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We show that injection of one-cell-stage zebrafish embryos with siRNA causes a significant reduction in the endogenous levels of processed miR-430 and other miRNAs, leading to unspecific de

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microRNA pathway and causes unspecific defects

in zebrafish embryos

Xiao-Feng Zhao, Anders Fjose, Natalia Larsen, Jon V Helvik and Øyvind Drivenes

Department of Molecular Biology, University of Bergen, Norway

MicroRNAs (miRNAs) are small RNA molecules of

 21 nucleotides in metazoan animals and plants that

influence mRNA stability and translation [1–3] These

mature miRNAs are generated from longer primary

transcripts (pri-miRNA) in two processing steps

cata-lyzed by two related RNase III endonucleases In

ani-mals, a nuclear microprocessor complex, containing

the RNase III enzyme Drosha and the dsRNA-binding

protein DGCR8, cleaves the pri-miRNA and exises a

stem loop of  70 nucleotides [3–6] This precursor

miRNA (pre-miRNA) is then exported to the

cytoplasm by a nuclear transport receptor complex, exportin-5⁄ RanGTP [7,8] In the cytoplasm, a second RNase III, Dicer, cleaves the pre-miRNA to generate the mature miRNA [3,9,10]

The function of miRNAs and the ability to knock down expression of specific genes by RNA interfer-ence (RNAi) methods depend to a large extent on the same cellular machinery [3] One important example is Dicer, which is required for miRNA processing as well as cleavage of dsRNA into small interfering RNAs (siRNAs) Moreover, mature miRNA and

Keywords

dicer; maternal mRNA; microRNA; RNA

interference (RNAi); zebrafish development

Correspondence

A Fjose, Department of Molecular Biology,

University of Bergen, PO Box 7803,

N-5020 Bergen, Norway

Fax: +47 555 89683

Tel: +47 555 84331

E-mail: anders.fjose@mbi.uib.no

Ø Drivenes, Department of Molecular

Biology, University of Bergen, PO Box 7803,

N-5020 Bergen, Norway

Fax: +47 555 89683

Tel: +47 555 84325

E-mail: oyvind.drivenes@mbi.uib.no

(Received 7 December 2007, revised 18

February 2008, accepted 3 March 2008)

doi:10.1111/j.1742-4658.2008.06371.x

MicroRNAs (miRNAs) are generated from primary transcripts through sequential processing by two RNase III enzymes, Drosha and Dicer, in association with other proteins This maturation is essential for their func-tion as post-transcripfunc-tional regulators Notably, Dicer is also a component

of RNA-induced silencing complexes, which incorporate either miRNA or small interfering RNA (siRNA) as guides to target specific mRNAs In ze-brafish, processed miRNAs belonging to the miR-430 family have previ-ously been shown to promote deadenylation and degradation of maternal mRNAs during early embryogenesis We show that injection of one-cell-stage zebrafish embryos with siRNA causes a significant reduction in the endogenous levels of processed miR-430 and other miRNAs, leading to unspecific developmental defects Coinjection of siRNA with preprocessed miR-430 efficiently rescued development This indicates that the abnormali-ties generally observed in siRNA-treated zebrafish embryos could be due to inhibition of miR-430 processing and⁄ or activity Our results also suggest that the miRNA pathway in mammals, under some experimental or thera-peutic conditions, may be affected by siRNA

Abbreviations

GFP, green fluorescent protein; hpf, hours postfertilization; miRNA, microRNA; MMB, mesencephalic–metencephalic boundary; MZdicer, maternal–zygotic dicer; pre-miRNA, precursor miRNA; pri-miRNA, primary transcript of microRNA; RISC, RNA-induced silencing complex; RNAi, RNA interference; siGFP, siRNA specific for green fluorescent protein coding sequence; siRNA, small interfering RNA; TRBP, transactivating response RNA-binding protein.

