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A new rice zinc-finger protein binds to the O2S box of the a-amylasegene promoter Rihe Peng 1 1, Quanhong Yao1, Aisheng Xiong1, Huiqin Fan1, Xian Li1, Youliang Peng2, Zong-Ming Cheng3 an

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A new rice zinc-finger protein binds to the O2S box of the a-amylase

gene promoter

Rihe Peng

1 1, Quanhong Yao1, Aisheng Xiong1, Huiqin Fan1, Xian Li1, Youliang Peng2, Zong-Ming Cheng3 and Yi Li4

1

Shanghai Key Laboratory of Agricultural Genetic and Breeding, Agro-Biotechnology Research Center, Shanghai Academy of Agricultural Sciences, China;2Department of Plant Pathology, Chinese Agricultural University, Beijing,

Sciences, University of Tennessee, Knoxville, USA;4Department of Plant Science, University of Connecticut, Storrs, USA

3A putative transcription factor, named RAMY, that binds

to the 20-bp O2S sequences of the regulatory region of the

Amy2 gene promoter has been identified using the yeast

one-hybrid system from a rice library The full length RAMY

cDNA clone encodes a 218-amino acid protein and is

homologous to the late embryogenesis-abundant protein

(LEA5) In vitro mutagenesis and electrophoretic mobility

shift assays confirmed that RAMY can bind with O2S

spe-cifically through an unusual zinc finger with a CXCX4CX2H

consensus sequence Low levels of RAMY mRNAs were

detected in rice leaves and roots by Northern blot

hybrid-ization The plant hormone gibberellin (GA) induces expression of both RAMY and Amy2 genes, as performed by Northern blot hybridization,

mRNA level occurs prior to that of the Amy2 mRNA level

in the GA-treated aleurone tissues These data suggest that RAMY may act as a trans-acting protein and is probably involved in the GA-induced expression of the rice a-amylase gene

Keywords: rice zinc-induced protein; O2S box; yeast one-hybrid system

Cereal a-amylase genes have been one of the primary

systems for exploring the molecular mechanisms involved in

hormone-regulated gene expression in plants

ger-mination of cereal grains, the embryo releases GA to the

aleurone layer, where it induces the transcription of

a-amylase genes [1]

Functional analyses of a-amylase gene promoters using

transient expression assays with reporter genes have shown

both GA and abscisic acid (ABA) may interact with

transcriptional regulatory proteins or transcription factors

that bind to a short nuclear nucleotide sequence referred to

as the GA response element (GARE) [2–4] Lanahan et al

[5] has demonstrated that GARE mediates the hormonal

control of transcription in the promoter of the low-PI gene,

Amy32b At least three other distinct regulatory elements

have been found to be necessary for high-level a-amylase

gene expression regulated by GA A closely associated

group of elements is composed of an opaque-2-like protein

binding sequence (O2S), a sequence element with an

enriched pyrimidine nucleotide motif (the pyrimidine

box), the GARE, and box I (TATCCAT) [6] Using

quantitative transient expression assays, the most

import-ant elements have been found to be GARE and O2S; mutation or deletion of either GARE or O2S resulted in lower GA-induced transcription [4,5] Rogers and Rogers [4] found that both GARE and O2S functioned only when positioned in one orientation with respect to each other and with respect to the TATA box, and when the distance between them was relatively short In searching for factors that interact with the sequences and regulate a-amylase gene expression, a Myb protein, GAMyb (GA-responsive Myb protein), was isolated that may specifically bind to a portion of the GARE box [7] GAMyb is able to activate the expression of a-amylase and other GA-regulated genes [8] A zinc-finger protein has been identified by South-western screening with baits containing a GARE box and has been found to repress the expression of a-amylase and other genes [9] In Arabidopsis, at least three proteins, SPY, RGA and GAI, are thought to negatively regulate GA responses [10–12] However, although the O2S box is another important element for controlling the level of transcription in a-amylase gene, little is known about the regulatory proteins or transcription factors that bind to the O2S sequence Our interest in the mechanism of seed germination and development in rice prompted us to search for the O2S binding protein Using the yeast one-hybrid system, we screened the rice cDNA libraries using O2S-containing baits ATTGACTTGACCGTCATCGG from the low pI amy54 promoter [13] We have isolated

a cDNA clone, RAMY, which encodes a protein that contains a zinc-finger Our experimental data indicate that RAMY protein binds specifically to the O2S element We have also determined the importance of the amino acids within the binding domain of RAMY protein and analyzed the time course for the induction of RAMY and a-amylase mRNA by GA

Correspondence to Q Yao, Shanghai Key Laboratory of Agricultural

Genetic and Breeding, Agro-Biotechnology Research Center,

Shang-hai Academy of Agricultural Sciences, 2901 Beidi Road, China.

