 10)7

to 0.02

Quantitative PCR

RNA was extracted de novo from all the cardiac tissue

sam-ples (exercised, n¼ 11; sedentary, n ¼ 12) Reverse

tran-scription was performed using the Omniscript RT Kit

(Qiagen, Valencia, CA, USA) on 2 lg total RNA samples

and random hexamer primers according to manufacturer’s

instructions Primers were designed using PRIMER3 (MIT

and available online at http://www-genome.wi.mit.edu/cgi/

bin/primer/primer3.cgi/primer3_www.cgi) and sequence

information retrieved from the NCBI database Intron

spanning pairs were used to avoid amplification of genomic

sequences, and primer specificity and emergence of only

one product of the predicted size were ascertained by

agarose gel electrophoresis and real-time melting curve

ana-lysis of all PCR products Each sample reaction contained

cDNA synthesized from 10 ng heart RNA Standard curve

reactions contained cDNA pooled from all samples and

diluted 1 : 2, 1 : 4, 1 : 10, 1 : 50 and 1 : 100 (corresponding

to 50, 25, 10, 2 and 1 ng of total heart RNA, respectively)

DNA amplification was carried out using the RotorGene

(Corbett Research, Sydney, Australia) and the SYBR green

PCR Master Mix (Quantitect, Berkely, CA, USA) The

reactions were set up in 0.1 mL microtubes in a total

vol-ume of 20 lL with 1 lL of template Standard curves in

duplicate were included in every run, and quantification of

individual samples performed by normalization to

GAP-DH Constant GADPH expression between exercised and

sedentary animals was confirmed by northern blotting (data

not shown) At least three independent runs were

per-formed for every target transcript The primer sets used in

quantitative PCR are shown in Table 5

Statistical analysis

Array data were analysed as described above All other

comparisons were made by an unpaired Student’s t-test

P-values¼ 0.05 were considered significant

Acknowledgements

We thank the staff at the Microarray Center,

Rigshos-pitalet, Denmark, for performing the microarray

hy-bridizations and scannings We thank Peter Schjerling

for Northern blots of GAPDH and Pernille Gundelach

and Katrine Kastberg for technical assistance The

work was supported by the John and Birthe Meyer Foundation, the Danish Heart Foundation

(01-1-2-59-22907, 99-1-2-31-22684), the Villadsen Family Founda-tion, the Foundation of 17.12.1981, the University of Copenhagen, Rigshospitalet, the Novo-Nordisk Foun-dation and the Danish National Research FounFoun-dation

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