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siRNA are assembled into the RNA-induced silencing

complexes (RISCs) miRISC and siRISC, respectively

[3] Both of these effector complexes contain, in

addi-tion to similar Argonaute proteins, Dicer and other

factors such as the transactivating response

RNA-binding protein (TRBP) [11,12] Interestingly, it has

also been demonstrated that TRBP associates with

Dicer to facilitate generation of siRNAs and mature

miRNAs [13,14]

RNAi has been employed extensively as a research

tool in several animal models, including

Caenorhabd-itis elegans, Drosophila melanogaster and mice, as well

as mammalian cells [15–18] RNAi targeting of specific

genes has also been demonstrated in zebrafish

(Danio rerio) cell lines [19] However, experimental

studies on zebrafish embryos have revealed substantial

unspecific defects of RNAi that have prevented further

use of this technology for gene function analyses [19–

22] By circumventing these problems, studies on

zebrafish maternal–zygotic dicer (MZdicer) mutants,

which do not process pre-miRNA, have uncovered

extensive embryonic abnormalities reflecting the

impor-tance of miRNAs in developmental processes [23]

Remarkably, the brain morphogenesis defects in MZ

dicer mutants could be suppressed by injection of

preprocessed miR-430 family miRNAs, which are the

only abundant miRNAs during the first hours after

the transition from maternal to zygotic gene expression

[23] Further studies of the developmental regulatory

function of miR-430 revealed that these miRNAs

accelerate deadenylation and degradation of several

hundred different types of maternal mRNAs, leading

to a sharpening of the maternal-to-zygotic transition

[24]

We have investigated the possible connection

between the miRNA pathway and the unspecific

defects caused by RNAi in zebrafish embryos

Accom-panying the induction of unspecific defects, the

treat-ment with different siRNAs was also shown to

significantly reduce the levels of processed miR-430

and other miRNAs Moreover, we demonstrated, by

coinjecting siRNA with preprocessed miR-430, that

most of the morphological abnormalities could be

pre-vented Hence, the unspecific defects generally caused

by RNAi in zebrafish embryos are mainly due to

inhi-bition of miR-430, which has been shown previously

to have an essential role in the clearance of maternal

mRNAs [24] These observations may have

implica-tions for the development of new RNAi techniques in

zebrafish In addition, our results suggest a need for

investigating whether treatment of mammalian cells

with larger amounts of siRNA may also cause some

inhibition of the miRNA pathway

Results

Different siRNAs cause similar unspecific defects

We have previously characterized the structure and embryonic expression of zebrafish six3a (originally named six3 [25]), and more recently we have identified genomic and cDNA sequences representing eri1, a zebrafish homolog of the enhanced RNA interference-1 (eri-1) gene in C elegans (see Experimental proce-dures) Using specific siRNAs (siEri1 and siSix3a) to target the mRNAs expressed from these two genes, we observed similar but not identical embryonic defects (Fig 1C–F) Following injection of sufficient amounts

of siRNA (see Experimental procedures), most embryos at 28 h postfertilization (hpf) displayed tail truncations and loss of distinct morphological features

at the mesencephalic–metencephalic boundary (MMB; Table 1) In addition, enlarged heart cavities occurred

at lower frequencies in these embryos (not shown) Notably, we also observed tail truncations and MMB defects in embryos treated with siRNA specific for green fluorescent protein (GFP) coding sequences (siG-FP; Fig 1G,H; Table 1), suggesting that these malfor-mations are general consequences of siRNA treatment

siGFP siSix3a siEri1

WT

*

*

*

Fig 1 Injection of different siRNAs causes brain and tail defects Light micrographs are shown for wild-type (WT) and siRNA-injected zebrafish embryos At the 28 hpf stage, the zebrafish embryos injected with siRNAs targeting eri1 (siEri1), six3a (siSix3a) and GFP (siGFP) show tail and brain defects The MMB is easily visible in wild-type embryos (arrowhead), whereas this morphological con-striction is missing in embryos injected with the different siRNAs [stars in (D), (F) and (H)].