Fax: + 86 021 62209988, Tel.: + 86 021 62209988,

E-mail: pengrihe69@yahoo.com

Abbreviations: GST, glutathione S-transferase; O2S, opaque-2-like

protein binding sequence; GA, gibberellin; ABA, abscisic acid;

GARE, GA response element.

(Received 30 January 2004, revised 28 April 2004,

accepted 19 May 2004)

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trp–, ura–, leu–, his–) was used to rescue cDNA library

plasmids from yeast DNA preparations The bait plasmid

pLGD-265 UP1 is a URA-marked

plasmid carrying a lacZ reporter gene under the control of

the CYC1 minimal promoter [14]

The rice cDNA library was constructed in pPC86 vector,

which is a marked

7 yeast expression plasmid containing a

GAL4 activating domain under the control of the yeast

ADC1 promoter [15] The cDNA was derived from poly(A)

RNA isolated from 15-day-old rice (Oryza sativa L.,

genotype IR36) seedlings grown at 25C in a greenhouse

Yeast one-hybrid screen

A yeast one-hybrid screen was performed to isolate genes

encoding proteins that associated with the O2S box

ATTGACTTGACCGTCATCGG in the Amy2 gene

pro-moter [12] To construct bait plasmid, the cis-element

containing three copies of O2S was synthesized by PCR

using two primers: Amyb1: 5¢-ACCCTCGAGGTCGA

CGGTATCGATAAGCTTGATTGACTTGACCGTCA

TCGGATTGACTTGACCGTCATCG-3¢, Amyb2: 5¢-CA

GGATCCATCACGACAGTCAGTGCCGATGACGG

TCAAGTCAATCCGATG-3¢ (the PCR conditions were:

94C, 20 s; 58 C 30 s; 72 C, 30 s; 25 cycles) Following

PCR, the 110-bp fragment isolated from PAGE was

digested with restriction enzymes, and inserted into the

XhoI/BamHI sites of the vector pLGD

The lithium acetate protocol was used for yeast

transfor-mation [16] An overnight culture of yeast cells (0.5 mL) were

inoculated into 50 mL fresh YPD medium and grown for

4 h Yeast cells were centirfuged at 5000 g for 8 min, and the

pellets washed once with 20 mL sterile distilled water, and

then with 10 mL Tris/EDTA/LiAc (100 mMLiAc in Tris/

EDTA) Finally, the cell pellet was resuspended in 0.5 mL

Tris/EDTA/LiAc An aliquot of 50 lL yeast cells, 1 lg

plasmid DNA, 50 lg salmon carrier DNA and 300 lL Tris/

EDTA/LiAc containing 40% (w/v)

each tube, and the mixtures were incubated for 30 min at

30C with shaking (150 r.p.m.) After heat shock at 42 C

for 15 min, the collected yeast cells were resuspended in Tris/

EDTA buffer and plated on selective yeast media

The total DNA from each positive yeast clone was

isolated according to the method of Robzyk and Kassir [17];

DNA cloning was performed using to standard procedures

[18] The DNA extracted from yeast cells was electroporated

into E coli strain MC8 [19] The transformants were

selected on M9 minimal medium containing all amino acids

except tryptophan (M9-TRP), thus selecting

pPC86-con-taining colonies The plasmid DNA was re-introduced into

a yeast reporter strain to confirm the b-galactosidase

activity Two oligonucleotide primers GAL4 5¢-GGA

TGTTTAATACCACT-3¢ and TAD4 5¢-TTGATTG

GAGACTTGACC-3¢ derived from the DNA sequence

flanking the GAL4 activating domain and the ADC1

Southern–Northern blot analyses Extraction of plant DNA and Southern blotting analysis were performed based on the method of Bringloe [20] Total RNA was prepared from rice (O sativa L IR36); leaves and roots were treated with 10 lM GA, and control seedlings were treated with water by the standard method

In order to examine the time course of the GA-induced RAMYand Amy2 gene expression, steady state levels of their transcripts in the GA-treated aleurone tissues were determined with Northern blot hybridization De-embryo-nated rice half-seeds were de-husked, sterilized with 10% (v/v) commercial Clorox, and treated with 95% (v/v) ethanol for 30 s to remove the outer wax layer After rinsing with water, the rice de-embryonated half-seeds (20 g) were submerged in seed buffer (20 mM calcium chloride, 20 mM sodium succinate, pH 5.2) in cell culture dishes After 10 h of incubation in seed buffer, appropriate amounts of GA were added to a final concentration of

10 lM Isolated aleurone tissues were incubated with GA for 2, 4, 6, 8, 10, 12 or14 h

RNA was separated by gel electrophoresis and trans-ferred to a Hybond N+ nylon membrane (Amersham-Pharmacia) Hybridization was performed at 65C in 5· NaCl/Cit, 10% (w/v) dextran sulfate, 0.5% (w/v) SDS

and 0.1 mgÆmL )1 denatured salmon sperm DNA Filters were washed twice (each for 15 min) at 65C in 2· NaCl/ Cit, 0.1% SDS, and once in 0.1· NaCl/Cit, 0.1% SDS at

65C for 15 min

Production and analyses of GST–RAMY fusion protein The GST–RAMY fusion protein was generated by inserting RAMY gene open reading frame between the sites of BamHI and SacI in the vector pALEX [21] The primers used were RAMYZ (5¢-AGGATCCATGGCT CTCGCTCTCTCCACC-3¢) and RAMYF (5¢-AGA GCTCAGTGGTGGTGGTGGTGGTGCACTCGGGT ACGTGGTGAAAC-3¢) Mutated RAMY polypeptides were produced by in vitro mutagenesis using the follow-ing primers: C182SZ (5¢-CGTGTGGGCTGGATGCT CTCCT-3¢), C182SF (5¢-GAGGAGAGCATCCAGCCC AC-3¢), C184SZ (5¢-GTGGGCTGGATGCTCTGCTCG TCTG-3¢), C184SF (5¢-GCAGACGAGCAGAGCATC CAGC-3¢), C189SZ (5¢-CTGCTCGTGTGCTGGTTCTT CGTCCAC-3¢), C189SF (5¢-GAGGTGGACGAAGAAC CAGCACACG-3¢), H192AZ (5¢-TGCTGGTTCTTCGT GCACCTCTGCTGTAAC-3¢), and H192AF (5¢-GTGAG GCCCTGCTCGCTGTTACAGCAGAGGTGC-3¢) All mutant genes were cloned into a pUC18 vector and sequenced for confirmation The resultant mutant RAMY genes were then inserted into the BamHI/SacI sites of the vector pALEX

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The resulting GST–RAMY construct was used to