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Consistent with this assumption, equal numbers of

molecules of the same GFP sequence caused very few

abnormalities when injected as ssRNA (sense and

anti-sense in separate experiments) or dsRNA without the

2 bp 3¢-overhangs (Table 1)

siRNAs affect the endogenous levels of miRNAs

The defects caused by siRNA injections showed a

resemblance to the abnormalities reported previously

for MZdicer mutants, which are due to failure in the

processing of miR-430 [23] Interestingly, the MZdicer

phenotype also included tail and MMB defects [23]

Therefore, it seemed plausible that miRNA processing

could be affected by the injection of siRNAs To

inves-tigate this possibility, we analyzed by northern blotting

the levels of processed miR-430b and three additional

miRNAs expressed in early embryos [26,27] This

anal-ysis showed that all three siRNAs caused reductions in

the amounts of mature miRNAs at 12 hpf (Fig 2A)

Although the level of processed miR-430b seemed to

be most strongly affected, we also detected significant

reductions for the other three miRNAs tested

Further-more, we generally observed stronger reductions for

the largest dosage of siRNA (500 pg) These results

were reproducible, and for miR-430b the level was

reduced by as much as 70% (supplementary Fig S4)

The effects of siRNAs on miRNA levels were less

prominent at later embryonic stages, as revealed by

analyses at 24 hpf, where a significant reduction in the

amount of the mature form was detected only for

miR-430b (supplementary Fig S1)

To examine whether the reduced amounts of

pro-cessed miRNAs could be due to a unique feature of

siRNAs, we analyzed the possible effects following

microinjection of other types of RNA molecules

con-taining the same GFP sequence As expected from the

minimal effects on embryonic development caused by

injection of equal numbers of these GFP-specific RNA

molecules (Table 1), we did not detect any reduction in

the level of processed miR-430b at 12 hpf (Fig 2B) Consistent with the common MMB defects of the three siRNAs, expression of the pax2a gene, which is an

Table 1 Analysis of the efficiencies of different siRNAs and

related RNA molecules in inducing MMB defects asGFP, antisense

strand of GFP; dsGFP, double-stranded GFP without 3¢-overhangs;

sGFP, sense strand of GFP.

Embryos analyzed MMB defects (%)

A

B

C

Fig 2 Injection of different siRNAs affects the levels of miRNAs (A) The endogenous levels of the processed forms of four different miRNAs were analyzed at the 12 hpf stage by northern blotting Treatment with each of the three different siRNAs caused reduc-tion of the levels of all four miRNAs as compared to the wild-type (WT) (B) Northern blot analysis of the endogenous level of mature miR-430b at 12 hpf following injection of different types of RNA molecules corresponding to the same GFP sequence Single-stranded and double-Single-stranded molecules without the characteristic features of siRNA did not affect the level of miR-430b, as com-pared to non-injected (WT) and buffer-injected embryos (C) Endog-enous levels of mature miR-430b were reduced at 12 hpf following injection of miR-206 The different amounts (pg) injected are indi-cated for each type of RNA asGFP, antisense strand of GFP; dsGFP, double-stranded GFP without 3¢-overhangs; sGFP, sense strand of GFP.