trans-form E coli BL21 Transtrans-formants were used to inoculate

50 mL cultures of LB/ampicillin and were grown overnight

at 37C and harvested by centrifugation Cell pellets were

resuspended in 9 mL phosphate buffer (pH 7.4), 20 mM

imidazole was added, and the bacteria were lysed by

sonication After centrifugation at 8000 g

4C, the GST–RAMY fusion protein was isolated using

HiTrap chelating columns according to the manufacturer’s

instructions (Amersham-Pharmacia) SDS/PAGE and

Coomassie blue staining were used to determine the purity

of the protein Protein concentrations were determined

using a protein assay kit (Bio-Rad) Mutant GST–RAMY

fusion protein

13 was expressed and purified in the same way as

for the GST–RAMY fusion protein

The mutant O2S box was synthesized by PCR using the

primers mAmyb1 (5¢-ACCCTCGAGATTGAGCTAGCC

GCTAGCTCAATCCGATG-3¢) The PCR conditions

were: 94C, 20 s; 58 C 30 s; 72 C, 30 s for 25 cycles

The core binding sequence CTTGA in the conserved O2S

domain was replaced by GCTAG A gel retardation assay

was carried out as described by Jensen [22] The XhoI and

BamHI fragment containing three copies of the O2S box

was labelled using a random primer method with the

wild-type or mutant O2S motifs as competitors One nanogram

of labelled O2S DNA fragments, competitor DNA, 2.5 lg

poly(dI–dC) and 10 lg GST–RAMY binding protein were

mixed in 25 lL of DNA binding buffer [5 mM Hepes

pH 7.5, 2 mMMgCl2, 0.2 mMdithiothreitol, 1 mMCaCl2,

2% (w/v) glycerol

14 ] The mixture was incubated for 20 min

at room temperature and loaded onto a 6% polyacrylamide

gel After migration, the gel was fixed in 5% (w/v) glycerol,

5% (w/v) methanol, and 5% (w/v) acetic acid

DNA was then transferred to Whatman paper

autoradiographed

Results Screening for rice cDNA encoding the O2S binding protein

To isolate genes whose products bind to the O2S domain (ATTGACTTGACCGTCATCGG) in the Amy54 gene promoter, two plasmids were used in the yeast one-hybrid system The plasmid pPC86 contained a rice cDNA library to express GAL4–cDNA fusion proteins, and plasmid pLGD

17 -265UP1 was used as the bait with an insertion of three copies of the O2S domain at the 5¢ end

of the CYC1 mini-promoter region Following transfor-mation of the URA-marked plasmid pLGD-265 UP1 containing the O2S domain and the TRP-marked pPC86 plasmid carrying rice cDNA library

and selection on selective medium for 2 days, approxi-mately 5· 106 yeast transformants were overlaid onto SC-TRP-URA X-gal medium using nitrocellulose filters

In the first round of selection, 31 positive (blue) colonies were selected To verify the true positive clones after the first round selection, total yeast DNA was extracted and transformed into the E coli strain MC8 Following selection for the E coli strain MC8, 14 individual transformants were positive (blue) on medium containing X-gal

Nucleotide sequence and predicted amino acid sequence

of rice RAMY cDNA Using GAL4 and TAD4 primers, sequencing analyses of both strands of all 14 cDNA fragment

contained identical, overlapping sequences encoding the same protein The complete nucleotide sequence encoded a predicted protein of 218 amino acids (Fig 1)

A search in a number of random protein databases 22

revealed that there is no significant homology between

Fig 1.

32 The rice RAMY cDNA sequences

and the predicted product of its longest ORF

(GenBank accession no AY072712) The

putative DNA binding domain is underlined,

and the putative nuclear localization signal

is double-underlined.

RAMY 60 DGSSSSA AREVS WVPDPVTGHYRP SNFAGGRRRRPPRRPPRP 101 G.max LEAS 59 DTRDGSK AYSTD W PDPVTG Y YRP INHTPEIDPVELRHRLLR 100 N.tabacum LEA5 51 KWEESS -KKTTS WVPDPVTG Y YRP ESHAKEIDAAELRQMLLN 91 G.hirsutum LEA5 49 AMKESSSSETRAYSSA W PDPVTG Y YRP ENCGAEIDAAELREMLLN 94 V.radiata ARG2 52 KSGEEKVR- GGEKVS WVPDPVTG Y YRP EN-TNEIDVADMRATVLG 94 A.thaliana ARG21 53 KGVEES -TQKIS WVPDPKTG Y YRP ETGSNEIDAAELRAALLN 203 H.vulgare G3 59 REAEKA -AADSS WVPDPVTGHYRP ANRSSGADPADLRAAHLG 100

Fig 2 Alignment of the conserved domain of RAMY with some related proteins RAMY is compared with the LEA5 proteins from G max (accession no AAB38782), N tabacum (accession no AAC06242) and G hirsutum (accession no P46522), the ARG2 proteins from V radiata (accession no P32292) and A thaliana (accession no AAC19273), and with the G3 protein from H vulgare (accession no CAA55482).

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RAMY with other proteins deposited in the databases.

However, the N-terminal half of RAMY is homologous

to the LEA5 proteins from Glycine max (GenBank

acces-sion no AAB38782), Nicotiana tabacum (accesacces-sion no

AAC06242) and Gossypium hirsutum (accession no

P46522), the ARG2 protein encoded by cDNAs isolated

from Vigna radiata (accession no P32292) [23] and

Arabid-opsis thaliana (accession no AAC19273), and the G3

protein encoded by Hordeum vulgare (accession no

CAA55482) [24] (Fig 2) The C-terminal half of RAMY

contained a motif with Cys and His residues similar to the

zinc finger C3H

23 (Fig 1, DNA binding domain)