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important midbrain marker [28,29], was also clearly

reduced in the affected region of the brain

(supplemen-tary Fig S2)

Coinjection with preprocessed miR-430b can

prevent unspecific defects

Microinjection of preprocessed miR-430 has previously

been shown to rescue tail and brain defects of MZdicer

mutants [23] Similarly, we investigated whether

coin-jection of miR-430b could rescue the effects of siRNA

treatment In these experiments, we also performed

control injections with miR-206, and a mutated version

of miR-430b (miR-430b-mis) that lacks the power to

rescue MZdicer embryos [23] Consistent with the

results of Giraldez et al [23], the dsRNA molecules of

preprocessed miR-430b did not induce any embryonic

defects (Fig 3A,B; Table 2) However, preprocessed

miR-206 duplexes clearly affected the morphologies

of both the tail and MMB of injected embryos

(Fig 3C,D; Table 2), indicating that treatment of

zebrafish embryos with miRNA duplexes may

generally induce the same kind of unspecific defects as

siRNAs In support of this assumption, we also

observed reduced levels of mature miR-430b in

miR-206-injected embryos (Fig 2C)

Coinjection of preprocessed miR-430b efficiently

res-cued the siEri1-induced defects (Fig 3E,F; Table 2),

and a similar result was observed for coinjections of

miR-430b with siSix3a (supplementary Fig S3;

Table 2) Preprocessed miR-430b also rescued embryos

from defects caused by siGFP, and the efficiency was

clearly improved with a higher dosage (Fig 3K,L;

Table 2) By contrast, coinjection of miR-430b-mis,

which has two point substitutions in the 5¢-seed region

[23], did not rescue the MMB or tail defects

caused by any of the three gene-specific siRNAs

(Fig 3G,H,M,N; supplementary Fig S3; Table 2)

Similarly, siEri1-induced defects were not rescued by

coinjection with miR-206 duplexes (Fig 3I,J; Table 2)

These results show that unspecific defects induced by

siRNA, which correlate with a significant reduction of

the endogenous level of mature miR-430b, can be

pre-vented by coinjection of this particular miRNA If

inhibition of miR-430 activity by siRNAs occurs also

at the level of miRISC assembly and⁄ or function,

miR-430b coinjection would be expected to reduce this

effect as well (see Discussion)

Discussion

The rapidly growing knowledge on RNAi and miRNA

has revealed many common factors and

Fig 3 Rescue of siRNA-induced abnormalities by coinjection

of miR-430b The effects of injecting preprocessed duplexes of miRNAs alone and in combination with siRNAs were analyzed Whereas embryos were not significantly affected by injection of miR-430b (A, B), injection of miR-206 caused similar tail and MMB defects as siRNA injections (C, D) (see Fig 1).The tail ⁄ MMB defects caused by injections of the two different siRNAs, siEri1 and siGFP (see Fig 1), were rescued by coinjection of miR-430b alone (E, F, K, L) but not by the mutated variant miR-430b-mis (G,

H, M, N) Coinjection of miR-206 did not rescue the tail ⁄ MMB defects caused by siEri1 (I, J) Arrowheads and stars indicate the presence and absence of an MMB, respectively.

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tions between these two pathways Recently, it has also

been shown that modulation of the processing of

miR-NAs is an important feature of their regulatory

func-tion and may be directly connected to cell signaling

[30–32] However, in relation to the extensive use of

RNAi as a tool to knock down the expression of

spe-cific genes, the possible influence on miRNA

process-ing, which may cause various side effects, has been

analyzed only recently [33] In this study, we have

investigated these aspects in zebrafish, where RNAi

experiments have previously been shown to result in

high frequencies of unspecific defects [19–22] Because

of these problems, RNAi has not become a useful

technique for studying gene function in zebrafish As

an alternative, morpholino antisense oligonucleotides

have been extensively used for transient knockdown of

gene expression in zebrafish embryos and larvae

[34,35] However, unspecific effects can be a problem

with this method as well, and it cannot be further

developed as a transgenic technique with the

possibili-ties of achieving tissue-specific and⁄ or long-term

knockdown of the targeted genes

In Drosophila and mouse, transgenic RNAi

tech-niques have been developed to facilitate tissue-specific

or inducible knockdown [16,17] In principle, this

strat-egy can also be used in zebrafish, but it may not be

feasible, due to the unspecific effects associated with

RNAi Although the reason why treatment with

siR-NA causes a high frequency of general abnormalities

in zebrafish has remained unclear, some clues

regard-ing this issue have been obtained from studies of the

MZdicer mutation [23] The MZdicer mutant embryos,

which display several defects similar to those caused

by siRNAs, were rescued by injection of preprocessed

miR-430 miRNAs [23] Remarkably, further investiga-tions on the mRNA targets of miR-430, which are the only abundant miRNAs before gastrulation, demon-strated that miR-430 is essential for efficient removal

of maternal mRNAs during the maternal-to-zygotic transition [24] Hence, considering the common factors

in the RNAi and miRNA pathways, and the impor-tance of miR-430 at early stages of zebrafish develop-ment, we assumed a possible involvement of miR-430

in the unspecific defects caused by siRNA treatment Using siRNAs corresponding to sequences in two endogenous genes (eri1 and six3a) and the exogenous reporter gene GFP, we investigated the possibility that miRNAs may in some way be influenced by the siR-NAs introduced into zebrafish embryos By northern analysis of miR-430b and three additional miRNAs,

we found a general reduction in the levels of processed miRNAs in embryos treated with siRNAs Injection of other types of RNA molecules, such as ssRNAs and dsRNAs without the 3¢-overhangs, which contained the same sequence, did not cause any general abnor-malities, and the levels of mature miRNAs were not affected These results suggest that the characteristic features of siRNAs are critical for reducing the levels

of processed miRNAs, particularly miR-430, and this may lead to the unspecific defects observed in zebrafish embryos

If this interpretation is correct, it will be natural to ask how injection of siRNAs can possibly interfere with the endogenous levels of mature miRNAs Although correctly sized siRNAs ( 21 bp) are not cut

by Dicer, which is the enzyme responsible for the last processing step of miRNAs, siRNAs are known to be assembled into effector complexes (siRISCs) containing Argonaute proteins as well as Dicer and other factors [3] One of the additional factors is TRBP, which together with Dicer facilitates generation of siRNAs and mature miRNAs from dsRNAs and pre-miRNAs, respectively [13,14] Accordingly, the injection of large amounts of siRNAs would affect the availability of these factors for processing of pre-miRNAs Thus, the most plausible explanation is that the observed reduc-tion of mature miRNAs is due to inhibireduc-tion of pre-miRNA processing by siRNAs competing for binding

to Dicer, TRBP, and⁄ or other limiting factors How-ever, since our northern blot analysis did not reveal a concomitant increase of pre-miRNAs, we cannot exclude other possibilities, such as enhanced degrada-tion of mature miRNAs

When discussing the relevance of miR-430 to the unspecific defects caused by siRNAs, it should be noted that these miRNAs are most abundant during early stages of zebrafish development [26,36,37]

Follow-Table 2 Analysis of the influence of siRNAs and miRNAs on MMB

morphology Coinjection of miR-430b efficiently rescued MMB

defects caused by siRNA treatment The MMB defects were not

significantly rescued by miR-206 and the mutated variant

miR-430b-mis.

Embryos analyzed

MMB defects (%)

250 pg of siEri1 + 250 pg of miR-430b 111 9 (8.1)

250 pg of siEri1 + 250 of pg miR-430b-mis 115 97 (84.3)

250 pg of siEri1 + 250 pg of miR-206 110 110 (100)

250 pg of siGFP + 250 pg of miR-430b 88 55 (62.5)

250 pg of siGFP + 450 pg of miR-430b 46 21 (45.7)

250 pg of siGFP + 250 pg of miR-430b-mis 109 107 (98.2)

400 pg of siSix3a + 250 pg of miR-430b 91 7 (7.7)

400 pg of siSix3a + 250 pg of miR-430b-mis 112 101 (90.2)