Using the 720-bp full-length RAMY cDNA as a

probe for hybridization of rice genomic DNA that had

been digested separately with HindIII, XbaI, and BamHI,

we observed only one DNA band that hybridized with

the probe from each of the digested DNA samples

(Fig 3) Because there are no HindIII, XbaI, and BamHI

sites within the 720-bp cDNA, a single band observed in

the Southern blot hybridization experiment suggests a

single copy of the RAMY gene is present in the rice

genome

RAMY contains a novel zinc finger

Using the yeast one-hybrid system, the GAL4–RAMY

fusion protein exhibited a strong transcriptional activation

function in yeast cells The GAL4–RAMY fusion protein

24

bound to the cis-element in bait pLGD

induced transcription of the LacZ reporter gene

To examine whether RAMY protein binds to the O2S

sequence directly and specifically, we performed an

elec-trophoretic mobility shift assay experiment As shown in

Fig 4A, the presence of the purified GST–RAMY protein

resulted in a mobility shift of the 32P-labelled O2S DNA

Fig 3 Southern blot analysis of Oryza sativa genomic DNA Total

genomic DNA (10 lg per lane) was digested with the restriction

enzymes, HindIII (H), XbaI (X) and BamHI (B) The positive control

(CK) was pPC86 (RAMY) DNA digested with SalI Full-length

RAMY cDNA was used as the probe The molecular marker (in kb)

was kDNA digested with EcoRI and HindIII.

Fig 4 Characterization of the DNA binding affinity of RAMY recombinant protein to the Amy2/O2S sequences (A) The [a- 32 P]dATP labelled O2S probes were incubated in the presence or absence of GST

or GST–RAMY Lane 1, purified GST; lanes 2–5, GST–RAMY Binding is competed by the same length of fragment containing three copies of unlabelled Amy2/O2S sequence; lane 2, 50 · competitor DNA; lane 3, 10 · competitor DNA; lane 4, 5 · competitor DNA; lane 5, 1 · competitor DNA (B) Comparison of DNA binding pref-erences of RAMY protein to the mutants (M) and the wild-type O2S (W) Lane 1, Purified GST; lane 2, GST–RAMY; lanes 3–6, EMSA by preincubating 25-fold (25 ·) or 100 fold (100 ·) excess amounts of unlabelled DNA fragments F, free probe; S, shift probe.

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fragment on the gel, suggesting that the GST–RAMY

protein binds directly to the O2S sequence Because the

purified GST alone did not produce such a mobility shift,

the shift must be caused by RAMY protein Furthermore,

the unlabelled O2S DNA competed well with the 32

P-labelled O2S DNA but nonspecific DNA or mutant O2S

DNA did not (Fig 4B), demonstrating that the binding of

RAMY to the O2S is specific

We performed an in vitro mutagenesis experiment to

identify amino acid residues of RAMY protein that are

important for the DNA binding In the C-terminal region

of RAMY, there are three Cys and one His residues

Figure 5

26 shows that mutagenesis of Cys182 severely

reduced binding activity of RAMY to the O2S DNA

sequence Furthermore, mutagenesis of Cys184, Cys189 or

His192 abolished the binding of the protein to the O2S

sequence completely

RAMY mRNA accumulation in GA-treated tissues

To determine whether the expression of the RAMY gene is induced by GA, and the possible relationship between the expression of the RAMY gene and the Amy2 gene, we performed a Northern blot hybridization experiment As shown in Fig 6A, RAMY was expressed at low levels in leaves but almost not at all in roots

and leaves, expression of RAMY was significantly induced

by exogenous GA We also used aleurone tissues to study the time course of the GA-mediated induction of RAMY and Amy2 expression Figure 6B shows that RAMY mRNA was observed 4 h after the GA treatment, but an increase in Amy2 mRNA was seen only after 10 h of the

GA treatment The level of RAMY mRNA reached its maximum 10 h after the GA treatment and returned to its basal value within 14 h In contrast, Amy2 mRNA reached

a maximum at 14 h after the GA treatment (Fig 6B) These data suggest that RAMY could act as a regulatory or transcription factor for the expression of a-amylase genes Discussion

We have cloned a gene, RAMY, from a rice cDNA library using O2S-containing baits with the yeast one-hybrid method that encodes a zinc-finger protein

the O2S-box binding domain is present in the protein This conclusion is supported by the observations that the RAMY