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ing siRNA injection, we detected a > 50% reduction

of processed miR-430b, and this would be at least

par-tially equivalent to the conditions in MZdicer embryos,

in which processing of pre-miRNAs does not occur

[23] Similar to the rescue of MZdicer mutants by

miR-430b [23], we observed efficient rescue when

siRNAs were coinjected with the preprocessed duplex

form of this particular miRNA In contrast,

coinjec-tion of another early embryonic miRNA (miR-206) or

a mutated version of miR-430b (miR-430b-mis) did

not give any rescue These results are entirely

consis-tent with the documented role of mature miR-430 in

promoting deadenylation and degradation of maternal

mRNAs, which is required for a normal

maternal-to-zygotic transition [24] Because of this crucial function

of miR-430, development of zebrafish embryos is likely

to be affected by treatment with siRNAs Our results

from experiments with three different siRNAs suggest

that this effect is a general phenomenon in zebrafish

However, some variations with respect to the abilities

of different siRNAs to cause unspecific defects and

reduced levels of mature miRNAs suggest a certain

degree of sequence dependence This may simply reflect

differences in the binding affinities of various siRNAs

to one or more factors that are shared between the

RNAi and miRNA pathways

Relevant to this issue, we also noted that single

injections of 206 duplexes, in contrast to

miR-430b, caused a high frequency of brain and tail

abnor-malities, as well as a reduction of the endogenous level

of processed miR-430b These observations indicated

that the level of the mature form of miR-430 was

affected by miRNA injection but was compensated by

the introduction of preprocessed miR-430b Therefore,

we conclude that injected miRNA duplexes (with

inter-nal mismatches) can probably affect the endogenous

concentrations of mature miRNAs in the same way as

siRNA duplexes

The importance of miR-430 was confirmed by

coin-jection of preprocessed miR-430b duplexes, which

apparently rescued most of the unspecific defects

caused by siRNAs However, at lower doses of

siRNAs, when the endogenous level of mature

miR-430 was less affected, we also observed relatively

high frequencies of unspecific defects This could reflect

a particularly high sensitivity to changes in the

concen-tration of this important miRNA, but it seems more

likely that siRNAs may cause an additional block of

miRNA function at the level of the effector complex

miRISC Hence, excess amounts of siRNAs may

effi-ciently compete with miR-430 (and other miRNAs)

for binding to Dicer, Argonaute proteins and⁄ or other

factors of this complex, and prevent interaction with

the mRNA targets For the same reason, coinjection

of preprocessed miR-430b duplexes would be expected

to reduce this inhibition

The results reported here suggest that siRNAs injected into zebrafish embryos compete for limiting factors that are required in the miRNA pathway By contrast, a recent study of systemic administration of synthetic siRNA in mouse and hamster did not reveal any effect on miRNA levels or activity in the liver [33] However, a more complete investigation is required to analyze whether or not treatment of mammals with higher doses of siRNA can inhibit the endogenous miRNA pathway in particular tissues and⁄ or during embryogenesis Another issue, which is also relevant to therapeutic use of siRNA in humans, concerns the possible sensitivity to changes in miRNA levels or activity Negative side effects reflecting such sensitivity have already been reported from experiments where short hairpin RNAs were expressed at high levels in the liver of mice [34] This treatment was shown to sat-urate the nuclear exportin-5 transporter, leading to reduction of the levels of processed miRNAs and lethality

Experimental procedures

Isolation and analysis of genomic DNA and cDNA Two zebrafish eri1 expressed sequence tags (BQ285328 and BI888174), reported previously [38], were subjected to blast analysis against the zebrafish genomic database at ENSEMBL, and a genomic region containing the eri1 locus was identified (GenBank accession number BX511222) Using genscan [39], webgene [40] and eri1 expressed sequence tag alignments, we identified a putative eri1 cod-ing region composed of seven exons spanncod-ing a genomic region of 7542 bp Using primers located in the putative 5¢-region and 3¢-region, ERI1F1 (5¢-AAA CCA GAT GTG AGT GTT TCT GA-3¢) and ERI1R1 (5¢-CAC AAC ATG GCA GGT TTT CA-3¢), we isolated the complete eri1 coding sequence by PCR using adult zebrafish cDNA as template

Injections of siRNA and miRNA duplexes Adult fish were kept at 28.5C on a natural 14 h light ⁄ 10 h dark cycle, and all embryos were obtained from natural mating The siRNAs targeting eri1, six3a and GFP (see below) were designed using the Dharmacon siRNA design center (http://www.dharmacon.com/sidesign/) and pur-chased from MWG Biotech (Ebersberg, Germany) Embryos were injected in the yolk at the one-cell stage, with an average injection volume of 2 nL, which contained

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250 pg of siRNA and⁄ or miRNA In the case of six3a, a

larger amount of siRNA (400 pg) was required to achieve a

high frequency of defects (Table 1) Following injection,

embryos were incubated at 28.5C in E3 medium

Oligonucleotide sequences

The sequences are given in the 5¢- to 3¢-direction: siEri1,

UCAGUGAUCCGGUGUAUAA(TT); siSix3a, CUAUCA

GGAGGCCGAGAAA(TT); siGFP, AAGCUGACCCU

GAAGUUCA(TT); dsGFP, AAGCUGACCCUGAAGU

UCA; sGFP, AAGCUGACCCUGAAGUUCA(TT);

asGFP, UGAACUUCAGGGUCAGCUU(TT)

Northern blot probes: miR-430b, BIO-GUACCC

CAACUUGAUAGCACUUU; miR-206, BIO-CCACATG

CTTCCTTATATTCCATA; miR-17a-1, BIO-ACTACCTG

CACTGTAAGCACTTTG; miR-19b, BIO-TCAGTTTT

GCATGGATTTGCACA miR-206 duplex: AAUGUAA

GGAAGUGUGUGGGU; CCACACACUUCCUUACAA

UUU

miR-430b duplex: AAAGUGCUAUCAAGUUGGG

GU; CCCAACUUGAUAGCACUAUUU miR-430b-mis

duplex, as described in [23]: AAAGACCUAUCAAG

UUGGGGT; CCCAACUUGAUAGGUCUAUTT

Northern blot analysis

Total RNA was isolated from wild-type and injected

embryos at 12 hpf and 24 hpf using Trizol (Invitrogen,

Carlsbad, CA, USA) Five micrograms of total RNA was

separated on a 15% denaturing polyacrylamide gel

contain-ing 8 m urea, and was blotted accordcontain-ing to standard

proce-dures Biotin-labeled probes were purchased from MWG

Biotech Prehybridization and hybridization were carried out

in 0.25 m sodium phosphate (pH 7.2), 7% SDS, and 0.5%

sodium pyrophosphate After hybridization, the membrane

was washed in 2· SSC and 1% SDS at 37 C The biotin

signal was detected using the Chemiluminescent Nucleic

Acid Detection Module kit (Pierce, Rockford, IL, USA)

Acknowledgements

We thank Dr Hee-Chan Seo for technical advice and

the Faculty of Mathematics and Natural Sciences at

the University of Bergen for special support

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Supplementary material

The following supplementary material is available online:

Fig S1 Northern blot analysis of the effects of siRNA injections on endogenous levels of different miRNAs Fig S2 Expression of the pax2a gene at the MMB is affected by siRNA injection

Fig S3 Rescue of siSix3a-induced MMB and tail defects by coinjection of miR-430b

Fig S4 Changes in the endogenous level of miR-430b following injection of different amounts of siGFP Each column represents the average level of the mature form of miR-430 (relative to the wild-type), obtained from three different experiments

This material is available as part of the online article from http://www.blackwell-synergy.com

Please note: Blackwell Publishing are not responsible for the content or functionality of any supplementary materials supplied by the authors Any queries (other than missing material) should be directed to the corre-sponding author for the article

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