Fig 5 DNA binding is mediated by the zinc finger domain (A) SDS/

PAGE showing the purity of the recombinant GST-fusion proteins

(lanes 2–6) The GST-fusion proteins were over-expressed in E coli

BL21 (DE3), extracted under nondenaturing conditions and purified

by affinity chromatography (B) Gel mobility assay with the purified

GST–RAMY fusion protein (lane 2) or GST-mutant RAMY fusion

protein (lanes 3–6), showing RAMY binding to DNA and the effects

of mutations within the RAMY DNA-binding domain on the ability

of the purified fusion protein GST–RAMY to bind a probe containing

three copies of the Amy2/O2S region.

Fig 6 RAMY transcript levels in a rice plant subjected to GA treat-ment (A) GA induced RAMY mRNA accumulation in leaves and roots L, leaves; L + GA, leaves treated with GA; R, roots; R + GA, roots treated with GA (B) Induction of RAMY protein and a-amylase (GenBank accession no AF411220) by GA Aleurone tissue was incubated with GA for 2, 4, 6, 8, 10, 12 or 14 h Total RNA samples were loaded (20 lg per lane), fractionated on a 1.2% formamide/ agarose gel, probed with a 32P-labelled RAMY probe 18S, RNA probed with a 32 P-labelled 18S rRNA probe a-amy, RNA probed with a 32 P-labelled a-amylase gene probe.

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to the O2S domain Several plant zinc-finger proteins are of

the cluster type with multiple repeated fingers separated by

sequences of different length The spacing between the

fingers is the main element to determine the specificity of

binding target sequence [25] However, we only detected one

zinc-finger domain in RAMY, perhaps because the different

structure of the zinc finger motif in RAMY influences the

binding domain A putative nuclear localization signal

[26,27] sequence is also found in RAMY (Arg90–Arg97),

suggesting that RAMY may be transported into the nucleus

through the nuclear pore complex using its own nuclear

localization signal

Database searches revealed RAMY was homologous

only to part of the LEA5 (late embryogenesis-abundant)

proteins LEA5 proteins display a hydrophobic N-terminal

half and a hydrophilic C-terminal half [28] This family of

proteins is further characterized by a highly conserved motif

of 12 amino acids with the consensus WAPDPVTGYYRP

RAMY can be grouped into the Lea5

presence of the canonical 12 amino acid sequence motif

(WAPDPVTGYYRP)

Most LEA5-like proteins are induced in embryos or

vegetative tissues by desiccation, ABA or high osmoticum

The soybean Lea5-like (D-73 like) cDNA accumulates in

desiccating seeds from 20 to 80 days after flowering

roots but not in leaves of drought-stressed plants [29,30]

The related gene (Di21) from Arabidopsis displays increased

transcript accumulation in roots and leaves after drought

induction, but is not detected in mature dry seeds of

nonstressed Arabidopsis plants [31,32] In cotton, the Lea5

transcripts are highly induced in mature leave of

water-stressed plants or in water-water-stressed detached leaves [28]

However, the evidence presented here indicates that RAMY

transcription is induced by GA The interaction between GA

and ABA may be important in controlling the a-amylase

gene expression

The effects of GA and ABA on a-amylase gene

transcription have been established from transient

expres-sion experiments using a-amylase promoter-reporter gene

constructs in aleurone protoplasts [33,34] Two physically

associated elements are essential: a GA response element

(GARE) regulated by GA and ABA, and an opaque-2

binding sequence (O2S) This is consistent with the

hypo-thesis that protein binding and interaction between two

separate binding sites are required for high-level

transcrip-tion and proper hormonal regulatranscrip-tion [5] The expression of

GAMybat the mRNA level is upregulated by GA [7] and

the increase in the GAMyb mRNA occurs before that of

Amy21 mRNA after GA treatment In addition, GAMyb

specifically binds to an Amy21 GARE, and transient

expression experiments have shown that GAMyb activates

transcription of a high-pI a-amylase promoter fused to a

reporter gene in the absence of GA These results suggest

that GAMyb is a GA-regulated transcription factor

required for transcriptional activation of the high-pI

established

Acknowledgements

We would like to thank Dr Qun Zhu for proving us the rice cDNA library This research was supported by China PR Committee of Science.

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